金刚石单晶合成工艺与铁基触媒中初生Fe3C形貌的关系

利用光学显微镜和X射线衍射等手段,表征了高温高压下合成金刚石单晶时不同合成工艺的铁基触媒合金组织结构.结果发现:金刚石合成效果较好时的触媒组织中Fe3C呈规则的条状,而合成效果不好时的触媒组织中局部出现了不规则的团絮状Fe3C.分析认为,Fe3C在不同的结晶条件下表现出不同的生长行为,高温高压下金刚石单晶的生长与触媒中Fe3C的生长行为有密切关系.     

生物应用锌(Ⅱ)荧光探针研究进展

本文对近年来生物应用锌(Ⅱ)荧光探针研究进展进行了较详细地评述,并对其化学规律、性质和某些局限性进行了讨论。     

以TiO2-SiO2为载体的联吡啶钌对氧敏感性的研究

近年来,有关氧传感器的研究最主要的是氧猝灭传感器,它是基于降低荧光强度,或通过时间分辨荧光进行测定。研制氧传感器的关键在于制备性能优良的氧传感膜。即要求使用对氧敏感性较强的荧光指示剂。其敏感物主要有两类,第一类是有机金属络合物,如钌络合物,锇络合物等。另一类是多环芳香烃和卟啉,如芘二丁酸,四苯基卟啉等。本文使用的是有机金属络合物联吡啶钌（Ru（bpy）3Cl2）,它在蓝色波长光的激发下能产生红色荧光,而氧对其荧光具有猝灭作用。通过检测荧光被猝灭的程度则可达到检测氧气的目的。     

薄壁件加工系统动态响应分析

薄壁件在铣削加工中容易产生共振或变形,直接影响加工稳定性及加工精度。采用主轴-刀具-工件整体铣削系统连续梁模型,系统研究在动态铣削力作用下,刀具端部与工件端部的动态响应之间的相互影响关系以及对整体系统动态响应影响较大的薄壁件尺寸。结果表明,工件横截面高度对系统共振的影响较为明显,当高度尺寸较小时,工件的低频共振会通过动态铣削力直接反映到刀具端部的振动频响上。工件横截面底边宽度尺寸的增大虽然对共振频率的改变不太明显,但会导致激发出来的刀具共振幅度出现明显降低。研究成果可以为薄壁件铣削加工系统的稳定性控制提供理论基础。     

Dielectric and ferroelectric properties of Sr_4CaSmTi_3Nb_7O_(30) with tetragonal tungsten bronze structure

Sr4CaSmTi3Nb7O30ceramics are synthesized and indexed as tetragonal tungsten bronze structure. The dielectric behavior and ferroelectric nature are investigated. Three dielectric anomalies are observed. The phase transition is a displacive phase transition with some diffusive characteristics, which indicates possible compositional variations within the materials on the microscopic scale. The weak distortion disappears in cooling process for differential scanning calorimetry measurement, and the large depression of Curie–Weiss temperature T0 indicates the difficulty in forming macroferroelectric domain. The ferroelectric nature in these filled tungsten bronze niobates originates from the off-center displacement of Bsite cations, but they are primarily dominated by A-site cation occupation. Both the radius and the valence of A1-site cations play an important role on ferroelectric properties of the filled tungsten bronze compounds. Existence of spontaneous polarization with a remanent polarization of 0.16 μC/cm2 a coercive field of Ec = 11.74 kV/cm confirms the room-temperature ferroelectric nature of Sr4CaSmTi3Nb7O30 ceramics.     

近红外激光照明器均匀性评价技术研究

近红外激光照明是在低照度情况下,用近红外激光作为光源对远距离目标进行主动照明.由于激光的产生机制、匀光装置和照明器采用的光学系统公差、大气湍流等因素,近红外激光光束在目标面上的光强空间分布不均匀,对成像、观测准确度产生较大影响.本文提出采用近红外激光光强功率谱衡量照明近红外激光光强分布均匀性,即采用归一化后光强功率谱所围成的面积作为衡量近红外激光照明均匀性的参量.利用这种方法,对不同的近红外激光照明器,在相同的工作状态下的照明均匀性评估参量进行了研究,结果验证了采用归一化后光强功率谱所围成的面积作为评价参量的合理性.     

Performance of an Accelerometer Suspended by a Pendulum

Performances of an accelerometer suspended by a pendulum and set on ground directly are both discussed. Theoretical analysis shows that the isolation from seismic disturbances of such a suspending accelerometer is equal to that of a narrow band-pass electronic filter. This means that the effect of seismic noises to the accelerometer can be substantially suppressed by means of a pendulum suspension during its performance tests.     

两个模糊数乘积运算

两个模糊数的乘积运算是根据扩张原理定义的。本文根据扩张原理给出了非线性规划方法、解析法、计算机作图法和计算机模拟方法四种求解两个模糊数的乘积问题的方法，四种方法各有优缺点，对每个方法通过实例作了说明。     

病毒与致癌作用——有关肿瘤的病毒病因问题

一引言致癌作用指诱发肿癌的成癌的因子及其作用的方式,因此它包括病的病因与发病机理。两个世纪的临床观察和七○年来的实验研究,特别是最近二十年对致癌作用累积了相当丰富的知识,但在许多重要方面仍旧还不清楚,对这问题的全面分析在目前还有一定的困难。我们对这问题的认识似乎已到了一个极端复杂性的阶段而还不能把所累积的知识作出满意的和有条理的综合。     

THE FORMATION, EVOLUTION AND CAUSE OF THE Mu Us DESERT IN CHINA

Comprehensive correlation and analysis on the stratigraphic structure of the Quaternaryeolian sand in the Mu Us Desert comfirm that the Desert has been in existenceintermittently since the initial stage of the Quaternary at latest. The Desert is asteppe type sandy desert characterized by mosaic distribution of shifting, semi-shifting, semi-fixed and fixed dune and areas of loess grass land. It did not evolve toward uniform shift-ing sand, but underwent a series of normal and reverse development processes from the occur-rence of shifting sand to the spread, fixation and reduction of the sandy desert to grassland.Climatic fluctuation since the Quaternary is the primary factor for the formation and evolutionof the Desert, while neotectonics and human activities are the secondary factors.