高温超导体Hg0.9Tl0.2Ba2Ca2Cu3O8+δ的热导

测量了高温超Ｈｇ０．９Ｔｌ０．２Ｂａ２Ｃａ２Ｃｕ３Ｏ８＋δ的热导率,温度范围为２０～３００Ｋ。在超导转变温度Ｔｃ以下观察到热导率明显的增加。在６５Ｋ（～０．５Ｔｃ）附近,超导体的热导率表达到了一个宽的极大,热导率的极大值为的１．６倍。用正常态电子散射的模型对实验结果进行了拟合。     

Solid-Phase Microextraction Followed by Gas Chromatography-Mass Spectrometry Analysis of the Volatile Components of Flos Chrysanthemi indici in Different Growing Areas

Headspace solid phase microextraction coupled with gas chromatography-mass spectrometry (HS-SPME-GC-MS) has been applied to the determination of the volatile compounds of a common traditional Chinese medicine , Flos Chrysanthemi indici. Twenty-six compounds were identified by the present method, which are similar to the results from steam distillation. Difference in analysis from ten growing areas was found to be in their relative content and total concentrations. Four active compounds (cineole, 3-thujanone, borneol and bornyl acetate) were applied to the evaluation of the quality of Flos Chrysanthemi indici from different areas. By comparing their peak areas, it was found that Flos Chrysanthemi indici with the best quality was from Hangzhou in China. These results show that HS-SPME-GC-MS is a simple, rapid and solvent-free method for the analysis of the volatile compounds in this material and a potential tool for its quality assurance.     

A PREDATOR-PREY SYSTEM WITH STAGE STRUCTURE AND HARVESTING FOR PREDATOR

In this paper, we consider a predator-prey system with stage structure and harvesting (where the predator population has two stages, an immature stage and a mature stage with harvesting, and the growth of the prey population is of Lotka-Volterra nature). We obtain the conditions of the globally asymptotic stability for three nonne-gative equilibria of this system.     

ISOLATION AND CHARACTERIZATION OF THE PRESUMED PHOTORECEPTOR PROTEIN OF Blepharisma japonicum

Abstract— Photosensory responses in the ciliated protozoan Blepharisma japonicum are mediated by a hypericin-like chromophore, blepharismin, localized in granules distributed under the cell membrane. A blepharismin-binding protein, with an apparcnt molecular weight ranging between 35 and 38 kDa, has been isolated by means of column separations and preparative isoelectric focusing and characterized by means of gel electrophoresis, analytic isoelectric focusing as well as absorption and fluorescence spectroscopy.     

TBP萃淋树脂吸附钪的性能研究及应用

本文采用静动态两种方法较系统地研究了TBP草淋树脂在高氟酸介质中吸附钪的性能，并用自己设计的减压微色谱柱考察了共存离子的萃取色谱行为，选择了分离微量钪的最佳条件，获得了良好的分离效果，用于标准矿样中微量机的测定，分析结果与标准值相近。     

瞬态功率光限幅实验

应用单脉冲时间分辨技术测量了富勒烯溶液瞬态功率光限幅特性。在激发波长为532nm,脉冲宽度为8ns,峰值功率密度达到180MW/cm²的条件下,其瞬态功率光限幅的开关速度约为5ns.     

测量液体粘滞系数实验的研究

本文利用液体的绝对速度理论得到液体的粘滞系数随温度变化的关系式，在不同的温度下测得液体的粘滞系数，找出液体的粘滞系数随温度变化的数学表达式。     

The nature of the lowest triplet configuration of flavins

Abstract— The phosphorescence spectrum of riboflavin has been reexamined at 77°K in an ethylene glycol: water matrix. The phosphorescence occurs at approximately the 605 nm (ca. 2-·05 eV) region, in reasonable agreement with the theoretical calculations of 1·6–1·8 eV [21]. The emission was found to be negatively polarized, and to have a relatively long lifetime (0·56 sec). On the basis of this data and additional theoretical results, it is concluded that the lowest triplet of riboflavin is of ³(τ,τ*) type. Upon addition of potassium iodide, the phosphorescence emission is enhanced through spin-orbit perturbation. The presence of oxygen (atmospheric pressure) in the frozen glass apparently has no effect on the emission. The phosphorescence spectra of alloxazine are also presented. Results of the present work have been applied to the photodephosphorylation of menadiol diphosphate in elucidating its mechan ism involving the riboflavin triplet and singlet oxygen.     

Crystal structure and properties of FeSr2NdCu2O7+δ

The compound FeSr₂NdCu₂O₇₊ (Fe1212) was successfully synthesized by solid-state reaction. X-ray diffraction data indicate that the sample is of single phase. Rietveld whole-pattern-fitting method was used to refine the crystal structure of samples prepared under different annealing conditions using the tetragonal system with space group P4/mmm. Magnetization measurements indicate that magnetic susceptibility changes with temperature in a Curie-type manner. Resistance measurements indicate that these samples have a semiconductor-like behavior. PACS 61.10.Nz; 74.72.Jt