CATALYSIS OF POLYSTYRENE N-HYDROXYL SULFONAMIDE FOR ESTERIFICATION OF BUTANOL WITH ACETIC ANHYDRIDE

1. INTRODUCTION The development of efficient polymer-supported catalysts has attracted much attention [1]. For obtaining polymeric catalysts, catalytically active groups were introduced onto polymers mostly by copolymerization of the appropriate monomers bearing the desired catalyticfunctionalities (e.g. imidazole, OH, and COOH) or by modification of preformed polymers.Another possibility involves the attachment of side chains, containing the desired arrangement of functional groups, o…     

Synthesis of New 13-O-Acylavermectin Bl Aglycones

Six new 13-O-acylavermectin Bl aglycones(3-8) were synthesized from avermectin B1 aglycone and their bioactivities were evaluated against Spodoptera exigua, Spodoptera eridania, Tetranychus urticae and Aphis fabae.     

A monotone iterative scheme for a nonlinear second order equation based on a generalized anti–maximum principle

In this paper, a generalized anti–maximum principle for the second order differential operator with potentials is proved. As an application, we will give a monotone iterative scheme for periodic solutions of nonlinear second order equations. Such a scheme involves the L^p norms of the growth, 1 ≤ p ≤ ∞, while the usual one is just the case p = ∞.     

Birkhoff系统的Hojman定理的几何基础

研究了Birkhoff系统的Hojman定理的几何基础.建立了系统的运动微分方程和Hojman守恒 定理，利用现代微分几何给出了Birkhoff系统的Hojman定理的一个证明. 关键词： Birkhoff系统 Hojman定理 对称性 微分几何     

Spectra Analysis of a Novel Ti-Doped LiAlO2 Single Crystal

LiAlO2 single crvstals doped with Ti at concentration 0.2at.% are grown by the Czochralskl technique with dimensions φ42×55mm. Ti ions in the crystal are quadrivalence proven by comparing the absorption and fluorescence spectra of pure LiAlO2 and Ti： LiAlO2. After air and Li-rich atmosphere annealing, the absorption peaks in the range of 600-800nm disappear. We conclude that 682 and 756nm absorption peaks are attributed to the VLi and Vo absorptions, respectively： The peaks at 716nm and 798nm may stem from the VLi^＋ and absorptions. The colour-centre model can be applied to explain the experimental phenomena. Ti^4＋-doping produces more lithium vacancies in the LiAlO2 crystal. The intensities of [LiO4] and the associated bonds remain unchanged, which improves the anti-hydrolyzation and thermal stability of LiAlO2 crystals.     

微模塑法制备PMMA/SiO2二氧化硅杂化材料微结构

以摩尔比为 1∶1的甲基丙烯酸甲酯 (MMA)、甲基丙烯酸 (3 三乙氧基硅烷基 )丙酯 (ESMA)单体、0 .2 %(单体总量的质量分数 )的偶氮二异丁腈AIBN引发剂和四氢呋喃 (THF)溶剂 ,及 2 0 % (总质量分数 )的正硅酸乙酯TEOS合成出PMMA/SiO2 有机 无机杂化的杂化溶胶 .将溶胶在洗净的普通光学玻璃基片表面甩膜 .利用软刻蚀中的微模塑法 ,把有机硅弹性印章复制有精细图纹一面轻放在杂化溶胶膜上进行微模塑 ,外加 1N压力于12 0℃下处理 2h使溶胶凝胶化 .印章剥离后在基片表面就形成了PMMA/SiO2 有机 无机杂化材料的微图纹结构 .从微图纹的光学显微镜照片可以看出微模塑方法制备杂化材料复制的图纹精细度高 ,操作简单易行 ,是一类比较理想的微细图纹结构加工的方法 .     

On a Generalized Cochrane Sum and Its Hybrid Mean Value Formula

The main purpose of this paper is to use a mean value theorem of Dirichlet L-functions to study the asymptotic property of a hybrid mean value of a generalized Cochrane sum, and give an interesting mean value formula.2000 Mathematics Subject Classification: Primary—11F20; Secondary—11F99     

基于ZBLANⅩⅣPr,Yb频率上转换发光的三维立体显示

本文对利用ZBLANⅩⅣPr,Yb频率上转换发光的三维立体显示做了研究,探讨了其中的一些物理问题.在实验中,我们利用Yb³⁺离子敏化的方法提高Pr³⁺的上转换发光效率;通过降低能引起单频上转换发光的激光强度来提高寻址点和非寻址点在显示过程中的对比度.     

The accurate dimensional measurements within small internal structures

This paper shows that the dimension of internal structure of a component can be measured remotely to a resolution better than 5 μm by use of the combination of high resolution optical microscopy and image processing.A specialised high resolution, long working distance and diffraction limited lens was used to image within the component. A series of digital images were made to map spatially the interior of the component. An edge detector was then used to localise the specific location of features in order that an accurate internal measurement could be made. A visualisation of the internal surface finish was also achieved.