不同后处理方法对溶胶-凝胶SiO2膜层抗污染能力的影响

以正硅酸乙酯作为前驱体,利用碱催化方式制备了SiO2溶胶,采用提拉法在K9基片上镀制SiO2单层薄膜,分别用热处理、紫外辐射处理、氨水加六甲基二硅胺烷气氛处理和酸碱复合膜4种后处理法对膜层进行处理,采用分光光度计、红外光谱、扫描探针显微镜、静滴接触角测量仪、椭偏仪等分析了薄膜的特性,通过真空环境加速污染实验对处理前后的膜层进行抗污染能力对比,结果表明:在碱性SiO2膜层上加镀一层酸性SiO2膜的复合膜层整体透过率仍保持在99%以上,疏水角达到128°,膜层真空抗污染能力大大加强。     

某些完备李代数的结构

本文讨论了完备李代数的同构问题，并对幂零根基为一些Ｈｅｉｓｅｎｂｅｒｇ代数及交换李代数之直和的可解和一般完备李代数的结构进行了讨论．     

单个函数平移和伸缩的叠加在L~p(R~d)中的逼近(英)

本文主要讨论单个函数平移和伸缩的线性组合对Lp（Rn）中任一紧集内函数的逼近．给出一个很强的逼近结果．这在神经网络应用研究中具有重要意义．     

Influence of annealing temperature on the formation, microstructure and magnetic properties of spinel nanocrystalline cobalt ferrites

Nanocrystalline cobalt ferrites were synthesized by a simple, general, one-step sol–gel auto-combustion method. An interpretation based on the measurement of the adiabatic flame temperature and the amounts of gas evolved during reaction had been proposed for the nature of combustion. The influence of annealing temperatures on the magnetic properties was investigated. The microstructure was characterized by means of X-ray diffractometer (XRD) and transmission electron microscopy (TEM). It was found that the particle size and magnetic properties of the as-prepared ferrite samples showed strong dependence on the annealing temperature. The coercivity initially increased and then decreased with increasing annealing temperature whereas the particle size and saturation magnetization continuously increased.     

大面积染料敏化太阳电池的串联阻抗特性研究

在电子扩散微分方程的基础上,研究了染料敏化太阳电池光生电流和光生电压随光照强度不同的变化关系.提出敏化太阳电池串联阻抗功率损耗模型,理论模拟了大面积电池（有效面积>1 cm²）光电转换效率随多孔薄膜有效面积宽度变化的曲线、透明导电基底膜与银栅极的比接触电阻以及在不同入射光强下银栅极体电阻对大面积染料敏化太阳电池光伏性能的影响.结果表明透明导电基底膜的方块电阻和银栅极体电阻对大面积染料敏化太阳电池的性能有很大影响,而这种影响随光强的减弱逐渐减小. 关键词： 染料敏化 太阳电池 串联阻抗 光电转换效率     

An improved loopless mounting method for cryocrystallography

Based on a recent loopless mounting method, a simplified loopless and bufferless crystal mounting method is developed for macromolecular crystallography. This simplified crystal mounting system is composed of the following components: a home-made glass capillary, a brass seat for holding the glass capillary, a flow regulator, and a vacuum pump for evacuation. Compared with the currently prevalent loop mounting method, this simplified method has almost the same mounting procedure and thus is compatible with the current automated crystal mounting system. The advantages of this method include higher signal-to-noise ratio, more accurate measurement, more rapid flash cooling, less x-ray absorption and thus less radiation damage to the crystal. This method can be extended to the flash-freeing of a crystal without or with soaking it in a lower concentration of cryoprotectant, thus it may be the best option for data collection in the absence of suitable cryoprotectant. Therefore, it is suggested that this mounting method should be further improved and extensively applied to cryocrystallographic experiments.     

Contrast-enhanced MR angiography with frequency-dependent mask subtraction

One of the main challenges for high-resolution contrast-enhanced magnetic resonance angiography (CE-MRA) is the limited signal-to-noise ratio (SNR). In conventional CE-MRA, spoiled gradient-recalled echo sequence is typically used to acquire raw data before and after contrast material injection, followed by mask subtraction to improve vessel contrast at the cost of increased image noise. We reported here on a frequency-dependent mask subtraction technique where only low spatial frequency data were subject to mask subtraction to improve image contrast and reduce motion artifact while high spatial frequency data were not subtracted to preserve image noise level. The feasibility of this technique was demonstrated through phantom, animal, and human volunteer studies. The lowest half, quarter, 1/8 and 1/16 of all spatial frequencies were subject to mask subtraction, respectively. These partial subtraction techniques were compared with conventional mask subtraction in terms of SNR and artifact power. An SNR gain up to 37% was achieved without significant artifact power increase for quarter-subtraction where only the central one quarter k-space data were subject to mask subtraction.     

Explicit bounds on some new nonlinear integral inequalities with delay

The purpose of the present note is to establish some new delay integral inequalities, which provide explicit bounds on unknown functions and generalize some results of Li et al. [Some new delay integral inequalities and their applications, J. Comput. Appl. Math. 180 (2005) 191–200]. The inequalities given here can be used to investigate the qualitative properties of certain delay differential equations and delay integral equations.     

Effect of the thermal and hydrothermal treatment on textural properties of Zr-MCM-41 mesoporous molecular sieve

Zr-containing mesoporous molecular sieves were synthesized by hydrothermal method using cetyltrimethyl ammonium bromide as a template and sodium silicate and zirconium sulfate as raw materials. The structure and morphology of the synthesized samples were characterized via various physicochemical methods, including X-ray diffraction (XRD), transmission electron microscopy (TEM), Fourier transform infrared (FT-IR) spectroscopy, solid state nuclear magnetic resonance (²⁹Si MAS-NMR) techniques, thermal gravimetric-differential scanning calorimeter (TG-DSC) and N₂ physical adsorption, respectively. The effect of the different initial ZrO₂:SiO₂ molar ratio, the different thermal treatment temperature and the different hydrothermal treatment time on textural property was investigated. The experimental results reveal that the as synthesized samples possess a typical mesoporous structure of MCM-41. On the other hand, the specific surface area and pore volume of the synthesized Zr-MCM-41 mesoporous molecular sieve decrease with the increase of the amount of zirconium incorporated in the starting material, the rise of thermal treatment temperature and the prolonging of hydrothermal treatment time, the mesoporous ordering becomes poor. Also, when the molar ratio of ZrO₂:SiO₂ in the starting material is 0.1, the mesoporous structure of the Zr-MCM-41 mesoporous molecular sieve still retains after calcination at 750 °C for 3 h or hydrothermal treatment at 100 °C for 6 d, and have specific surface areas of 423.9 and 563.9 m²/g, respectively.     

Statistical properties of world investment networks

We have performed a detailed investigation on the world investment networks constructed from the Coordinated Portfolio Investment Survey (CPIS) data of the International Monetary Fund, ranging from 2001 to 2006. The distributions of degrees and node strengths are scale-free. The weight distributions can be well modeled by the Weibull distribution. The maximum flow spanning trees of the world investment networks possess two universal allometric scaling relations, independent of time and the investment type. The topological scaling exponent is 1.17±0.02 and the flow scaling exponent is 1.03±0.01.