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851.
Gallium Nitride (GaN) room temperature α particle detectors are fabricated and characterized, whose device structure is Schottky diode. The current-voltage (I- V) measurements reveal that the reverse breakdown voltage of the detectors is more than 200 V owing to the consummate fabrication processes, and that the Schottky barrier and ideal factor of the detectors are 0.64 eV and 1.02, respectively, calculated from the thermionic transmission model. ^241Am α particles pulse height spectra from the GaN detectors biased at -8 V is obviously one Gauss peak located at channel 44 with the full width at half maximum (FWHM) of 15.87 in channel. One of the main reasons for the relatively wider FWHM is that the air between the detectors and isotope could widen the spectrum.  相似文献   
852.
The purpose of this study was to determine the effect of the combination of hydroxyapatite (HA) and bioglass (BG) on polyethylene terephthalate (PET) artificial ligament graft osseointegration within the bone tunnel. The results of in vitro culturing of MC3T3-E1 mouse osteoblastic cells proved that this HA/BG composite coating can promote the cell compatibility of grafts. A rabbit extraarticular tendon-to-bone healing model was used to evaluate the effect of this composite coating on PET artificial ligaments in vivo. The final results demonstrated that HA/BG coating improved new bone formation at the graft-bone interface and increased the load-to-failure property of graft in bone tunnel compared to the control group at early time. The study has shown that HA/BG composite coating on the PET artificial ligament surface has a positive effect in the induction of artificial ligament osseointegration within the bone tunnel.  相似文献   
853.
854.
Benzyl sulfonamide/alcohol‐tethered alkylidenecyclopropanes undergo a rhodium‐catalyzed and substrate‐controlled selective C?C bond activation, producing three types of common organic structural units: benzo[c]azepine/oxepines, dihydronaphthalen‐1‐amines, and conjugated dienes. Epoxidation and aromatization of these products to construct two useful compounds have also been achieved.  相似文献   
855.
856.
857.
FT Raman investigation of sodium cellulose sulfates (NaCS) was reported. Different NaCS were prepared by two diverse sulfation methods and their total degrees of substitution (DS) of sulfate groups were determined through either 13C-NMR spectroscopy or elemental analysis. Subsequently, these NaCS were characterized with FT Raman spectroscopy. The caused bands through the introduction of the sulfate groups in cellulose chain were explained and assigned. Additionally, a strong linear correlation between the areas under the bands ascribed to the stretching vibrations of C–O–S groups and the total DS of NaCS was presented. A rapid method of quantifying the total DS of NaCS was established. Finally, sodium sulfate (Na2SO4), a salt that is very often produced during the sulfation of cellulose, was found to be analyzable even with a weight content of 0.12% in NaCS. The method of quantifying the content of this salt in NaCS was investigated with Raman spectroscopy.  相似文献   
858.
859.
茉莉花是我国的健康饮品,由于茉莉花具有药食两用功效,本实验对茉莉花中7种金属元素含量进行了研究,结果表明,茉莉花中含有丰富的人体所必需的金属矿质元素,K、Ca、Mg的含量较多,具有较高的开发利用价值,但不同金属元素含量存在差异。同时对茉莉花进行了全量浸提,不同元素的浸提率存在一定的差异,其中K的浸出率最高。研究结果对人们日常正确选择饮用花茶提供了一定的理论依据,具有一定的实际意义和推广价值。  相似文献   
860.
This paper describes three inexpensive and fast analytical methods to characterise grafted particle surfaces. The reaction of silica with (3-aminopropyl)triethoxysilane, (3-mercaptopropyl)trimethoxysilane and N-(phosphonomethyl)iminodiacetic acid hydrate, respectively, leads to NH2-, SO3H- or COOH-functionalised silica, which were characterised by X-ray photoelectron spectrometry and titration in nonaqueous media as well as with two titration methods in a water-based environment. In the work presented, factors influencing the titrations are pointed out and solutions are presented to overcome these limiting factors are shown.  相似文献   
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