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In this paper, the nanometer permanent magnetic BaFe12O19 powder was synthesized by a novel method of independent nucleation and crystallization steps and subsequent heat treatment,during the synthesis, Ba(NO3)2, Fe(NO3)2 and NH4HCO3·NH2COONH4 were used as starting materials. The effect of crystallization process and heat treatment conditions on the particle size, microstructure and magnetic properties of powder was studied by using XRD, TEM and vibration sample magnetometometer techniques.XRD results showed that the hematite, α-Fe2O3, was the main phase in the powder at heat treatment temperatures below 650℃ and its amount in the powder was decreased with increasing temperature and small amount of α-Fe2O3 was still remained after being heated at 900℃ for 8hrs. BaFe12O19 was formed about 650℃ and its amount increased in the powder as temperature raised and the higher temperature was needed to attain considerable amount of BaFe12O19 and ideal nanometer BaFe12O19 particle in the powder. The temperature between 40℃~60℃ in the crystallization process was favor to the formation of good BaFe12O19 crystal and to the good magnetic properties of the powder. TEM showed that the particle size in the powder increased with the enhancement of the temperature and the powder crystallized at 40℃ and heated at 800℃ for 8hrs afterwards had a very homogenous particle size distribution, and that the powder heated at 900℃ for 8hrs with the same crystalline condition as the former had a typical hexagonal shape and a chain aggregation. Specific saturation and residential magnetizations and coercive force of the powder increased mono-tonically with the increase of temperature, and reached 39.86A·m2·kg-1, 23.96A·m2·kg-1, 480kA·mg-1 at 900℃, respectively. 相似文献
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SPH后处理研究 总被引:1,自引:0,他引:1
提出一套相对完整的光滑粒子流体动力学(SPH)后处理方法.凸区域和严重变形的非凸区域上的SPH计算结果都可用该方法处理.首先,对SPH粒子集进行Delaunay三角化,可得到由粒子作为节点的三角单元集;根据每个单元中三个节点是否彼此为粒子作用对,决定是否将该单元从单元集中删除.将保留下的单元作为有限单元并利用它们节点上的函数值,根据有限元插值方法即可得单元内部任何一点的函数值.根据该方法,可提取介质的自由表面.数值算例表明方法可行.对含固体壁面、严重粒子飞溅、多重介质互相作用的情况,提出相应对策;为SPH以至其它无网格方法形成较通用的后处理软件提供可行的途径. 相似文献