达旦黄-曲通X-100体系共振光散射法测定蛋白质

基于在Triton X-100存在下,蛋白质与达旦黄作用使得体系的共振光散射增强,在λ＝492 nm处光散射强度最大,增强作用的强弱与蛋白质的含量成正比,据此建立了共振光散射测定蛋白质的新方法。此方法对牛血清白蛋白的检出限达到17.7 ng·mL-1,线性范围为0.03～0.9 μg·mL-1,用于合成样与人血清样品的分析,取得了令人满意的结果。同时也研究了人血清白蛋白、鸡蛋白蛋白、溶菌酶、胰蛋白酶与达旦黄的作用。     

基于铰链式六面顶压机的二级6-8模超高压大腔体内置加热元件的设计与温度标定

 首次报道了一种新型的基于铰链式六面顶压机的二级6-8模大腔体静高压装置的内置加热元件的设计与温度标定。此加热组装结构简单,升温快,保温效果好,并有效地解决了国外基于两面顶压机构架下的二级6-8模内加热组装中热电偶在施加压力时易断的问题。以低成本的碳管为加热元件,采用直接和间接两种加热方式,用双铂铑（Pt6%Rh-Pt30%Rt）B型热电偶进行温度测量,并根据实验过程中加热功率与腔内实际温度的关系,对不同压力下腔体内的温度进行了标定。实验结果表明：此加热系统的油压达到40 MPa（腔体压力约10 GPa）时,温度可以达到1 700 ℃以上;在油压为30 MPa、样品室温度为1 000 ℃时,保温时间可达2 h,甚至更长;实验中获得样品的直径可达3 mm,高度可达7 mm,实现了在高温超高压条件下大样品的制备,满足了实验对产生高温超高压条件的需要。     

航天器对接相对位置姿态自主测量方法研究

航天器间相对位置姿态的准确测量是实现自主自动对接的先决条件。将三圆标志靶安装在目标航天器上;追踪航天器用数码相机对靶拍照。设计了亚像素处理方法实时处理数字照片,可精确测定圆心像点位置和特征直径的像长;用其作为基本特征参数,基于透视投影原理,建立了求圆心物空间坐标的公式,求出靶面的平面方程,可用来求两航天器间的相对位置姿态参数和实时标定相机的可变参数。计算机仿真结果表明,测距为2m时,测圆心像点位置的误差小于0.03个像素,测距误差小于1mm,测姿态角的误差小于0.01°。该方法也适用于无人直升飞机定点着陆时自主测量其相对位姿参数。     

A review of the metal stud stiffness on the sound insulation of gypsum-board partitions

For the sound insulation of a double-panel partition,the stud between two leaves creates a vibration transmission path,which can often be more critical and more important in the mid-frequency range than the airborne path through the cavity.Owing to the fact that partitions with light-weight steel studs are commonly used in building construction,studies on the sound insulation effect of such studs have been conducted.Especially,a model,initiated by Gu and Wang(1983),has been widely studied during the past decades.In the model,the steel stud is considered as an elastic spring with its cross-section stiffness in the sound insulation index prediction of such a partition.Experimental results of different stud profiles have been reported from different testing laboratories and more information has been gained to understand the stiffness effect of the stud on the sound insulation of the double-leaf partitions.In this paper,the authors have given this subject a thorough review and have concluded that a critical problem needs further investigation on the determination of the stiffness of the connecting elements in the double-leaf partitions.     

缩合法合成磁性荧光高分子CdTe@Fe_3O_4/P(NIPAM-co-AA)复合微球及其表征

具有超顺磁性和荧光特性的CdTe@Fe_3O_4/P(NIPAM-co-AA)多功能复合微球是以P(NIPAMco-AA)为模板制备而成.首先,采用溶胀法使模板微球带有磁性;其次,辅助TEOS和APTES两种化学试剂实现对Fe_3O_4/P(NIPAM-co-AA)微球表面的氨基功能化;最后,携带氨基的磁性微球与巯基乙酸修饰的CdTe量子点通过酰胺缩合反应,将量子点键合到磁性微球表面上,最终获得单分散的磁性荧光高分子复合微球.分别采用扫描电子显微镜、透射电子显微镜、倒置荧光显微成像系统、荧光分光光度计以及振动样品磁强计等方法对所获复合材料的结构与性能进行了表征.结果表明:复合微球单分散性良好,平均粒径约为30μm,饱和磁化强度可达5.4emu/g,具有良好的超顺磁性和较高的荧光发光效率.该材料将磁性、荧光结合到微米级高分子共聚物上,不仅解决了纳米粒子分离和处理的困难,而且奠定了多功能材料在生物标记、荧光成像等诸多领域潜在的应用基础.     

The application of laser reflective tomography in near-field measurements of ultrasonic transducers

With Laser Reflective Tomography（LRT）,the near fields of ultrasonic transducers were measured and analyzed.The principle of LRT measurement of ultrasonic field distribution was introduced and an experimental system was set up.Acoustic pressure of a multiple element piston transducer was measured by using of a laser vibrometer.Its distribution in amplitude and phase was obtained.The acoustic pressure in the same region was measured with a needle hydrophone to validate the LRT method.Furthermore,through reconstruction of acoustic fields,it indicated that LRT method is suitable for predicting the distribution on transducers＇surface and conditions of active elements.     

扫描环形光斑激光束优化研究

激光束的形状和能量分布限定了激光的应用范围,为满足不同的激光加工需要,必须对激光束进行变换。针对实验室用CO2激光器在热处理方面的应用,提出了激光扫描环形光斑光束优化法。基于温度场叠加原理建立了扫描环形光斑温度场的数学模型,模拟其温度场,可得到其温度分布特性;通过实验研究,分析了聚焦光斑与扫描环形光斑在激光淬火中对材料的热作用效果。结果表明,扫描环形光斑能改善激光热处理硬化层分布。理论和实验研究表明,激光扫描环形光斑技术可以实现激光热处理光束的优化,有一定的应用前景。     

无穷积分余项与其被积函数比值的收敛阶

对一类函数的无穷积分余项与该函数的比值得到当x趋于无穷大时的收敛阶,这类函数是幂函数与指数函数的乘积函数,并将其应用到Mittag-Leffler函数.同时考虑了对应的级数情形.     

“工作组”模式：国家治理现代化的中国经验

“工作组”作为一个广泛出现在中国政治实践中的重要现象和运作机制,在中国政治发展道路上发挥了举足轻重的作用。研究表明,“工作组”总是围绕党中央的中心任务,在不断常规化的权力运作中,提升“政党−国家”的现代化治理水平。“工作组”模式能够在实践层面联结一统体制和有效治理,在理论层面回应有关国家治理能力的讨论,从而以一种治理模式形成了国家治理现代化的中国经验。     

Low dispersion finite volume scheme based on reconstruction with minimized dispersion and controllable dissipation

The reconstruction with minimized dispersion and controllable dissipation(MDCD) optimizes dispersion and dissipation separately and shows desirable properties of both dispersion and dissipation.A low dispersion finite volume scheme based on MDCD reconstruction is proposed which is capable of handling flow discontinuities and resolving a broad range of length scales.Although the proposed scheme is formally second order accurate,the optimized dispersion and dissipation make it very accurate and robust so that the rich flow features encountered in practical engineering applications can be handled properly.A number of test cases are computed to verify the performances of the proposed scheme.