反铁电相变陶瓷低频发射换能器

在具有高阶形式的广义压电方程基础上,讨论掺镧改性锆锡钛酸铅PbLa(Zr,Sn,Ti)O3(PLZST)反铁电相变陶瓷的非线性机电耦合问题,得到类似传统线性压电方程的近似线性电致伸缩方程,给出了一种解决非线性反铁电相变陶瓷换能器电声转换问题的分析方法,即在直流偏置状态下对PLZST反铁电相变陶瓷的材料参数进行近似线性等效化处理进而分析换能器的电声转换问题.在此基础上,研制了水中谐振频率1.1 kHz新型反铁电相变陶瓷低频弯张换能器.湖上试验结果表明,与同结构同尺寸压电陶瓷弯张换能器相比,目前反铁电换能器样品的发射电压响应约高3dB,声源级高出9dB,并验证了本文所提出的分析非线性反铁电相变陶瓷换能器方法的正确性.     

两个非平行波导间的能量转换

提出一种分析非平行波导间耦合的简明方法-耦合系数推广法.利用这种方法,导出一种新的非平行双波导的耦合方程,由此得到一组非平行波导耦合的完美的分析解,依据这些分析解可以优化非平行波导的传输距离、输入／输出端口波导间距和夹角.     

固体中微裂纹系统统计演化的基本描述

本文建议了一种在外界载荷作用下,在固体中产生的微损伤的统计演化的理论描述方法。特别是,作为一个例子,讨论了理想微裂纹系统,以便了解在微裂纹成核和扩展过程中,损伤演化的基本行为。本文也简单讨论了有关的平均损伤函数。     

损伤统计演化方程的性质和数值模拟

通过对一种含成核尺寸效应的损伤统计演化方程性质的分析和数值模拟,揭示了损伤率主要是由微损伤在二维相空间中的前沿的运动所决定的这也就是Kachanov提出的损伤率演化方程的物理基础数值结果进一步显示了含成核尺寸效应模型在损伤发展上与-维模型的区别而且,由几种形式的细观动力学算出的损伤率与损伤的关系简单,可近似拟合为宏观上封闭的形式     

UPLC fingerprint analysis and identification of flavonoids in Scutellaria indica by UFLC-triple-quadrupole time-of-flight mass spectrometry

The aim of this study was to raise the quality control level of Scutellaria indica. A quick and stable ultra performance liquid chromatography method was established for the fingerprint analysis of S. indica. A total of 32 common peaks were marked with 10 batches S. indica detected in 30?min using similarity evaluation system for chromatographic fingerprint of traditional Chinese medicine (2004A version). Besides, a high-resolution mass spectrometer was used to identify flavonoids in S. indica. A total of 27 flavonoids in S. indica were identified. And a series of fragmentation regularities were obtained, which could be used for the identification of other flavonoids. Therefore, the established liquid chromatography–tandem mass spectrometer method could be successfully utilized for the quality control of S. indica.     

胆固醇分子印迹聚合物的制备及其选择性吸附

随着人们生活水平的逐步提高,因人体内胆固醇过高所产生的疾病呈逐年增加的趋势.近年来的研究表明,胆固醇分子印迹聚合物对胆固醇具有良好的选择性吸附能力.将胆固醇分子印迹聚合物作为胆固醇的识别剂,提取食品中的胆固醇和治疔胆固醇有关的疾病,展现出了良好的应用前景.本文分别从胆固醇分子印迹聚合物的制备方法、识别机理、提高选择性识别途径以及新的印迹方法等方面进行了综述.     

Facile one-pot synthesis of yolk-shell superparamagnetic nanocomposites via ternary phase separations

Yolk-shell composites with an Fe(3)O(4)/silica hybrid shell and a polymer core are prepared via a facile one-pot and self-template process. Thicknesses of the inorganic shell and interior space of the composites are well controlled by tuning the ternary phase separations.     

Influences of travelling magnetic field on the dendritic structures of Sn–1.8Cd peritectic alloy during directional solidification

The effects of melt flow driven by a travelling magnetic field (TMF) on solidification structures of Sn–1.8 wt.% Cd peritectic alloy have been investigated numerically and experimentally. Numerical results indicate that the flow velocity at the solid–liquid interface under a downward TMF is smaller than that under an upward TMF. The experimental results show that the growth directions of dendrites are chaotic, and several crotches among the dendrites are observed at the solid–liquid interface in the case of no field. It is concluded from TMF results that the ordered growth of dendrites at two different directions occurs, and only one crotch among the dendrites appears at the solid–liquid interface. The location of the crotch gradually approaches the interface center with increasing magnetic field intensity (B≤10.3 mT). Moreover, the growth of high-order branches occurs at the crotch under a downward TMF. A simple model is established for explanation and it well corresponds to the experimental results.     

Differential algebraic method for time of flight property of electrostatic electron lenses

Differential algebraic method is a powerful technique in computer numerical analysis. It presents a straightforward method for computing arbitrary order derivatives of functions with extreme high accuracy limited only by the truncation error of the computer. When applied to nonlinear dynamical systems, the arbitrary high-order transfer properties of the systems can be computed directly with high precision. In this article, the time of flight (TOF) property of electrostatic electron lens systems is studied by differential algebraic method and their arbitrary order TOF transfer properties can be numerically calculated. As an example, Schiske's model electrostatic lens has been studied by the efficient differential algebraic TOF method.     

CHARACTERISTIC DIMENSIONLESS NUMBERS IN MULTl-SCALE AND RATE-DEPENDENT PROCESSES

Multi-scale modeling of materials properties and chemical processes has drawn great attention from science and engineering. For these multi-scale and rate-dependent processes, how to characterize their trans-scale for-mulation is a key point. Three questions should be addressed:How do multi-sizes affect the problems?How are length scales coupled with time scales?How to identify emergence of new structure in process and its effect?For this sake, the macroscopic equations of mechanics and the kinetic equations of the microstructural transforma-tions should form a unified set that be solved simultaneously.As a case study of coupling length and time scales, the trans-scale formulation of wave-induced damage evolution due to mesoscopic nucleation and growth is discussed. In this problem, the trans-scaling could be reduced to two inde-pendent dimensionless numbers: the imposed Deborah number De=(ac)/(LV) and the intrinsic Deborah num-ber D = (nNc5)/V* ,where a. L, c, V and nN are wave speed, sample size, micr