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51.
52.
Data on the structures and reactions of heterocyclic diazo compounds that lead to the formation of new heterocyclic systems as a result of intra- or intermolecular cyclization and rearrangements are systematized.Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 5, pp. 579–603, May, 1980. 相似文献
53.
The service life of ABS polymer, stabilized by 2-(3,5-di-tert-butyl-4-hydroxyanilino)-4,6-bis(octylthio)-1,3,5-triazine and containing 50% of a modifying rubber component, was estimated from oxidative induction times measured by DSC in isothermal mode in the temperature interval 140–170°C. The lifetime of ABS powder at the actual temperature of drying was predicted by linear extrapolation according to Arrhenius. However, the extrapolated value was much longer than the real lifetime determined from the long-term oven aging tests at 70 and 90°C, simulating the industrial drying process. The effect of changes in the apparent activation energy of oxidation due to antioxidant consumption during polymer aging is discussed. 相似文献
54.
Š. Višňovský 《Czechoslovak Journal of Physics》1987,37(12):1377-1393
The paper presents the classification of the electronic empty lattice eigenvalues and the classification of the Bloch sums for the garnet structureIa3d (O
h
10
) at the symmetry points, H, P, andN of the Brillouin zone. This provides a starting point for the energy band studies of these technologically important materials.The author thanks Dr. V. Frei for useful comments. 相似文献
55.
J. Kuriplach L. Lešták M. Rotter B. Sedlák M. Trhlík M. Finger T. Lešner J. Dupák P. Novák M. Vobecký 《Hyperfine Interactions》1987,34(1-4):339-342
First experimental results of160Tb nuclear orientation in yttrium single crystal matrix are described. The influence of external magnetic field in combination with the crystal field interaction is discussed. 相似文献
56.
In the framework of path integrals we present a solution to the Schrödinger equation for a free particle confined to the half-linex > 0. A solution in question corresponds to the boundary condition (/x) (0,t)= (0,t) where is a real constant. 相似文献
57.
58.
J. Brandštetr 《Journal of Thermal Analysis and Calorimetry》1981,21(2):357-365
A review of instruments for thermochemical (thermometric) solution analysis is given, including new types of isoperibol reaction of bomb calorimeters, the design of which can influence the future development of thermochemical measuring techniques. The new type of Dithermanal (Vaskut-EMG, Hungary, and Herrmann- Morris, France) controls the individual steps of the thermochemical analysis, adding memory and computing capabilities. Similar programming units with microprocessors for bomb and/or reaction calorimetry have been developed by Parr Comp. and Leco Comp. (USA). The latest modification of the Technicon flow analyzer permits on-line analysis of solid samples. For thermochemical titrations, the Sanda titrator (USA) and Vaskut automatic titrator (Hungary) are available. In the USA, the Tronac isothermal or isoperibol calorimeters are widely used. At the Technical University of Brno, ?SSR, smaller table instruments with a water-bath are applied for different modes of solution thermochemical analysis, and also for the reactions of solid samples in liquids. For the measurement of very small temperature differences, PTC thermistors are used. The possibilities of the future development of measuring techniques are outlined. 相似文献
59.
Unit cell parameters have been calculated from x-ray powder diffraction data of Mo2Br4
Py
4 (A), Mo2I4
Py
4 (B), Mo2I4
Pic
4 (C), Mo2(SCN)4
Py
4 (D) and Mo2(SCN)4
Pic
4 (E), A, B and C crystallize tetragonal. A witha=9,42,c=15,O2 Å; B witha=9,46,c=14,98 Å and C witha=9,66 andc=15,72 Å D and E crystallize orthorhombic. D witha=10,09,b=9,14,c=15,08 Å; E witha=10,22,b=9,41 andc=15,15 Å.Py=pyridine,Pic=4-methylpyridine. 相似文献
60.
A method for the determination of cadmium microamounts in mixtures with metallic ions withE
1/2 near toE
1/2 of cadmium is discussed. For higher selectivity cadmium was extracted in the form of the pyridin-thiocyanate complexes prior to polarography.
Bestimmung von Cadmium(II) neben anderen Metallionen
Zusammenfassung Es wird eine polarographische Methode zur Bestimmung von Cd(II) neben anderen Metallionen mitE 1/2 naheE 1/2(Cd) diskutiert. Zur Erhöhung der Selektivität und Genauigkeit wird eine Pyridin-Thiocyanat-Extraktion vorgeschalten.相似文献