高稳定LD泵浦腔内倍频Nd∶YVO4/KTP连续绿光激光器

设计出一种能够较好地补偿激光晶体热效应的激光谐振腔,实现了高稳定LD单端泵浦KTP腔内倍频Nd∶YVO4连续绿光激光器·当晶体吸收的泵浦功率为24.56W时,532nm激光功率达到5.3W,光-光转换效率达到21.6%,激光模式为TEM00模·在输出功率5W左右时,激光器1h功率不稳定度优于0.6%·     

Two New Xanthones from Polygala crotalarioides

Two new xanthones, 1,6,8-trihydroxy-2,3-methylenedioxyxanthone 1 and 1,4-dihydroxy-6, 7-methylenedioxyxanthone 2, were isolated from the roots of Polygala crotalarioides. Their structures were elucidated by spectroscopic and chemical methods.     

A Novel Tetraiodocadmate(Ⅱ)–PVC Membrane Electrode for the Potentiometric Determination of Cadmium(Ⅱ)

Cadmium is one of the most toxic heavy metal pollutants, so its determination is important. Carrier-based ion-selective electrodes (ISEs) have found wide application for being simple and economical. However, there are only limited reports on the ion-selec…     

氢原子团簇与金属氢形成的艹勾氏理论

全面系统介绍艹勾清泉教授有关Ｈｎ团簇的形成理论和利用该理论所取得的成果，阐明高压合成金属氢的可能性     

Two New Glycosides from the Roots of Ranunculus ternatus

Two new glycosides named as ternatoside A 1 and ternatoside B 2 were isolated from the roots of Ranunculus ternatus, the structures were determined by 1D and 2D NMR, ESI-MS techniques, and chemical methods.     

液晶的转动粘质系数的测试原理与方法(英文)

液晶的转动粘质度是液晶用于显示和通讯的重要物理参量.本文设计开发了基于微机的液晶参数测试光学系统,在该系统上研究了液晶的转动粘质系数的测试原理与方法:通过测试液晶盒在偏置电压下相位驰预时间,推导出转动粘质系数的值.测试Merck公司的E7液晶的转动粘质系数随温度变化的曲线,进行了理论拟合,测试结果与理论符合得很好.通过分析另一系统对液晶介质常数随温度变化的曲线的测试结果,验证了该测试原理与方法的正确性.该测试方法具有简单、自动化的特点.     

A Novel Biomolecular Immobilization Matrix Based on Nanoporous ZnO／Chitosan Composite Film for Amperometric Hydrogen Peroxide Biosensor

The performance of an enzyme electrode often depends on the method of enzyme immobilization when fabricating biosensors1. Therefore, the technique used to immobilize the enzyme is one of the key factors in developing a reliable biosensor. Organic-inorganic composite (or hybrid) materials have emerged in recent years. It combines the physicochemical attributes of components and improves their features. Organic components benefit the formation of defect-free inorganic membranes and make it less …     

小波分析中一个逆问题

本文证明:如果来自多尺度分析(伸缩因子为矩阵)的小波是标准正交的,那么相对应的尺度函数也是标准正交的,其中函数f_s(x)∈L~2(R~n)(s=1,2,…,r,r是正整数)的标准正交性是指f_s(x)的整平移所构成的函数族为L~2(R~n)的标准正交系。结果表明,如果我们想从多尺度分析出发构造正交小波,那么该多尺度分析必须有正交尺度函数。     

Reaction of Ketene Dithioacetals with Pyrazolylcarbohydrazide:Synthesis and Biological Activities of Ethyl 5-Amino-1-(5''''- methyl-1''''-t-butyl-4''''-pyrazolyl)carbonyl-3-methylthio-1H-pyrazole-4-carboxylate

Introduction Pyrazole and its derivatives represent one of the most active classes of compounds possessing a wide spectrum of biological activities. During the past years, considerable evidence has been accumulated to demon-strate the efficacy of pyrazole derivatives including an-tibacterial,1 antifungal,2 herbicidal,3 insecticidal4 and other biological activities.5-7 Up to now, a great variety of these kind of compounds have been synthesized, among which some commercially pesticides have been…     

Synthesis and Crystal Structure of 1D Coordination Polymer of N,N''''-Bis(3-pyridylmethyl)-1,4-benzenedicarboxamide and Cobalt(II) Nitrate

IntroductionTheresearchonarchitectureofcoordinationpoly-mershasbeenmushroomingrecentlyfortheirinterest-ingstructuralpropertiesandpotentialapplicationstomagnetism,NLOmaterial,electricalconductivity,ionexchange,etc.1-5Coordinationpolymerisafamilywhichiscomposedof1Dchains,2Dsheets,and3Dframeworkofbuildingblocksconnectedviametal-ligandcoordination.Hydrogenbondingand-stack-inginteractionareoftenfurtherutilizedtogeneratethosecoordinationpolymersintomultidimensionalsu-pramolecularnetworks.6-11Inth…