气相-红外光谱联用技术鉴定对羟基联苯加氢产物的异构体

对羟基联苯的选择性催化加氢反应是一个平行连串复杂反应,由于反应物的两个苯环加氢的难易程度不同,使得产物中含有两个不同的苯环分别加氢或者全部加氢而生成多个异构体,用通常的分析方法难于对异构体进行区分鉴定。使用气相-红外光谱联用分析手段,通过对苯环的对位和单取代位置的波数特征进行分析,可以鉴定出加氢反应的主产物是对环己基苯酚,副产物是由对环己基环己醇和对苯基环己醇的异构体组成。气-质联用、熔点测定、核磁共振等辅助分析,进一步验证了气相-红外光谱联用分析结果的准确性,表明气-红联用技术是一个快速准确分析具有特征官能团的有机化合物异构体的现代仪器方法。     

堆芯等离子体燃烧和控制

本工作描述我们编制的零维三流体粒子和功率平衡的等离子体动力学时关模拟程序。在物理上我们把等离子体动力学与新经典轮运理论结果结合起来,通过辅助加热、燃料粒子注入速率和纵场纹波控制堆芯等离子体燃烧。数值结果表明,通过控制完全可以实现堆芯等离子体的稳定燃烧和排灰要求。     

酶联免疫吸附法测定血浆中芍药苷浓度

建立了间接竞争酶联免疫吸附法测定血浆中芍药苷浓度.在10～200 μg/L浓度范围内,线性关系良好,线性回归方程为y=-0.1721 logC 1.9645,相关系数0.9927;回收率为89%～102%.运用本方法测定了大鼠一次灌胃后血浆中的芍药苷浓度.比较了分别给药芍药苷单体及中药复方四逆散提取物后,血浆中的芍药苷浓度.研究结果表明:四逆散配伍组方后,芍药苷的生物利用度较低.     

ICP-AES测定海产品中的微量元素

对照了湿法消解和微波消解直接消解湿基海产品的方法.采用微波消解样品,电感耦合等离子体-原子发射光谱法（ICP-AES）测定了12种海产品中Zn、Fe、Ca、Mg、Cu和Mn 6种元素的含量,在最佳工作条件下各元素的加标回收率在97.62％-106.0％之间,相对标准偏差（RSD）为0.59％-2.04％,实验结果为研究营养学提供科学依据.     

AO 3.0mm空心加压螺钉治疗腕舟骨骨折疗效观察

腕舟骨骨折是最常见的腕骨骨折,多发生于成年男性,易引起骨折不愈合和（或）腕舟骨缺血性坏死可能,一定程度上影响了患者的正常劳动生活。近年来,我院近采用AO 3.园mm空心加压螺钉治疗腕舟骨骨折,疗效满意,现报道如下。     

A New Exponential Gravity

We propose a new exponential f（R） gravity model with f（R） = （R - λc） e^λ（c/R）n and n 〉 3, λ ≥ 1, c 〉 0 to explain late-time acceleration of the universe. At the high curvature region, the model behaves like the A CDM model. In the asymptotic future, it reaches a stable de-Sitter spaeetime. It is a cosmologically viable model and can evade the local gravity constraints easily. This model shares many features with other f（R） dark energy models like Hu-Sawicki model and ExponentiM gravity model. In it the dark energy equation of state is of an oscillating form and can cross phantom divide line ωde = -1. In particular, in the parameter range 3 〈 n ≤ 4, λ ～ 1, the model is most distinguishable from other models. For instance, when n = 4, λ = 1, the dark energy equation of state will cross -1 in the earlier future and has a stronger oscillating form than the other models, the dark energy density in asymptotical future is smaller than the one in the high curvature region. This new model can evade the local gravity tests easily when n 〉 3 and λ 〉 1.     

Search for chiral bands in A~110 neutron-rich nuclei

High spin states in A~110 neutron-rich ¹⁰⁶Mo, ¹¹⁰Ru and ¹¹²Ru nuclei have been reinvestigated by measuring the prompt γ-rays from the spontaneous fission of ²⁵²Cf. Two similar sets of bands are observed to high spins in each of three nuclei. Through analyzing of characters of the band structures, the chiral doublet bands are suggested in ¹⁰⁶Mo, ¹¹⁰Ru and ¹¹²Ru.     

Control of dispersion in fiber coupled resonator-induced transparency structure

Induced transparency phenomena and strong dispersion can be produced in a coupled resonator induced transparency(CRIT) structure.In this paper,we investigate the influences of structure parameters,such as amplitude reflection coefficient and loss,on transmission spectrum and dispersion of CRIT structure,and further study the control of dispersion in the structure.The results show that in the CRIT structure,adjusting the loss of resonators is an effective method of controlling dispersion and producing simultaneous normal and abnormal dispersion.When we choose approximate amplitude reflection coefficients of the two couplers,the decrease of transmittance due to loss could be effectively made up.In the experiment,we achieve the control of dispersion and simultaneous strong normal and abnormal dispersion in the CRIT structure comprised of fiber.The results indicate the CRIT structure has potential applications in optical signal processing and optical communication.     

混凝土重力坝爆炸荷载数值分析及抗爆性能研究

利用LS-DYNA非线性有限元程序,基于Eulerian和Lagrangian耦合的方法,研究了RHT本构模型模拟的混凝土板在爆炸荷载下的动力反应,并且将数值结果与现场实验结果进行比较,由此说明了RHT本构模型模拟爆炸荷载下混凝土动力反应的有效性。研究了2tTNT炸药在距离坝体上游面10m不同起爆深度的情况下,有泡沫混凝土保护层和无泡沫混凝土保护层的坝体动力响应及其损伤状况。计算结果表明,无泡沫混凝土保护层时,坝体上游面主要损伤区域位置总是随起爆深度的增加向坝体底部移动;当上游表面有泡沫混凝土保护层时,坝体上游表面的损伤明显变小,下游面的损伤较无保护层情况也明显减小。表明泡沫混凝土能够有效减小混凝土大坝在爆炸荷载下的损伤,在提高混凝土大坝的抗爆性能方面起到很好的保护作用。