MEASUREMENTS OF ANGULAR MOMENTUM EFFECT OF FISSION BARRIER

The fission cross sections and the evaporation residue cross sections for ¹²C+²⁰⁹Bi and ¹⁴N+Pb reactions were measured with the gold surface barrier silicon detectors and the mica nuclear track detectors.The critical angular momentum l_er was deduced from the measured evaporation residue cross section σ_er on the basis of the sharp-off model.The fission barrier with the particular angular momentum i derived from the condition Γ_f/Γ_n=1 at l=l_e The angular momentum effect of the fission barrier was studied experimentally.     

ANGULAR DISTRIBUTIONS OF FISSION FRAGMENTS IN INTERACTIONS OF 12C IONS WITH VARIOUS TARGETS

Angular distributions of fission fragments were measured for a series of compound nuclei formed in the bombardment of ¹⁶⁹Tm,¹⁷⁵Lu,¹⁸¹Ta,W,Re,Pt,¹⁹⁷Au,Pb and ²⁰⁹Bi by ¹²C ions with mica track detectors and gold surface barrier silicon detectors.All the measured angular distributions can be fitted satisfactorily by the theoretical formula based on saddle point model.The variation trend for K² with the excitation energy increasing was given at various ranges of the fission parameter Z²/A.     

Discussion About Nonlinear Time Series Prediction Using Least Squares Support Vector Machine

The least squares support vector machine (LS-SVM) is used to study the nonlinear time series prediction. First, the parameter γ and multi-step prediction capabilities of the LS-SVM network are discussed. Then we employ clustering method in the model to prune the number of the support values. The learning rate and the capabilities of filtering noise for LS-SVM are all greatly improved.     

Charge Loss Characteristics of Different Al Contents in a HfA10 Trapping Layer Investigated by Variable Temperature Kelvin Probe Force Microscopy

Kelvin probe force microscopy （KFM） technology is applied to investigate the charge storage and loss characteristics of the HfAlO charge trapping layer with various AI contents. The experimental results demonstrate that with the increase of AI contents in the HfAIO trapping layer, trap density significantly increases. Improvement of data retention characteristic is also observed. Comparing the vertical charge loss and lateral charge spreading of the HfAIO trapping layers, the former plays a major role in the charge loss mechanism. Variable temperature KFM measurement results show that the extracted effective electron trap energy level increases with increasing AI contents in HfAIO trapping layer, which is in accordance with the charge loss characteristics.     

固相膜萃取-超声洗脱-原位衍生法分析水中不同极性农药残留

建立了水中极性除草剂和非极性杀虫剂固相膜萃取-超声洗脱-原位衍生-气相色谱质谱方法。在样pH≈3时,采用C8固相萃取膜,10 min可完成1000 mL水中两类化合物的萃取;将膜片置于反应瓶中,加入2 mL丙酮溶剂和衍生试剂,对杀虫剂进行超声洗脱、对除草剂进行洗脱衍生。其洗脱、衍生时间为30 min。以HP-5MS(30 m×0.25 mm×0.25μm)为分析柱,采用负化学源技术在10 min内完成两类物质的检测。由于衍生试剂与酸性除草剂是特定的官能团之间的反应,并且衍生时间较短,因此杀虫剂的回收率不受影响。方法实现了不同极性有机物的同时萃取、同时检测。在10~250μg/L线性范围内各组分线性关系良好,相关系数R2>0.9978,检出限<1.0μg/L。不同基质、不同浓度的加标回收率在88%~107%之间;相对标准偏差在3.6%~9.7%之间。     

A thermal entangled quantum refrigerator based on a two-qubit Heisenberg model with Dzyaloshinskii-Moriya interaction in an external magnetic field

Based on an isotropic two spin-1/2 qubits Heisenberg model with the Dzyaloshinskii-Moriya interaction in an external magnetic field, we have constructed an entangled quantum refrigerator. Expressions for the basic thermodynamic quantities, i.e., the heat exchanged, the net work input, and the coefficient of performance, are derived. Some intriguing features and their qualitative explanations in zero and non zero magnetic fields are given. The influence of the thermal entanglement on the refrigerator is investigated. The results obtained here have general significance and will be helpful to understand the performance of an entangled quantum refrigerator.     

含三脚架配体及吡啶甲酸根的锰(Ⅱ)配合物的合成及结构表征

本文合成了2种含有吡啶甲酸根的三(2-苯并咪唑亚甲基)胺合锰配合物,并对其进行了红外,元素分析和X-射线单晶衍射测定。结果表明,单核配合物1和2分别具有三角双锥和扭曲八面体的几何构型。在配合物1中,烟酸根阴离子利用一个羧基氧原子和锰离子配位;在配合物2中,邻吡啶甲酸根阴离子采取N,O螯合的配位方式。由于烟酸根和邻吡啶甲酸根的配位方式不同,导致配合物晶体结构中存在不同类型的氢键。配合物1形成了由氢键连接的二维网状结构,而配合物2只能形成由氢键连接成的一维链状结构。     

氢化物发生-原子荧光光谱法测定大米与圆白菜中痕量铅

建立了氢化物发生-原子荧光光谱法(HG-AFS)测定经HNO3-HClO4-H2O2湿法消解的大米与圆白菜等样品中痕量铅的方法,系统地优化了灯电流等仪器参数条件,探讨了载流、还原剂、样品酸度、氧化剂的最佳浓度,考察了掩蔽剂去干扰的情况。实验表明:在选定载流浓度HCl 2%(V/V)、还原剂KBH4浓度2%(m/V)[KOH恒为0.5%(m/V)]、样品酸度HCl 1%(V/V)、氧化剂K3Fe(CN)60.4%(m/V)、掩蔽剂H2C2O40.2%(m/V)及优化设置灯电流等参数的最佳实验条件下,测定铅的检出限为0.07μg/L,在0.00—50.00μg/L范围呈良好的线性关系,样品测定变异系数小于等于6.22%。该方法简便、干扰少、灵敏度高,应用于大米、圆白菜等样品中Pb的测定,结果与参考值相符,是一种切实可行的方法。     

HG-AFS同时测定锌锭中的砷和汞

采用盐酸分解样品,用聚环氧琥珀酸(PESA)掩蔽基体,建立了氢化物发生-原子荧光光谱法(HG-AFS)测定锌锭中砷和汞的方法.实验表明,0.1g锌锭溶解后加入2.0mL PESA可以有效地掩蔽基体元素Zn,共存元素Mg、Al、Cu、Sb和Sn不干扰As和Hg的测定.砷和汞的方法检出限分别为0.26μg/L和0.043μg/L.将方法应用于实际样品分析,砷和汞的相对标准偏差(RSD,n=5)分别在1.1％-2.0％和1.0％-1.6％之间.加标回收率分别为96.1％-120.0％和92.8％-108.8％.     

用逐次线性化法对储存环动力学孔径的解析研究

从逐次线性化法解粒子非线性Betatron振荡方程出发,对存在非线性六极场、八极场及六极场与八极场共存的粒子Betatron振荡方程进行研究.应用线性理论得出了粒子非线性Betatron振荡稳定性的判据,得到了动力学孔径的半解析表达式,分析了在小振幅下,导致粒子非线性不稳定性的另外一种机制———小振幅下,参量共振所引起的自激振荡.用此方法对实际lattice的动力学孔径进行了研究,所得结果与数值跟踪结果吻合得很好