电磁轨道炮高速滑动接触电阻的定量表征

从描述电磁轨道炮炮口电压波形的场路模型出发,构建了电枢/轨道高速滑动接触电阻与轨道电流波形、炮口电压波形、电枢膛内速度曲线和轨道结构参数之间的关系,依据此关系可定量表征电磁轨道炮高速滑动接触电阻。实例计算表明,电枢/轨道高速滑动接触电阻的变化依赖于轨道电流变化,对应电流上升段、平顶段和电流下降段。在平顶段接触电阻最小约0.2 m,在电流上升段和电流下降段,接触电阻达3 m。     

基于灰度曲线交点的结构光编码条纹边缘检测

在分析结构光编码白条纹扩散的原因和实际边缘形态的基础上,提出一种同时检测多边缘并消除扩散影响的亚像素精度方法--交点法.首先向被测表面投射互为反色的两组格雷编码图案,提取两组强度图像中灰度梯度较大的点作为边缘依据点,并对其进行曲线拟合,然后将对应拟合曲线的交点作为边缘.分析了交点法对结构光系统中常见的被测表面倾斜和离焦两个主要误差因素的适应能力.介绍了检测原理及误差因素分析,并进行了边缘检测实验.实验结果表明,对于宽度大于4 pixel的编码条纹,边缘检测相对误差小于1%,可消除被测表面倾斜和离焦的影响.     

PdNi/Ni Nanotubes Assembled by Mesoporous Nanoparticles for Efficient Alkaline Ethanol Oxidation Reaction

The optimization of structure and composition is essential to improve the performance of catalysts. Herein, mesoporous nanoparticles assembled PdNi/Ni nanotubes (mPdNi/Ni NTs) are successfully fabricated using nickel nanowires as sacrificial template. The combination of nanotubular structure with mesoporous nanoparticle morphology can provide facilitated transfer channels and sufficient active sites, allowing the full contact and reaction between catalysts and reactants. Therefore, the synthesized mPdNi/Ni NTs exhibite superior ethanol oxidation performance to mesoporous Pd nanotubes and commercial Pd black. This study proposes a rational strategy for the development of nanoparticle assembled nanotubes with surface mesoporous morphology, which can greatly improve catalytic performance in various electrocatalytic fields.     

IVDAS: an interactive visual design and analysis system for image data symmetry detection of CNN models

Journal of Visualization - Convolutional neural networks (CNNs) have achieved breakthrough performance in image recognition and classification. However, it is still a challenge for CNNs to classify...     

Chemical Constituents of the Roots of Phlomis betonicoides and Their Anti-Rotavirus Activity

Chemistry of Natural Compounds - Two new isobenzofuranone derivatives (1 and 2) together with six known compounds (3–8) were isolated from the roots of Phlomis betonicoides, a highly sweet...     

电磁轨道发射装置隔离式分压器

研制了一套用于测量电磁发射装置轨道电压信号的隔离式分压器,实现了测量回路与被测回路之间的电隔离,简化了电磁发射装置测试系统的复杂性。并对影响隔离式分压器频率响应的元件参数进行了参数扫描,结果表明：研制的分压器在-3 dB区间的频率响应范围为14 Hz~18 MHz,满足电磁发射装置轨道电压信号的测试要求。使用P6015A高压探头进行比对标定,输出信号的前沿约1s,频率响应满足电磁轨道发射装置轨道电压信号的测量要求。同时用隔离式分压器及电阻分压器测量轨道电压信号,两者波形符合较好。     

电化学条件下富电子芳烃的C—H官能团化实现烯烃的1,2-二芳基化

传统的烯烃二芳基化主要手段是,先通过过渡金属催化的芳基亲电试剂与烯烃发生交叉偶联,然后再与芳基亲核试剂发生反应[1].但是这种反应策略存在原子经济性低及反应步骤多的缺点.因此急需发展一种高效、高原子经济性的合成方法来实现烯烃的二芳基化.2015年,Bunel/Lei课题组[2]报道了FeCl3/2,3-二氯-5,6-二...     

Preparation and physicochemical properties of konjac glucomannan ibuprofen ester as a polysaccharide-drug conjugate

Abstract

A novel drug-polysaccharide conjugate with konjac glucomannan (KGM) as a drug carrier was fabricated through the esterification of ibuprofen (IBU), an anti-inflammatory drug, with KGM. The influences of the reaction conditions, such as the amount of ibuprofen acryl chloride, reaction time, reaction temperature, and the amount of catalyst, on the degree of substitution were investigated. KGM ibuprofen ester (KGM-IBU) was characterized by Fourier transform infrared spectrometry (FTIR), X-ray diffraction (XRD), solid-state ¹³C NMR, scanning electron microscopy (SEM), transmission electron microscopy (TEM), thermogravimetric analysis (TGA), differential scanning calorimetry (DSC), and dynamic mechanical analysis (DMA). The hydrophobic structure of IBU in KGM-IBU was proven by the fluorescence emission spectra of pyrene. In addition, by using commercially available ibuprofen sustained-release capsules (IBU-SRC) as a control, the in vitro controlled release performance of KGM-IBU was evaluated. The cumulative release of IBU-SRC within 36?h was 94%, while that of KGM-IBU within 36?h was 77%. The results showed that KGM-IBU had better sustained-release performance without a burst release effect. The obtained products could be used as a potential biocompatible sustained-release drug delivery system.     

毛细管气相色谱法同时测定水产品中的多氯联苯和有机氯农药残留量

建立了毛细管气相色谱法同时测定水产品中多氯联苯和有机氯农药的方法，用高氯酸与冰乙酸的混合溶液消化样品，以石油醚提取，浓硫酸净化后，用毛细管气相色谱法测定，方法的回收法为88％－110％，相对标准偏差为8％－19％（n=6)，检出限为0．08－0．60ug/kg，方法简便，快速，结果准确。     

丙酮在XeCl准分子激光辐射下的多光子电离和碎裂研究

我们用扩散分子束多光子电离光谱技术研究了丙酮在XeCl准分子激光辐射下的多光子电离和碎裂行为。实验表明丙酮没有产生母体离子峰(m/e=58), 只给出m/e=43和15两个峰, 分别对应于丙酮光解所产生的两个碎片CH_3 CO和CH_3。其离子信号(1)分别与激光强度(Ⅰ)的3和3.6次方成正比。分析表明离子是由中性碎片电离产生的。