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121.
本文提出了一种新的测定间三联苯和对三联苯的同步扫描-SS-RTP法。固体基质选用慢速定量滤纸,重原子盐为Tl2SO4。以激发单色器和发射单色器的波长差△λ=180nm进行同步扫描,其同步特征峰间三联苯为450nm,对三联苯为490nm(均指发射波长)。间三联苯可直接由该特征峰的高度进行定量测定。对三联苯在490nm处的特征峰略受间三联苯同步拖尾的影响,其峰值信号需加校正。间三联苯和对三联苯的线性范围分别为0.46~92ng/斑点和0.46~46ng/斑点 相似文献
122.
123.
建立反相-高效液相色谱法(RP-HPLC)测定罗勒(Ocimum basilicumL.)中石吊兰素的含量。用Microsorb-M V 100-5C18(4.6mm×250mm,5μm)色谱柱,甲醇:1%醋酸=86:14(V/V)为流动相,流速为0.5mL/min,检测波长为335nm。石吊兰素浓度在0.27—32.4μg/mL范围内与峰面积线性关系良好(r=0.9999),方法平均回收率大于99%(n=9)。方法简单、可靠,可应用于罗勒植物中石吊兰素的含量测定。 相似文献
124.
We experimentally analyze the heat capacity and thermal expansion of reference solids in a wide temperature range from several Kelvin to melting temperature,and establish a universal double-linear relation between the experimental heat capacity Cp and thermal expansion β,which is different from the previous models.The universal behavior between heat capacity and thermal expansion is important to predict the thermodynamic parameters at constant pressure,and is helpful for understanding the nature of thermal properties in solids. 相似文献
125.
Huaming?YangEmail author Guanzhou?Qiu Xiangchao?Zhang Aidong?Tang Wuguo?Yang 《Journal of nanoparticle research》2004,6(5):539-542
CdO nanoparticles of 43 nm in crystal size were successfully synthesized by the mechanochemical reaction (CdCl2 + Na2CO3) with NaCl as a diluent and subsequent thermal treatment at 700°C for 2 h. The samples were characterized by differential thermal analysis (DTA), thermogravimetric analysis (TGA), X-ray diffraction (XRD) and transmission electron microscopy (TEM). Effect of calcination temperature on the crystal size of CdO nanoparticles was primarily investigated. The apparent activation energy of CdO nanoparticle formation during thermal treatment was calculated to be 12.2 kJ/mol. 相似文献
126.
介绍了通过运用网络平台构建物理实验中心的管理系统,以实现学生选课、成绩管理、教学信息管理和发布、教学资料的上网及仪器管理等一系列的功能,使物理实验中心的各项工作有序而高效. 相似文献
127.
The theoretical investigation of all parameter noises in repetition-rate laser pulse train was presented. The expression of power spectrum of laser pulse trains with all parameter noises was derived, and the power spectra of pulse trains with different noise parameters were numerically simulated. By comparing the power spectra with and without pulse-width jitter, we noted that pulse-width jitter could not be neglected compared with amplitude noise and timing jitter and contributed a great amount of noise into the power spectrum under the condition that the product of pulse width and angular frequency was larger than 1. 相似文献
128.
An S-box modified one-way coupled map lattice is applied as a chaotic cryptograph. The security of the system is evaluated from various attacks currently used, including those based on error function analysis, statistical property analysis, and known-plaintext and chosen-ciphertext analytical computations. It is found that none of the above attacks can be better than the brute force attack of which the cost is exhaustively quantitated by the key number in the key space. Also, the system has fairly fast encryption (decryption) speed, and has extremely long period for finite-precision computer realization of chaos. It is thus argued that this chaotic cryptosystem can be a hopeful candidate for realistic service of secure communications. 相似文献
129.
Xinyi Liu Ying Tang Weiyu Ning Yihong Bao Ting Luo Jinling Wang 《Molecules (Basel, Switzerland)》2022,27(9)
This study aimed to elucidate the responses of a novel characterized Issatchenkia terricola WJL-G4 against citric acid stress by performing physiological analysis, morphology observation, and structural and membrane fatty acid composition analysis. The results showed that under citric acid stress, the cell vitality of I. terricola WJL-G4 was reduced. The cell morphology changed with the unclear, uncompleted and thinner cell wall, and degraded the cell structure. When the citric acid concentration was 20 g/L, I. terricola WJL-G4 could tolerate citric acid and maintain the cell structure by increasing the intracellular pH, superoxide dismutase activity, and contents of unsaturated fatty acids. As the citric acid concentration was ≥80 g/L, the stress has exceeded the cellular anti-stress ability, causing substantial cell damage. The cell membrane permeability, the content of membrane lipids, malondialdehyde and superoxide anion increased, but the intracellular pH and superoxide dismutase activities decreased, accompanying the increase of citric acid concentrations. The findings of this work provided a theoretical basis for the responsive mechanism of I. terricola WJL-G4 under high concentrations of citric acid, and can serve as a reference for biological acid reduction in fruit processing. 相似文献
130.