Cr80-xFe20Mnx(x=10,15,20)合金的低温电阻率和热导率

报道了Cr80-xFe20Mnx(x=10,15,20)合金在10—300K的电阻率和热导率．结果表明样品的电输运性质和热输运性质均与样品的磁状态有关．在SDW反铁磁转变附近,电阻率出现极小．对Neel温度以下电阻率-温度曲线拟合结果表明：取温度相关的能隙函数2△∝√（TN-T）可以很好地描述SDW反铁磁能隙随温度降低而打开的过程．合金在反铁磁转变温度以下表现出与无序样品或者玻璃态样品类似的热导率温度关系,这可能是源于合金中磁性团簇的散射．     

非线性Lipschitz算子半群的表示

本文通过引入若干Lipschitz对偶概念,将非线性Lipschitz算子半群对偶映射到Lipschitz对偶空间中,使其转化为线性算子半群。该线性算子半群被证明是一个C_0~*-半群,因而是某个C_0-半群的对偶半群。从而证明了,在等距意义下,一个非线性Lipschitz算子半群可以延拓为一个C_0-半群。基于这些结论,本文给出了一系列全新的非线性Lipschitz算子半群的表示公式。     

激光束照射下轴压圆柱薄壳热屈曲数值分析

 针对激光束照射下承受轴压作用的圆柱薄壳,实现了材料参数(弹性模量E，泊桑比μ、线膨胀系数α)随温度变化情况下热屈曲破坏有限元数值分析。数值计算结果表明,激光照射区域产生的热应力和材料软化将导致处于正常工作状态的轴压圆柱壳发生灾难性的热屈曲破坏。     

POLYMERIZATION OF N,N''''-(PYROMELLITOYL)-BIS-L-LEUCINE DIACID CHLORIDE WITH HYDANTOIN DERIVATIVES BY MICROWAVE IRRADIATION

INTRODUCTIONRecently, there has been growing interest in applying microwave energy to synthetic organic chemistry[1-4],sample preparation for analysis[5], extraction of natural products from plants[6], waste treatment[7] and polymersynthesis[8-13]. The reactions involved in these applications are very fast and are completed within a short periodof time. Recently, we have used microwave irradiation for the synthesis of poly(amide-imide)s and poly(ester-imide)s[14-17].Recently more attentio…     

透明边界条件算法的比较研究及改进

研究了束传播算法(BPM)中简单透明边界条件(STBC)和完全透明边界条件(CTBC)两种边界处理算法对计算结果精度的影响.通过改进和综合两种边界条件算法,提出改进型透明边界算法(ITBC).该边界算法相对于STBC与CTBC降低了计算精度对于传播步长的依赖性,提高了计算精度,改善了透明边界条件算法在BPM中的稳定性.     

Under load strain partition of a ceramic matrix composite using an ultrasonic method

A method for carrying out strain partition under load is described. An ultrasonic device and a suitable extensometer are used simultaneously. Applied to a ceramic matrix composite, it allows one to evaluate the contribution of the various damage mechanisms on its highly nonlinear behavior.     

甘蔗条螟性信息素——三组份的结构鉴定

甘蔗条螟(Chilo venosatus walker)属鳞翅目螟蛾科,广布于我国南方蔗区,尤其在珠江兰角州高产蔗区每年发生4～6代。它使甘蔗枯心或枯梢,影响甘蔗产量。若用杀虫剂防     

METAL CLUSTERS SYNTHESIZED BY SOLID STATE REACTION——PREPARATION AND CRYSTAL STRUCTURE OF TWO MIXED METAL CLUSTERS,Ni_2Nb_2Te_4(Ⅰ) AND Ni_2Ta-2Te_4(Ⅱ)

The two title compounds obtained by solid state reaction at high temperature were char-acierized as isomorphism by single--crystal X--ray diffraction. The space group of both crys-tals is C_(2v)~4-Pma2, with lattice constants a = 7.955(1), b=6.258 (1), c=7 .203(2)A forI, and a =7.914 (1), b=6.237 (1), c=7.236 (1) ? for Ⅱ, Z=2. The structures were de-termined by normal method and refined to the final R = 0.074 and 0.083, respectively. Theresults show that the structure may be regarded as building by cluster unit with formulaNi_2M_2Te_4 (M =Nb or Ta) in which two Ni atoms and two M atoms form a rhombus, whilethe Te atoms are distorted tetrahedrally coordinated with both kinds of metal atoms. In thecluster unit there exist interactions between Ni atoms as well as between Ni and M atoms.In addition, all the cluster units are linked together not only by bridging Te atoms, but alsoby weaker metal-metal interactions, so as to form two--dimensional network. Therefore, thestructure may be represented by the for     

TRANSFER MECHANISM OF QUININE DRUG ACROSS THE OIL/WATER (O/W) INTERFACE

The transfer phenomena of quinine drug at the aqueous 1,2- dichloroethane (DCE)interface have been studied by the current- scanning polarography. The relationships be-tween the wave height and pH of aqueous phase, concentration of quinine as well as therate of water drop are discussed. The effect of supporting electrolyte, buffer solution andthe nature of organic solvent on the polarographic wave is studied. The transfer char-acteristics of quinine in aqueous phase and in organic phase are compared, The mono- pro-tonated and diprotonated quinines can both transfer at the interface so as to produce twopolarographic waves. The transfer process of quinine at the interface is simultaneouslycontrolled by diffusion and reestablishment of the disturbed protonated equilibrium ofquinine. A further investigation is made by chronopotentiometry. On the basis of thetheoretical analysis, the formulae of the limiting current are derived and discussed. Thetheoretical results are in agreement with the experimental ones.     

X射线荧光法测定土壤总硫量

本文采用模拟土壤基体的方法人工制备测定用标准样品,应用回归分析求取经验系数校正基体效应,建立了测定土壤总硫量的X射线荧光光谱分析方法。该法简便快速、灵敏(最低检出限小于5μg/g)。测定结果与化学法基本一致。