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Gizem Gülsoy Toplan Turgut Takn Gkalp can Fatih Gger Mine Kürküolu Aye Civa Gülay Ecevit-Gen Afife Mat Kemal Hüsnü Can Baer 《Molecules (Basel, Switzerland)》2022,27(6)
The potential applications of Achillea species in various industries have encouraged the examination of their phytochemical components along with their biological potential. In the present study, phenolic contents and essential oil compositions together with the in vitro biological activities of the aerial parts from Achillea biebersteinii Afan. and Achillea millefolium subsp. millefolium Afan. collected from Turkey were evaluated. Different solvent extracts (n-hexane, chloroform, methanol, water) were prepared and their antimicrobial, anticholinesterase, and antioxidant activities were studied. The LC-MS/MS results revealed the presence of 16 different phenolic compounds, including chlorogenic acid, rutin, quercetin, and luteolin glycosides, in methanolic extracts. According to GC-FID and GC/MS results, the primary components of the oils were identified as 1,8-cineole (32.5%), piperitone (14.4%), and camphor (13.7%) in A. biebersteinii and 1,8-cineole (12.3%) and β-eudesmol (8.9%) in A. millefolium subsp. millefolium. The infusion and methanolic extracts of both species were found to be rich in their total phenolic content as well as their antioxidant and anticholinesterase activity. In contrast, the n-hexane and chloroform extracts of both species showed strong antimicrobial activity with MIC values ranging from 15 to 2000 μg/mL. Our findings suggest that the investigated Achillea species could be evaluated as potent natural agents, and further studies into the promising extracts are needed. 相似文献
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Büra Gizem Günetekin Hilal Medetalibeyoglu Necip Atar Mehmet Lütfi Yola 《Electroanalysis》2020,32(9):1977-1982
Direct‐methanol fuel cells are proton‐exchange fuel cell in which methanol is used as the fuel. The important advantage of these fuel cells is the simplicity of transport and storage of methanol. In this study, methanol fuel cell electrocatalysts including graphene quantum dots (GQDs), functionalized multi‐walled carbon nanotubes (f‐MWCNTs) and GQDs/f‐MWCNTs composite were synthesized. The structures of synthesized electrocatalysts were highlighted by scanning electron microscope (SEM), raman spectroscopy, UV–vis spectroscopy, fourier transform infrared spectroscopy (FTIR), electrochemical impedance spectroscopy (EIS) and x‐ray diffraction (XRD) method. After that, the effective surface areas (ESA) of GQDs, f‐MWCNTs and GQDs/f‐MWCNTs were calculated. Finally, GQDs/f‐MWCNTs composite modified glassy carbon electrode (GQDs/f‐MWCNTs/GCE) showed highest current signals for methanol oxidation than those of comparable GQDs/GCE and f‐MWCNTs/GCE. 相似文献
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Chromatographia - This article aims to present a simple and sensitive, HPLC–UV method, which was developed to determine carnosol in human plasma samples. Chromatographic separation was... 相似文献
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Recent scientific studies have proven the importance of trace elements on human health. The main food supplies are plants and animals, which are significant sources of these minerals. Studies on determining mineral compositions of herbs, spices and some other crops have increased all over the world. Published works revealed that spices, herbs and medicinal plants should be consumed to obtain beneficial trace elements. Selenium (Se), one of the most vital trace elements, has a significant role in human diet acting as a preventative agent against some serious illnesses. Despite numerous scientific works on mineral compositions of medicinal and aromatic plants, investigations of selenium content in these foods could not be successfully studied until recently due to the lack of suitable analytical methods for selenium analysis. Thus, publications on selenium concentrations of foods are recent. In this regard, selenium contents of some medicinal and aromatic plants commonly used as spices, herbal teas and traditional medicines in Turkey were studied in the present research. Selenium contents of the most used parts of these plants were analyzed by ICP-OES (Varian Vista-Pro, Australia). Of the analyzed 26 medicinal and aromatic plants, the highest Se concentration (1133 microg kg-1) was found in sweet basil (Ocimum basilicum L.) and the lowest in sumac (Rhus coriaria L.) fruits (11 microg kg(-1)). 相似文献
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Gizem Dübek Franziska Hanusch Dr. Dominik Munz Prof. Shigeyoshi Inoue 《Angewandte Chemie (Weinheim an der Bergstrasse, Germany)》2020,132(14):5872-5878
Air- and moisture-stable heterobimetallic tetrahedral clusters [Cp(CO)2MSiR]2 (M=Mo or W; R=SitBu3) were isolated from the reaction of N-heterocyclic carbene (NHC) stabilized silyl(silylidene) metal complexes Cp(CO)2M=Si(SitBu3)NHC with a mild Lewis acid (BPh3). Alternatively, treatment of the NHC-stabilized silylidene complex Cp(CO)2W=Si(SitBu3)NHC with stronger Lewis acids such as AlCl3 or B(C6F5)3 resulted in the reversible coordination of the Lewis acid to one of the carbonyl ligands. Computational investigations revealed that the dimerization of the intermediate metal silylidyne (M≡Si) complex to a tetrahedral cluster instead of a planar four-membered ring is due to steric bulk. 相似文献
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We consider a certain finite group for which Kloosterman sums appear as character values. This leads us to consider a concrete family of commuting hermitian matrices which have Kloosterman sums as eigenvalues. These matrices satisfy a number of “magical” combinatorial properties and they encode various arithmetic properties of Kloosterman sums. These matrices can also be regarded as adjacency matrices for multigraphs which display Ramanujan-like behavior. 相似文献
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Bergdahl Gizem Ertürk Hedström Martin Mattiasson Bo 《Applied biochemistry and biotechnology》2019,188(1):124-137
Applied Biochemistry and Biotechnology - A capacitive sensor for saccharide detection is described in this study. The detection is based on selective interaction between diols and... 相似文献
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Nonlinear Dynamics - Bifurcations of periodic orbits and band zones of a one-dimensional granular array are numerically investigated in this study. A conservative two-bead system is first... 相似文献