甲壳素预富集－火焰原子吸收分光光度法测定痕量铜

利用甲壳素对金属离子的选择性吸附，研究了甲壳素快速吸附铜离子的吸附条件和洗脱条件，在火焰原子吸收分光光度计上进行铜的测定，方法简单快速，检出限为８．０ｎｇ／ｍＬ，精密度ＲＳＤ为３．６％，用于矿样中痕量铜的测定，分析结果与推荐值相吻合。     

一种新型的光纤锥形耦合器

提出了一种光纤波导折射率渐变的新型锥形（Taper）耦合器件，其原理是基于光纤中Ge缺陷在紫外光照射下而产生的光致折射率的变化。利用光纤在高压、低温下渗氢技术使单模光纤的光致折射率变化△n达6×10-3数量级；通过控制曝光条件就可以在光纤中产生一定规律的锥形结构，使单模光纤的模场半径由4．8μm缩小到3．2μm。由耦合波理论分析表明该器件具有较好的基模传输特性。     

Dynamics of bid–ask spread return and volatility of the Chinese stock market

The bid–ask spread is taken as an important measure of the financial market liquidity. In this article, we study the dynamics of the spread return and the spread volatility of four liquid stocks in the Chinese stock market, including the memory effect and the multifractal nature. By investigating the autocorrelation function and the Detrended Fluctuation Analysis (DFA), we find that the spread return is the lack of long-range memory, while the spread volatility is long-range time correlated. Besides, the spread volatilities of different stocks present long-range cross-correlations. Moreover, by applying the Multifractal Detrended Fluctuation Analysis (MF-DFA), the spread return is observed to possess a strong multifractality, which is similar to the dynamics of a variety of financial quantities. Different from the spread return, the spread volatility exhibits a weak multifractal nature.     

Thermodynamic and physical properties of FeAl and Fe3Al: an atomistic study by EAM simulation

With this work we present a newly developed potential for the Fe–Al system, which is based on the analytical embedded atom method (EAM) with long range atomic interactions. The potential yields for the two most relevant phases B2-FeAl and D0₃-Fe₃Al lattice constants, elastic constants, as well as bulk and point defect formation enthalpies, which are in good agreement with experimental and other theoretical data. In addition, the phonon dispersions for B2-FeAl and D0₃-Fe₃Al show a good agreement with available experiments. The calculated lattice constants and formation enthalpy for disordered Fe–Al alloys are in good agreement with experimental data or other theoretical calculations. This indicates that the present EAM potentials of Fe–Al system is suitable for atomistic simulations of structural and kinetic properties for the Fe–Al system.     

A novel Si-based photodetector with flat-top and steep-edge spectral response

To meet the requirement of the dense wavelength-division-multiplexed (DWDM) system and optoelectronic integrated circuit, we design a Si-Based InGaAs photodetector, which is fabricated by bonding InGaAs/InP photodetector on a Si-Based dielectric film Fabry–Perot filter. The photodetector can exhibit an extremely good flat-top and steep-edge spectral response through designing the structure of Si-Based dielectric film Fabry–Perot filter. The simulation result of phtodetector demonstrates that the spectral response linewidth, ?at-top and steep-edge characteristics of these photodetectors are suitable to be used in 50 GHz, 100 GHz, 200 GHz DWDM system.     

一种基于~4He气闪烁体的裂变中子探测器

研制了一种新中子探测器,它以²³⁵UO₂裂变靶作为转换靶,⁴He气体作为闪烁体.该探测器充分结合了²³⁵U和⁴He两种核素的特点,从而具有中子能量响应平坦、中子灵敏度较高、n/γ分辨本领高等优点,能很好地在混合脉冲裂变辐射场中测量中子.本文对探测器的原理和结构设计进行了介绍,计算了不同能量中子、γ射线在探测器中的能量沉积,并从理论和实验上对探测器的中子灵敏度、γ射线灵敏度、n/γ分辨本领和时间响应进行了研究.结果表明探测器的中子灵敏度约10^-15C·cm²,γ灵敏度约10^-17C·cm²,时间响应约33.1 ns.     

快放电直线型变压器驱动源磁芯脉冲损耗特性

建立了快脉冲磁芯损耗特性测试平台,对比研究了50 m的DG6硅钢和25 m的2605TCA非晶两种材料磁芯损耗特性;采用一种新的特征参量(磁芯单位面积上激磁电压陡度)来规范磁芯的激磁电压条件,使得实验结果与快放电直线型变压器驱动源实际工作条件下磁芯性能具有可比性;通过测量初级漏电流及次级开路电压,获得了相同激磁条件下两种磁芯等效损耗电阻的大小,50 m 的DG6硅钢磁芯损耗约为25 m的2605TCA非晶磁芯损耗的4倍;计算了两种材料磁芯总损耗中涡流损耗所占的比例,50 m的DG6硅钢磁芯涡流损耗占总损耗的75%,25 m的2605TCA非晶磁芯涡流损耗占总损耗的28%。     

微分吸收法测量二极管电压

给出了微分吸收法测量二极管电压的基本原理和实验结果。利用MCNP程序对轫致辐射-衰减-探测器系统建模,模拟得到了输出剂量与二极管工作电压关系拟合曲线。建立了微分吸收法测量二极管电压测量系统,通过在探测器前端放置不同厚度的吸收片,得到了衰减程度不同的波形。结合理论计算的拟合曲线和实验波形,利用迭代法计算得到了晨光号加速器二极管电压,电压峰值为0.58 MV。和传统方法所测得二极管工作电压进行了比较,结果较为一致。     

Evolution of the 251 cm-1 infrared phonon mode with temperature in Ba0.6K0.4Fe2As2

The far-infrared optical reflectivity of an optimally doped Ba1-xKxFe2As2(x =0.4) single crystal is measured from room temperature down to 4 K. We study the temperature dependence of the in-plane infrared-active phonon at 251 cm-1 . This phonon exhibits a symmetric line shape in the optical conductivity, suggesting that the coupling between the phonon and the electronic background is weak. Upon cooling down, the frequency of this phonon continuously increases, following the conventional temperature dependence expected in the absence of a structural or magnetic transition. The intensity of this phonon is temperature independent within the measurement accuracy. These observations indicate that the structural and magnetic phase transition might be completely suppressed by chemical doping in the optimally doped Ba0.6K0.4Fe2As2 compound.     

Interstitial vortex in superconducting film with periodic hole arrays

The response of superconducting Nb films with a diluted triangular and square array of holes to a perpendicular magnetic field are investigated.Due to small edge-to-edge separation of the holes,the patterned films are similar to multi-connected superconducting islands.Two regions in the magnetoresistance R(H) curves can be identified according to the field intervals of the resistance minima.Moreover,in between these two regions,variation of the minima spacing was observed.Our results provide strong evidence of the coexistence of interstitial vortices in the islands and fluxoids in the holes.