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931.
在中专物理教学中如何建立一套适合素质教育的考试模式呢?下面笔者结合自己的物理教学实践谈一些做法与想法.1 校内考试手段多样性 现行的考试是一份试卷定优劣,很多学生对考试望而生畏.如何使全体学生都乐于考试?并通过考试的诱导,全面提高学生的基本素质,促进学生全面和谐发展,这就需要注重考试方式的多样性. 相似文献
932.
933.
Yingyu Hu Guoqiao Lai Yongjia Shen Yongfang Li 《Monatshefte für Chemie / Chemical Monthly》2004,33(2):1167-1172
Zinc(II) and magnesium(II) phthalocyanines bearing four substituted propylenedithiotetrathiafulvalene (PDT-TTF) units were synthesized and characterized by NMR, MS, EA, and UV/VIS spectra. The absorption peaks of two target molecules were hypsochromically shifted compared with the phthalocyanine parent compound. Studies using cyclic voltammetry indicated that introduction of Zn and Mg as central metals enhanced the electronwithdrawing between the phthalocyanine core and the PDT-TTF unit, thus losing one electron to form (PDT-TTF)+ becomes more difficult. 相似文献
934.
Klai Nadia Berredjem Malika Khettache Nawel Belghit Med Yazid Rgaïnia Zine Nour‐Eddine Aouf 《Journal of heterocyclic chemistry》2004,41(1):57-60
Dedicated to the memory of Pr. Ladjama Daif A series of chiral cyclosulfamides have been synthesized by alkaline cyclisation starting from N‐benzoylamino acids (Ala, Val, Leu, Phe) derivatives and chlorosulfonyl isocyanate. A simplified and regioselective deprotection of the cyclic compounds (cyclosulfamides) containing the tert‐butyloxycarbonyl group (Boc) has been achieved in good yield by fusion under reduced pressure. 相似文献
935.
Andrew Bach Xinglong Jiang Joseph Mckenna Kapa Prasad Oljan Repic Wen‐Chung Shieh 《Journal of heterocyclic chemistry》2004,41(4):637-640
An efficient approach has been developed for the synthesis of an isofervenulin analogue 1 employing a one‐pot condensation‐substitution reaction of a chlorocarboethoxytriazine (electrophile) with a urea (nucleophile). The resulting cyclization reaction resulted in the synthesis of a pyrimido‐heterocycle in good yield in either acidic or basic media. The former was assisted by utilizing trimethylsilyl chloride. 相似文献
936.
Crystal Structure of the Zinc Amide Zn[N(SiMe3)2]2 X‐ray quality crystals of Zn[N(SiMe3)2]2 (monoclinic, P21/c) are obtained by sublimation of the zinc amide Zn[N(SiMe3)2]2 at —30 °C in vacuo (300 torr). According to the result of the X‐ray structural analysis, Zn[N(SiMe3)2]2 contains an almost linear N‐Zn‐N unit with two short N‐Zn bonds. 相似文献
937.
Qingfa Wang Li Wang Yaquan Wang Fei He Zhenhua Li Zhentao Mi 《Reaction Kinetics and Catalysis Letters》2004,81(2):297-304
Deactivated palladium catalysts in the hydrogenation of anthraquinione were regenerated with ethanol, nitric acid, hydrogen
peroxide, boiling water and steam, respectively. The deactivated and regenerated catalysts were characterized by XPS, ICP,
TG, FTIR, TPD, XRD, etc., and studied in the hydrogenation of anthraquinone. The results showed that the main cause of catalyst deactivation is the
coverage of the active component by deposits. The treatments by hydrogen peroxide and boiling water can effectively regenerate
the deactivated catalysts.
This revised version was published online in August 2006 with corrections to the Cover Date. 相似文献
938.
T. G. Elizarova A. V. Zherikov I. S. Kalachinskaya Yu. V. Sheretov 《Computational Mathematics and Modeling》2004,15(1):52-68
A new quasi-hydrodynamic algorithm is proposed for numerical analysis of convective flows in the presence of a homogeneous external magnetic field. The Marangoni convection problem in a square cross-section cavity is solved. 相似文献
939.
940.
A new chemiluminescence method for the determination of carbamazepine (CBZ) has been developed. The method is based on the chemiluminescence produced in the reaction of tris(2,2'-bipyridine)ruthenium(III) and CBZ in an acidic medium. The chemiluminescence intensity was enhanced by organic solvents in the reaction system. Under the optimum experimental conditions, the calibration curve was linear over the range 4.0 x 10(-3)-8.6 x 10(-7) mol/L for CBZ. The detection limit (S/N = 3) was 2.5 x 10(-7) mol/L and the relative standard deviation of six replicate measurements was 2.6% for 4.0 x 10(-4) mol/L of CBZ. The possible reaction mechanism were also discussed. The chemiluminescence method was successfully applied to assay the CBZ contents in pharmaceutical tablets. 相似文献