抗缺氧藏药中微量及宏量元素的测定

用HNO₃-HClO₄(4∶1) 混酸作消化液对红景天胶囊、安神散、五味石榴散、章松八味沉香散、十六味杜鹃散、二十五味余甘子丸、二十五味竹黄胶囊、十五味龙胆丸、秘诀清凉散、七十味珍珠丸、八味沉香散、六味丁香散和七味葡萄散等13种抗缺氧藏成药进行消化,采用火焰原子吸收分光光法测定了其中银、铝、镉、钴、铬、铜、铁、汞、镁、锰、镍、铅、锡和锌等14种微量及宏量元素的含量。结果表明,抗缺氧藏成药中含有比较丰富的铁、镁、铜、铬、锌及锰等微量元素。为探讨微量、宏量元素与藏成药抗氧化作用之间的关系提供了有用的数据。     

Spectrally scanned,repetitively pulsed erbium-doped fiber laser for spectral and temporal multiplexing of fiber Bragg grating sensors

An erbium-doped fiber laser that emits a series of spectrally scanned pulses is used to monitor an array of fiber Bragg grating (FBG) sensors. The cavity for this Fabry-Perot laser is formed by two spectrally selective reflectors: a rotating mirror-grating combination for scanning the reflectance peak wavelength and a fiber Fabry-Perot interferometer (FFPI) with a periodic reflectance spectrum. During a scan of the rotating mirror, the laser produces a set of Q-switched pulses over the 1522-1568-nm spectral range at each of the FFPI reflectance peak wavelengths. This laser is used to simultaneously demonstrate wavelength-division multiplexing of FBGs with reflectance peaks in different spectral regimes and time-division multiplexing of FBGs with overlapping spectra. The spectral location of the FBG peaks was determined to an accuracy of 1.4 pm.     

旋量值函数的Plemelj公式

对比于多复变中的Bochner-Martinelli型积分的Plernelj公式,定义了艾米尔特Clifford分析中旋量值函数的Cauchy型积分及Cauchy主值积分,得到了旋量值函数的Plemelj公式,最后给出一些特殊情形的Bochner-Martinelli型积分的Plemelj公式.     

关于求各向异性介质中电磁场的格林张量函数的一个方法

本文提出一个方法,来推求在(3)式中所定义的、在全空间中的格林张量函数。它有时亦称为对应微分方程的基本解。这个方法是以富氏变换为基础。由于问题的复杂性,我们不得不作某些近似。首先,把各向异性介质分为两类,一类是磁迴旋介质,另一类是电迴旋介质。对于磁迴旋介质,如铁氧体,取μ为张量而ε为标量。而对电迴旋介质,如等离子体,取ε为张量而μ为标量。其次,由于矩阵μ_p非常小(在(15)式中定义),我们可以把解展为μ_p的冪级数,并计算出一级近似。具体结果在式(23)、(25)、(28)、(32)和(33)中表示。最后对Г函数的物理意义和它的渐近展开式的有效范围作了讨论。     

Preparation and Cellular Uptake of pH‐Dependent Fluorescent Single‐Wall Carbon Nanotubes

Fluorescent single‐wall carbon nanotubes (SWCNTs) were prepared by mixing cut SWCNTs with acridine orange (AO). The optical absorbance and fluorescence characteristics of AO–SWCNT conjugates display interesting pH‐dependent properties. Fluorescence microscopy in combination with transmission electron microscopy proves that AO–SWCNTs can enter HeLa cells and are located inside lysosomes. The endocytosis‐inhibiting tests show that the clathrin‐mediated endocytosis is a key step in the internalization process. The internalized AO–SWCNTs remain inside lysosomes for more than a week and have little effect on cell proliferation. These findings may be useful in understanding the SWCNT‐based intracellular drug delivery mechanism and help to develop new intracellular drug transporters.     

考虑水压效应的基坑边坡稳定性计算分析

地下水的存在给工程带来了巨大的隐患。如何研究分析地下水对工程的作用是地质工程界的一个重点和难点。本文基于地下水的破坏效应,分析研究了地下水引起的接触面积的变化,并推导了饱水情况下平面滑动的临界角变化公式。A^* 越小,即λ越小,发生失稳破坏的临界角θ就越小。而地下水p的增加有助于A^* 的减小,造成了在水压作用下土体更容易发生失稳破坏。     

PMD and CD Characterization of Chirped FBG Using Microwave Photonic Technique

We present and demonstrate experimentally a new method for measuring the polarization-mode-dispersion(PMD) of a Chirped Fiber Bragg Grating. The technique has also been applied to accurate chromatic dispersion evaluation by removing the influence of PMD.     

Ionic liquid foam floatation coupled with ionic liquid dispersive liquid–liquid microextraction for the separation and determination of estrogens in water samples by high‐performance liquid chromatography with fluorescence detection

An ionic liquid foam floatation coupled with ionic liquid dispersive liquid–liquid microextraction method was proposed for the extraction and concentration of 17‐α‐estradiol, 17‐β‐estradiol‐benzoate, and quinestrol in environmental water samples by high‐performance liquid chromatography with fluorescence detection. 1‐Hexyl‐3‐methylimidazolium tetrafluoroborate was applied as foaming agent in the foam flotation process and dispersive solvent in microextraction. The introduction of the ion‐pairing and salting‐out agent NH₄PF₆ was beneficial to the improvement of recoveries for the hydrophobic ionic liquid phase and analytes. Parameters of the proposed method including concentration of 1‐hexyl‐3‐methylimidazolium tetrafluoroborate, flow rate of carrier gas, floatation time, types and concentration of ionic liquids, salt concentration in samples, extraction time, and centrifugation time were evaluated. The recoveries were between 98 and 105% with relative standard deviations lower than 7% for lake water and well water samples. The isolation of the target compounds from the water was found to be efficient, and the enrichment factors ranged from 4445 to 4632. This developing method is free of volatile organic solvents compared with regular extraction. Based on the unique properties of ionic liquids, the application of foam floatation, and dispersive liquid–liquid microextraction was widened.     

Hydrodynamic properties of squirmer swimming in power-law fluid near a wall

Hydrodynamic properties of squirmer swimming in power-law fluid near a wall considering the interaction between squirmer and wall are numerically studied with an immersed boundary-lattice Boltzmann method. The power-law index, Reynolds number, initial orientation angle of squirmer, and initial distance of squirmer from the wall are all taken into account to investigate the swimming characteristics for pusher (β?<?0), neutral squirmer (β?=?0), and puller (β?>?0) (three kinds of swimmer types) near the no-slip boundary. Four new kinds of swimming modes are found. Results show that, for the pushers and pullers, the wall displays an increasing attraction with increasing power-law index n, which differs from the neutral squirmer who always departs from the wall after the first collision with the wall. Both the initial orientation angle and initial distance from the wall only affect the moving situations rather than the moving modes of the squirmers. However, the squirmers depart from the wall as the Reynolds number increases and chaotic orbits appear for some squirmers at Re?=?5. Several typical flow fields are analyzed and the power consumption and torque for different kinds of flows are also studied. It is found that, as the absolute value of β increases, the power consumption generally increases in shear-thinning (n?=?0.4), Newtonian (n?=?1), and shear-thickening (n?=?1.6) fluids. Moreover, the pushers (β?<?0) and the pullers (β?>?0) expend almost the same power if the absolute value of β remains the same. In addition, the power consumption of the squirmers is highly dependent on the power-law index n.