Remote filament-induced fluorescence spectroscopy from thin clouds of smoke

Remote filament-induced fluorescence spectroscopy is used to probe a cloud of smoke, produced from burning mosquito coils, located at a distance of 25 m from the laser source and LIDAR detector. CN, CH and C₂ molecular fragments were identified in the sample. We demonstrate that temporally gated measurement is an efficient technique to easily suppress spectral contaminations, such as white light and atmospheric N₂ fluorescence.     

Synthesis of Novel Polyfunctionally Substituted Thieno[2,3‐c]pyridazines

4‐Cyano‐5,6‐dimethylpyridazin‐3‐(2H)‐thione 3b was used as a key intermediate for the synthesis of novel polysubstituted thieno[2,3‐c]pyridazines.     

Distribution of natural radionuclides and hot points in coasts of Hormozgan, Persian Gulf, Iran

Summary A reconnaissance study has been made on the distribution of ²³⁸U, ²³² Th, ⁴⁰K, ¹³⁷Cs and geochemical features in soil and sediment samples at various locations in the coast of Persian Gulf. Activity concentration levels due to radionuclides were measured in 50 samples of soils and sediments collected from the coast of Hormozgan. From the measured spectra, activity concentrations were determined for ⁴⁰K (range from 140 to 1172 Bq ^. kg^-1), ¹³⁷Cs (from 0 to 15 Bq ^. kg^-1), ²³⁸ U (from 29 to 385 Bq ^. kg^-1) and ²³²¹ Th (from 9 to 156 Bq ^. kg^-1) with the lowest limit of detection (LLD) of 68, 3.2, 4.3 and 4.3 Bq ^. kg^-1, respectively. The dose rate from ambient air at the soil ranges was between 23 to 177 nGy ^. h^-1 with an average of 60±7.86 nGy ^. h^-1.     

The Bochner–Schoenberg–Eberlein Property for Totally Ordered Semigroup Algebras

The concepts of BSE property and BSE algebras were introduced and studied by Takahasi and Hatori in 1990 and later by Kaniuth and Ülger. This abbreviation refers to a famous theorem proved by Bochner and Schoenberg for \(L^1({\mathbb {R}})\), where \({\mathbb {R}}\) is the additive group of real numbers, and by Eberlein for \(L^1(G)\) of a locally compact abelian group G. In this paper we investigate this property for the Banach algebra \(L^p(S,\mu )\;(1\le p<\infty )\) where S is a compact totally ordered semigroup with multiplication \(xy=\max \{x,y\}\) and \(\mu \) is a regular bounded continuous measure on S. As an application, we have shown that \(L^1(S,\mu )\) is not an ideal in its second dual.     

A Kinetic spectrophotometric method for determination of amlodipine and Nifedipine in pharmaceutical preparations

A simple, accurate, sensitive and economical procedure for the estimation of amlodipine besylate and nifedipine, both in pure and dosage forms, has been developed. The method is based on the reduction of iron(III) by the studied drugs and subsequent interaction of iron(II) with ferricyanide to form Prussian blue. The reaction develops through a slow kinetics and completes in about 10 min. Both initial slope and fixed time methods were used to derive calibration graphs. The resulted calibration equations were linear in the concentration ranges of 1.0-20.0 and 3.0-19.0 μg ml^-1 for AML and NIF, and the detection limits were 0.10 and 0.19 μg ml^-1, respectively. Seven replicate analyses of solutions containing three different levels of each drug resulted in very low relative error of prediction (less than 1.6%) and relative standard deviation (less than 4%) confirming accuracy and precision of the proposed method. The proposed method was applied to the determination of these drugs in pharmaceutical formulations and excellent recoveries were obtained.     

Warm-intermediate inflationary universe model with viscous pressure in high dissipative regime

Warm inflation model with bulk viscous pressure in the context of “intermediate inflation” where the cosmological scale factor expands as $a(t)=a_0\exp (At^f)$ , is studied. The characteristics of this model in slow-roll approximation and in high dissipative regime are presented in two cases: 1—Dissipative parameter $\Gamma $ as a function of scalar field $\phi $ and bulk viscous coefficient $\zeta $ as a function of energy density $\rho $ . 2— $\Gamma $ and $\zeta $ are constant parameters. Scalar, tensor perturbations and spectral indices for this scenario are obtained. The cosmological parameters appearing in the present model are constrained by recent observational data (WMAP7).     

Electron (positron) impact excitation (2p state) of lithium at intermediate energies

In this work, studies have been carried out to investigate theoretically the electron (positron)-impact-induced 2s → 2p lithium (Li) transition at 20 and 60 eV using the coupled-channel optical method (CCOM). The inelastic differential cross sections (DCS) together with the reduced Stokes parameters ( $\bar P_1$ , $\bar P_2$ , $\bar P_3$ ) and other parameters such as the alignment (γ, $\bar P_l$ ), orientation (L _⊥) and coherence parameters (P ⁺) are reported in the present calculations. Comparison is made with other available theoretical and experimental measurements.     

Effects of Some Parameters on Particle Size Distribution of Chitosan Nanoparticles Prepared by Ionic Gelation Method

In this research, chitosan nanoparticles were prepared based on the ionic gelation of chitosan with tripolyphosphate anions. Effects of parameters such as chitosan concentration, tripolyphosphate concentration, and reaction time on the particle size distribution were investigated. In order to determine optimum conditions, tests were designed by Qualitek-4 software, using Taguchi method. The best conditions were determined based on three factors at three levels. Therefore, the main object was to investigate the effect of some parameters on particle size distribution and determine the optimum conditions for preparing chitosan nanoparticles by ionic gelation, followed by evaluation of the physicochemical and structural properties. The size distribution of original chitosan and chitosan nanoparticles were determined by Laser Diffraction and Dynamic Light Scattering, respectively. The physicochemical properties of the chitosan nanoparticles were studied using SEM, TEM, XRD pattern, FTIR, UV–vis, TGA, and NMR spectra. The optimum chitosan concentration, tripolyphosphate concentration, and reaction time were found to be 1.0 mg/ml, 1.0 mg/ml, and 60 min, respectively.