Generalized mean-square amplitudes of vibration in some XY4 type ions (II)

The generalized mean-square amplitudes of vibration and mean amplitudes of vibration have been computed for CrO^3-₄, Mn¹⁸O^-₄, MoSe^2-₄ and WSe^2-₄ ions at three temperatures, T = 0°K, T = 298°K, T = 500°K, employing Cyvin's method. The results have been discussed in the light of atomic weight and electronegativity of the atom in the ionic system.     

Tüpfelmethode auf Phosphat,angewandt in prähistorischer Forschung (als Feldmethode)

Zusammenfassung Die Tüpfelmethode nachFeigl auf Phosphat wurde durch die Einführung von Ascorbinsäure als Reduktionsmittel als Feldmethode modifiziert. Sie eignet sich entsprechend ihrer leichten und raschen Ausführbarkeit und Empfindlichkeit zur Untersuchung von Bohrprofilen auf die in prähistorischen Siedlungsschichten erhöhten Phosphatgehalte.

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Summary The spot test for phosphate developed byFeigl was modified by the use of ascorbic acid as the reducing agent; a field method results. In accord with the ease of conducting this test and its rapidity, and sensitivity, it has proved useful for the study of boring profiles with respect to their enhanced phosphate contents in prehistoric settlement strata.

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Résumé On a modifié la méthode à la touche deFeigl pour les phosphates sur le terrain, en employant l'acide ascorbique comme agent de réduction. En raison de son exécution facile et rapide et de sa sensibilité, elle convient à l'étude des profils de carottage pour les teneurs en phosphates élevées dans les couches de dépôts préhistoriques.

     

Beiträge zur Chromatographie organischer Substanzen. VI. Die Dünnschichtchromatographie der Kohlehydrate

Zusammenfassung Es wird über die Trennung einiger Mono-, Di- und Trisaccharide auf Kieselgur- und Kieselgelträgern berichtet. Ferner wird die Trennung Raffinose-Saccharose bei ungünstigen Mengenverhältnissen (z.B. Melasse) durchgeführt und hierzu eine verbesserte Keilstreifentechnik entwickelt.

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Summary A report is given on the separation of several mono-, di-, and trisaccharides on kieselguhr and silica gel carriers. In addition, the raffinose-saccharose separation was carried out with unfavorable quantity ratios (for example molasses) and an improved wedge strip technique was developed.

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Résumé On décrit la séparation de quelques mono-, di- et trisaccharides sur supports de kieselguhr et de gel de silice. On réalise ensuite la séparation raffinosesaccharose en proportions quelconques (par exemple mélasse) et l'on propose à partir de cela une technique de la bandelette en forme de coin améliorée.

     

我国区域绿色技术创新效率的分类测度和提升模式研究——基于非期望产出的SBM-SupSBM模型

本文首先运用考虑非期望产出的SBM-SupSBM模型估计我国各省市绿色技术创新效率并进行分类:稳定上升类、平稳类、大幅度波动类以及下降类。之后从企业内部和外部两方面对绿色技术创新效率提升的影响因素提出假设,着重考虑大幅度波动类别省份的效率提升。运用面板数据模型各影响因素进行验证,结论显示:企业规模对绿色技术创新效率波动较大的省份起到显著的抑制作用,环境规制和技术进步对绿色技术创新效率波动较大的省份作用不明显。针对分析结果,提出结论:在提升绿色技术创新效率的过程中,应注重企业规模和技术进步的协同作用,以及技术的开放程度。     

Scanning Kelvin Microscope: a new method for surface investigations

Based on the well known Kelvin probe for work function measurements a new microstructure analysis system - the Scanning Kelvin Microscope - has been developed. It allows to measure simultaneously with high lateral resolution the distribution of the contact potential difference (CPD) between a conductive sample and a reference probe together with the topographical structure of the sample surface. The measurement is contact free and non-destructive and can be carried out in natural environments. At present the lateral resolution of the measurement approaches 5 microm. The results can be displayed on a computer in three dimensional colour pictures.     

AFM and XRD investigation of crystalline vapor-deposited C60 films

The morphological and structural properties of C₆₀ films deposited on quartz substrates by sublimation at 320–500° C under high vacuum have been investigated using atomic force microscopy (AFM) and reflection X-ray diffraction (RXRD). The thickness of the films varied between 0.2 m and 10 m. AFM showed that the films consist predominantly of cubic crystals of a few micrometer in size with well-developed (111) and (100) faces. The crystallographic investigation revealed a strongly preferred [111] growth direction which is very sensitive to the deposition rate and substrate temperature. The influence of the experimental parameters on the morphology of the crystals and on the preferred orientation of the films is discussed in view of the AFM and RXRD results.     

Laser processing integrated into machine tools — design,applications, economy

In the last few years, lasers have found new applications in production engineering as tools for surface treatment, cutting, welding, drilling and marking. So far, the laser has mainly been used in special laser processing machines (laser-only) directly integrated into a production line or serving as stand-alone stations in the workshop. By combining conventional metal cutting technologies with laser processes in one machine, complete processing of a workpiece with different technologies in one setting can be realized. The main advantages are a reduction of the material flow between the production machines, which leads to a reduction in processing time and logistics, and an enhancement of manufacturing quality due to the processing in one setting. In addition to this approach, new processing technologies such as laser-assisted machining are possible.Applications of laser caving, hardening, welding and drilling of production parts in combination with the cutting process in one setting have been investigated with the aim of adapting these technologies to the characteristics of the machines and the typical parts spectra. Furthermore, various technical solutions for the integration of lasers into milling centres and lathes have been elaborated. In both situations the laser tool is handled like a standard tool and can be exchanged automatically. The main results will be reported, together with a brief discussion of the economic aspects of laser processing integrated into machine tools.This article is based on an invited paper presented at LANE '94, Erlangen, 12–14 October 1994.