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61.
The paper presents construction and principle of operation of passive IR detectors (PIR detectors) of a large detection range.
Important virtue of these detectors is highly efficient detection of slowly moving or crawling people. The described here
PIR detector detects crawling people at the distance of 140 m. To ensure high probability of detection of slowly moving objects,
new method of signals analysis was applied. On the basis of the carried out real-time measurements, both probability of detection
and false alarms were determined. 相似文献
62.
S.?Pi?olEmail author M.?Najib D.?M.?Bastidas A.?Calleja X.?G.?Capdevila M.?Segarra F.?Espiell J.?C.?Ruiz-Morales D.?Marrero-López P.?Nu?ez 《Journal of Solid State Electrochemistry》2004,8(9):650-654
We have prepared pure electrolytes of Ce0.8Gd0.2O1.9 (CGO) and Ce0.8Sm0.2O1.9 (CSO), useful for SOFCs, by a sol–gel-related technique like the acrylamide method. This method consists of preparing a solution from the single oxides followed by gelation. Then, the combustion or decomposition of the organic molecules is initiated, producing nanometric calcined powders of the above-mentioned compounds. Thermal treatments were optimized in order to obtain good electrochemical properties of the electrolytes. We have observed that the synthesis temperature to obtain the pure phase is lower for the sol–gel samples than for the pellets prepared by solid-state reaction, and the final density is higher. The microstructure and composition of the powders were characterized by TEM, SEM, and EDX analysis. The electrical properties of the electrolytes were measured by impedance spectroscopy at different temperatures and oxygen partial pressures.Presented at the OSSEP Workshop Ionic and Mixed Conductors: Methods and Processes, Aveiro, Portugal, 10–12 April 2003 相似文献
63.
Monosized poly(styrene/N-[3-(dimethylamino)propyl]methacrylamide/poly(ethylene glycol) ethyl ether methacrylate) [poly(St/PEG-EEM/DMAPM)] cationic nanoparticles were synthesized by emulsifier-free emulsion polymerization conducted in the presence of a cationic initiator, 2,2-azobis(2-methylpropionamidine) dihydrochloride (APDH or V-50). Particle sizes and surface charge densities were measured with a Zeta Sizer. The structure of the terpolymers was determined by Fourier transform IR and 1H NMR spectroscopies. The amounts of the main monomer (St), cationic comonomer (DMAPM), stabilizer (PEG-EEM), and initiator (APDH), and the water-to-monomer phase ratio were all effective on both the average size and the surface charge of the nanoparicles. The average particle size was in the range 75–400 nm depending on the recipe applied; it decreased on increasing the amount of DMAP or PEG-EEM or the water-to-monomer phase ratio in the feed, while it increased with increasing St or APDH content. These nanoparticles were quite monodisperse with a polydispersity index of 1.008–1.14. 相似文献
64.
In this paper, we study orthogonal polynomials with respect to the bilinear form (f, g)
S
= V(f) A
V(g)
T
+ <u, f
(N)
g
(N)V(f) =(f(c
0), f "(c
0), ..., f
(n – 1)
0(c
0), ..., f(c
p
), f "(c
p
), ..., f
(n – 1)
p(c
p
))
u is a regular linear functional on the linear space P of real polynomials, c
0, c
1, ..., c
p
are distinct real numbers, n
0, n
1, ..., n
p
are positive integer numbers, N=n
0+n
1+...+n
p
, and A is a N × N real matrix with all its principal submatrices nonsingular. We establish relations with the theory of interpolation and approximation. 相似文献
65.
Using a density functional method, we investigate the properties of liquid 4He droplets doped with atoms (Ne and Xe) and molecules ( SF6 and hydrogen cyanide). We consider the case of droplets having a quantized vortex pinned to the dopant. A liquid-drop formula is proposed that accurately describes the total energy of the complex and allows one to extrapolate the density functional results to large N. For a given impurity, we find that the formation of a dopant+vortex+(4)He(N) complex is energetically favored below a critical size N(cr). Our results support the possibility to observe quantized vortices in helium droplets by means of spectroscopic techniques. 相似文献
66.
Ailan Qu Xiufang Wen Pihui Pi Jiang Cheng Zhuoru Yang 《Applied Surface Science》2007,253(24):9430-9434
A superhydrophobic surface originated from quincunx-shape composite particles was obtained by utilizing the encapsulation and graft of silica particles to control the surface chemistry and morphology of the hybrid film. The composite particles make the surface of film form a composite interface with irregular binary structure to trap air between the substrate surface and the liquid droplets which plays an essential role in obtaining high water contact angle and low water contact angle hysteresis. The water contact angle on the hybrid film is determined to be 154 ± 2° and the contact angle hysteresis is less than 5°. This is expected to be a simple and practical method for preparing self-cleaning hydrophobic surfaces on large area. 相似文献
67.
Hui Fang Pi Peng Zhang Han Li Ruan Yong Hui Zhang Han Dong Sun Ji Zhou Wu 《中国化学快报》2009,20(11):1319-1320
A new alkaloid was isolated from the bulbs of Lycoris aurea(L'Herit.) Herb.Its structure was established as 3-o-ethyltazettinol through chemical and spectroscopic studies including 2D NMR. 相似文献
68.
Yong Wang Xinyi Cao Jingfei Ji Xiuling Cui Chao Pi Leyao Zhao Yangjie Wu 《中国化学快报》2021,32(5):1696-1700
A green tandem reaction, including insertion/aerobic oxidation/bisindolylation, starting from indoles and diazo compounds has been developed. The combination of water and fluorinated alcohol plays dual roles as solvent and promoter in this chemical transformation. Molecular oxygen in the air acts as an oxidant. 3,3′-Bis(indolyl)methanes with quaternary carbon were produced under metal-free conditions. No any catalyst and additive were required. N2 and water were released as sole by-products. Absence of water and fluorinated alcohol resulted in Wolff rearrangement product. 相似文献
69.
The suitability of thallium halide electrodeless discharge tubes as a radiation source for atomic fluorescence was investigated. Effects of various parameters, affecting the emission intensities, were investigated. 相似文献
70.
An enzyme-linked immunometric assay for cortisol based on idiotype-anti-idiotype reactions 总被引:1,自引:0,他引:1
Cortisol levels in body fluids are useful for monitoring the function of the pituitary-adrenal axis. Here, we established an “enzyme-linked immunometric assay” (a noncompetitive-type ELISA) for cortisol based on idiotype-anti-idiotype reactions. Six different anti-idiotype monoclonal antibodies that recognized the variable regions of a newly established anti-cortisol antibody were generated using hybridoma technology; these were two β-type and four α-type anti-idiotype antibodies, recognizing the paratope and framework regions, respectively. An immunometric assay was established using a combination of a selected α-type and a selected β-type antibody. The analyte (cortisol) was captured by an excess amount of anti-cortisol antibody immobilized on microplates, and the unoccupied paratope was saturated with the β-type antibody. Hapten-occupied anti-cortisol antibody, with less steric hindrance, was then selectively bound by the α-type antibody, labeled with biotin. The amount of biotin residue on the microplates was colorimetrically monitored using a peroxidase-labeled streptavidin. This assay had an approximately threefold higher sensitivity (detection limit: 90 pg = 248 fmol cortisol) than a competitive ELISA using the same anti-cortisol antibody, as well as a practical specificity for providing reasonable determination of normal urinary cortisol levels. 相似文献