电场催陈米酒核磁共振分析

以自行研制的设备对新产广东玉冰烧米酒进行催陈 (处理条件 :4 0kV·m- 1 的电场强度处理 180min ,5 0Hz) ;然后采用1 HNMR对新酒、电场催陈酒及成品酒进行了分析 ,研究发现新酒中甲基和亚甲基峰出现了 4个杂峰而其他样品没有 ,说明新酒中单分子与各种状态的缔合结构共存 ,其他各主要有机物质亦参与成峰 ;而关于羟基质子峰 ,新酒为平头峰 ,推断出溶液中有 2种羟基质子存在 ,一种参与形成缔合 ,另一种未参与缔合 ;成品酒为单一峰 ,说明溶液中形成了单一稳定的大分子缔合结构 ;电场处理酒样为不规则峰 ,反映出多种缔合状态共存 ,其主要缔合结构接近成品酒缔合结构     

表面活性剂增敏2,4-二氯苯基荧光酮分光光度法测定煤中的微量锗

研究了在表面活性剂存在下,锗与2,4二氯苯基荧光酮(2,4DClPF)的显色条件,在18～25mol·L-1硫酸介质中,锗与2,4DClPF、阳离子表面活性剂十六烷基三甲基溴化铵(CTMAB)形成有色三元胶束络合物,其最大吸收波长为516nm,表观摩尔吸光系数ε为138×105L·mol-1·cm-1。方法的线性范围为0～125μg·25mL-1,回收率为103%～106%,相对标准偏差为11%～17%。所拟方法用于煤样中微量锗的测定,结果较满意。     

Direct numerical simulation of passive scalar in decaying compressible turbulence

1IntroductionDirectnumericalsimulation(DNS)becomesanimportanttoolinrecentresearchofturbulence[1].DNSofcompressibleturbulenceismoredifficultthanthatoftheincompressibleturbulence.WhentheturbulentMachnumberisgreaterthan0.3theshockletsmayappearinthecompressibleturbulentflowfields.Thereasonandmechanismofshockletsexistencearenotclearyet.TheturbulentMachnumberinDNScannotbeveryhighwiththepresentexistingnumericalmethodsandcomputerresource.Fortheproblemofcompressibleisotropicturbulencewiththeinitia…     

Calculation of geometrical birefringence from two-dimensional refractive-index profile in single-mode fibres

We present two numerical approaches to calculate the geometrical birefringence from two-dimenslonal refractive-index profile in single-mode fibres. One is the improved perturbation model theory, the other is based on the general solution of noncircular uniform optical waveguide in an arbitrary coordinate system. Using these methods, we can obtain not only the magnitude of geometrical birefringence, but also the orientation of birefrlngent axes. We report the calculation results of geometrical birefringence in a real single-mode fibre.     

Investigation of photoelectron temporal characteristics in silver halide microcrystals using the microwave absorption technique

The free photoelectron lifetime reflects to a large extent the latent image formation efficiency and sensitivity of silver halide material. The microwave absorption dielectric-spectrum technique enables measurement of the photoelectron decay process of silver halide emulsion exposed to 35ps laser pulse. For T-grain AgBr emulsion, the relationship between exciting energy and photoelectron action has been obtained, and the influence of iodide dopants on photoelectron lifetime was measured and analysed. The photoelectron lifetime of dye-sensitized AgBr emulsion with tabular grains is shorter than that with cubic grains, and the latent image formation efficiency of the former is higher than the latter.     

Determination of q=1 surface by the variation of pellet ablation rate on the HL-1M

Strong drop of Hα emission has been observed on the HL-1M tokamak by means of a detector array while a pellet crosses the q=1 surface. In this article, the q=1 surface has been determined precisely by the interval and the shape of the Hα emission striations on the pellet trajectory due to the variation of pellet ablation rate. The q-profile and current density distribution at the plasma centre region have been calculated according to the pellet ablation rate and the magnetic shear feature.     

General demonstration of principal states of polarization and real-time monitoring of polarization mode dispersion in optical fibres

We investigated the general properties of polarization effects in optical fibres and demonstrated the existence of socalled principal states of polarization (PSP), which mean the fixed points in mathematics, in different polarization effects,such as birefringence and polarization mode dispersion, by using fixed point theory. Furthermore, a time evolution vector is defined to describe the time evolution of polarization state in optical fibres, which is used to investigate the time evolution of polarization mode dispersion vector (PDV), including differential group delay and PSP. The experimental results of real-time monitoring of PDV by using this method are reported. To our knowledge, this is the first report on monitoring PSP evolution in optical fibres.     

环形光束的聚焦性质研究

从理想的环形光束出发,理论上分析了环形聚焦光束在焦点附近的光强分布情况,以及光束内外径之比对聚焦性质的影响.然后利用数值模拟的手段,研究了带软化因子的环形光束的聚焦性质,在整体上给出了环形光束的聚焦性质.     

红外单站被动定位技术速度更新算法研究

针对红外单站被动定位技术中空中机动目标的运动速度不断变化这一实际情况,提出了一种基于红外相机运动特性的对目标的运动速度进行实时更新的校正算法.该算法克服了大多基于匀速直线运动这一空间模型的红外单站被动定位方案目标速度不变的缺点,客观地反映了空中机动目标的实际运动状况,不仅能对目标的运动速度进行实时准确的更新校正,而且可推演出一种新的红外单站被动定位算法,对推动红外单站被动定位技术的工程实用化进程具有重要的意义.     

变线距光栅线密度的干涉测量

变线距光栅在同步辐射装置、激光核聚变装置上有着广阔的应用前景，它的制作和检测方法尚未成熟。用干涉法测量变线距光栅的线密度，给出了测量原理、实验中的光路、数据处理的方法、测量结果。在待测光栅表面，衍射光干涉条纹的数量和密度是入射光干涉条纹和倍增后光栅的刻线之差。采用共光路的方案，使光路具有很强的抗干扰能力。用中值滤波消除干涉图像中的干扰。针对不同的干涉条纹，讨论和比较了两种测量方法，提出相对密度不变性。证明了干涉法完全可以用于变线距光栅的线密度测量，并能达到一定的精度，初步解决了检测问题，认为这种方法也可以用于变线密度光栅的加工中。