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31.
Wastewater containing a mixture of hypophosphites and phosphites was treated in order to assess the possibility of attaining high levels of phosphorus oxidation to phosphate. An initial series of tests based on chemical oxidation by means of Fenton's reagent demonstrated the feasibility of this process for solutions containing 250-750 mg/l of phosphorus. Removal yields of up to 98% were attained at pH 3.5 by using variable ratios of [H2O2]/[Fe2+]. The second series involved the electrolytic generation of Fenton's reagent at pH 2-2.5 through cathodic oxygen reduction. This demonstrated the possibility of obtaining quantitative yields for solutions containing 80-160 mg/l P with a constant [H2O2]/[Fe2+] ratio of 3.94. Economic comparison of the two processes showed that the operative cost of the electrochemical treatment is comparable to that of the chemical process. 相似文献
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Control and measurement of residual stress in glass is of great importance in the industrial field. Since glass is a birefringent material, the residual stress analysis is based mainly on the photoelastic method. This paper considers two methods of automated analysis of membrane residual stress in glass sheets, based on the phase-shifting concept in monochromatic light. In particular these methods are the automated versions of goniometric compensation methods of Tardy and Sénarmont. The proposed methods can effectively replace manual methods of compensation (goniometric compensation of Tardy and Sénarmont, Babinet and Babinet-Soleil compensators) provided by current standards on the analysis of residual stresses in glasses. 相似文献
35.
In this paper an automated photoelastic method based on the phase stepping technique is described. It provides full-field
maps of the isoclinic parameter and the relative retardation. The technique is based on processing six images of a photoelastic
specimen acquired using plane and circularly polarized light. The number of acquisitions and the type of polariscope used
in this approach have been chosen with the aim at reducing the influence of quarter wave plate errors and obtaining raw photoelastic
data in a periodic form suitable for easy applications of automatic unwrapping routines. 相似文献
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Francesco Petrucci Pietro Delle Femmine Alessandro Alimonti Sergio Caroli 《Mikrochimica acta》1989,97(1-2):57-63
A simple and inexpensive recycling nebulizer for inductively-coupled plasma atomic emission spectrometry has been devised by slightly and reversibly modifying a conventional external pneumatic nebulizer. Its performance was checked with a number of analytes (Ca, Cu, Mg, P, Pt) in aqueous and serum solutions. Results show that the system is entirely reliable provided that argon carrier gas is presaturated with water vapor. The use of a peristaltic pump even in the recirculating version was found to be essential for a proper functioning if complex media are investigated. 相似文献
38.
M. Bregman M. Calvetti G. Carron S. Cittolin M. Hauer H. Herr H. Koziol F. Krienen P. Kristensen G. Lebée D. Möhl G. Petrucci C. Rubbia D. Simon G. Stefanini L. Thorndahl S. van der Meer T. Wikberg 《Physics letters. [Part B]》1978,78(1):174-175
Antiprotons have been stored in the ICE Storage Ring and held for 85h with the help of stochastic cooling. We set a limit of at least 32 h for the antiproton lifetime (in its rest frame). 相似文献
39.
H. Beissler G. A. Petrucci K. Bächmann U. Panne P. Cavalli N. Omenetto 《Fresenius' Journal of Analytical Chemistry》1996,355(3-4):345-347
A method is described for measuring the gold content of integral and size-segregated samples of atmospheric particulate matter. After acid digestion and a liquid/ liquid extraction, the sample are analysed by Two-Colour Laser Induced Fluorescence in a graphite furnace. An absolute instrumental detection limit of 1 fg is achieved. Assuming a sampled volume of 1 m3, this corresponds to an atmospheric concentration of 50 fg m–3. Due to blank limited noise, the above limits increase to 20 fg and 1 pg m–3, respectively. Results of the analysis of filter samples as well as of size-segregated impactor samples are presented. 相似文献
40.
Armstrong TA Bettoni D Bharadwaj V Biino C Blanford G Borreani G Broemmelsiek D Buzzo A Calabrese R Ceccucci A Cester R Church M Dalpiaz P Dalpiaz PF Dimitroyannis D Fabbri M Fast J Gianoli A Ginsburg CM Gollwitzer K Govi G Hahn A Hasan M Hsueh S Lewis R Luppi E Macrí M Majewska AM Mandelkern M Marchetto F Marinelli M Marques J Marsh W Martini M Masuzawa M Menichetti E Migliori A Mussa R Palestini S Pallavicini M Passaggio S Pastrone N Patrignani C Peoples J Petrucci F Pia MG Pordes S Rapidis P 《Physical review D: Particles and fields》1995,52(9):4839-4854