湿化学法合成Co掺杂ZnO薄膜的微结构及发光特性

采用湿化学法在ITO玻璃衬底上制备了纳米棒结构的Co掺杂ZnO薄膜.XRD结果表明Co掺杂的ZnO没有出现杂相.SEM结果表明掺杂样品是由ZnO纳米棒团簇结构组成,且团簇的密度随着Co掺杂浓度的增大而增大.光致发光光谱表明Co掺杂导致薄膜的带隙发生红移.     

Riemann–Hilbert problem for the modified Landau–Lifshitz equation with nonzero boundary conditions

Theoretical and Mathematical Physics - We study a matrix Riemann–Hilbert (RH) problem for the modified Landau–Lifshitz (mLL) equation with nonzero boundary conditions at infinity. In...     

聚芳亚胺的合成、结构与性能

以不同的二碘化合物和芳香二胺为单体,通过两种不同的方法经缩聚反应得到了系列高分子量、低分布的聚芳亚胺。其结构由FT-IR, 1H NMR1和元素分析表征。由DSC和TG测定结果可知,该系聚合物具有较高的玻璃化转变温度(Tg＞150℃)和良好的热稳定性(TD＞400℃)。另外,该系聚合物还表现出良好的溶解性能。     

Determination of residues of 446 pesticides in fruits and vegetables by three-cartridge solid-phase extraction-gas chromatography-mass spectrometry and liquid chromatography-tandem mass spectrometry

A method was developed for determination of residues of 446 pesticides in fruits and vegetables through the use of cleanup by a 3-cartridge solid-phase extraction-gas chromatography/ mass spectrometry (GC/MS) and liquid chromatography/tandem mass spectrometry (LC/MS/MS). Fruit and vegetable samples (20 g) were extracted with 40 mL acetonitrile, salted out, and centrifuged. Half of the supernatant was passed into an Envi-18 cartridge, eluted with acetonitrile, and cleaned up with Envi-Carb and aminopropyl Sep-Pak cartridges in series after concentration of the eluates. Pesticides were eluted with acetonitrile-toluene (3 + 1, v/v), and eluates were concentrated to 0.5 mL and then added into internal standards after solvent exchange with 2 mL hexane and used for determination of 383 pesticides by GC/MS. The other half of the supernatant was concentrated to 1 mL and cleaned up with Envi-Carb and aminopropyl Sep-Pak cartridges in series. Pesticides were eluted with acetonitrile-toluene (3 + 1, v/v), and the eluates were concentrated to 0.5 mL, dried with nitrogen gas, diluted to 1.0 mL with acetonitrile-water (3 + 2, v/v), and used for determination of 63 pesticides by LC/MS/MS. The limit of detection for the method was 0.2-600 ng/g depending on the individual pesticide. In the method, fortification recovery tests at high, medium, and low levels were conducted on 6 varieties of fruits and vegetables, i.e., apples, oranges, grapes, cabbage, tomatoes, and celery, with average recoveries falling within the range of 55.0-133.8% for 446 pesticides, among which average recoveries between 60.0-120.0% accounted for 99% of the results. The relative standard deviation was between 2.1-39.1%, of which a relative standard deviation of 2.1-25.0% made up 96% of the results. Experiments proved that the method was applicable for determination of residues of 446 pesticides in fruit and vegetables.     

光反射材料对飞行时间探测器性能的影响

在北京正负电子对撞机直线加速器试验束上测试TOF闪烁体在不同光反射材料下(tyvek, teflon, millipore, ESR及镀铝薄膜)的性能, 包括时间分辨率, 衰减长度及光在闪烁体中的有效传播速度. 就时间分辨率来说镀铝薄膜较好达到95.6±2ps, 就衰减长度来说ESR最好, 对于光在闪烁体中的有效传播速度几种光反射材料大致相同.     

YL12铝合金铁离子注入层的摩擦学特性研究

对 YL12铝合金进行了铁离子注入 ,用俄歇电子能谱 (AES)分析了注入层剖面元素分布 ,同时考察了注入层的表面显微硬度、脆性和在干摩擦条件下的摩擦磨损特性 .采用扫描电子显微镜 (SEM)对磨痕表面形貌进行了观察分析 .研究结果表明 :铁离子在注入层中沿剖面呈高斯分布 ;注入层表面显微硬度有所增加 ,摩擦系数显著降低 ;当注入剂量为 7× 10 1 6 Fe / cm2 时 ,注入试样的耐磨性为未注入试样的 3 80 0倍 ;随着铁离子注入剂量的增大试样的表面脆性增加 ,耐磨性降低 ;注入前材料的磨损机制以粘着磨损和磨粒磨损为主 ,注入后磨损机制则以氧化磨损为主     

The N-coupled higher-order nonlinear Schrödinger equation: Riemann-Hilbert problem and multi-soliton solutions

In this work, the Riemann-Hilbert (RH) problem of the N-coupled high-order nonlinear Schrödinger (N-CHNLS) equations is studied carefully, which controls the propagation of N fields with all high-order effects such as high-order dispersion, self-steepening effect, and Raman scattering in optical fiber. The spectral analysis of the Lax pair associated with a (2N+1)×(2N+1) matrix spectral problem for the N-CHNLS equations is firstly carried out, from which a kind of RH problem is structured. Then a series of multi-soliton solutions including breather, bright, and dark solutions for the N-CHNLS equations can be formulated by the RH problem with the reflection-less case. In addition, with N=4 taken as an example, the propagation behavior of these solutions and their interactions are presented by selecting appropriate parameters with some graphics.     

兰州重离子加速器冷却储存环上强子物理研究计划及现状

An internal target experiment at HIRFL-CSRm is planned for hadron physics, which focuses on hadron spectroscopy, polarized strangeness production and medium effect. A conceptual design of Hadron Physics Lanzhou Spectrometer (HPLUS) is discussed. Related computing framework involves event generation, simulation, reconstruction and final analysis. The R & D works on internal target facilities and sub-detectors are presented briefly.     

一种基于分支过程的信息流行度动力学模型

Web 2.0时代,建模和预测在线信息流行度是信息传播中的重要问题.本文基于社交网络系统信息传播的机制,通过假设和简化,提出了分支过程的概率模型,来描述在线社交网络信息的流行度动力学过程.对典型在线社交网络系统的信息流行度数据和网络结构数据进行了分析,统计结果表明信息流行度衰减遵循幂律分布(幂指数为1.8),微博网络的入度和出度分布也均服从幂律分布(幂指数为1.5).模型仿真结果发现,该模型能够再现真实社交网络数据的若干特征,且信息流行度与网络结构相关.对模型方程进行求解得到理论预测的结果与仿真分析和实际数据结果相符合.