Coprecipitation of Naphthol Azosulfonates with Organic Coprecipitants and Its Use in Flow-Injection Analysis

The coprecipitation of azo compounds based on 4-nitrophenyl- and 4-sulfophenyldiazonium naphthol sulfonates as their diphenylguanidinium ion-pair complexes with analogous compounds of naphthalene-2-sulfonic acid and 4-phenylsulfodiazonium is investigated. The optimization of the coprecipitation is considered based on the notions of the driving force of the cocrystallization of impurities. The optical characteristics of colored ion-pair complexes are measured. It is found that the water solubility is decreased most substantially for azosulfonates with hydrophobic nitro groups and with no more than two sulfo groups in different aromatic nuclei, which can lead to a decrease in the detection limit due to preconcentration by coprecipitation, which stimulates the thermodynamic flux of concentrate elution. Coprecipitation is combined with flow-injection analysis in the on-line mode, and new procedures are developed for determining naphthol sulfonates and related azo compounds with the detection limit equal to 0.003–0.006 mg/50 mL.     

光敏电阻基本特性测量实验的设计

介绍了测量CdS光敏电阻的伏安特性和光照特性的实验方法，并给出了相应的实验结果。     

Influence of Pretreatment of Expanded Graphite on Its Sorption Properties with Respect to Petroleum

Petroleum sorption on expanded graphite prepared from residual graphite hydrosulfate at 300-900°C was studied as influenced by pretreatment of the sorbent with water.     

岩盐型ZnO纳米微粒的光电子发射结构

报道了岩盐型氧化锌纳米微粒的X射线光电子发射结构,发现其中3d电子的强烈成键作用,还存在着3d-4sp杂化和离域电子弛豫态的贡献,表现出与纤锌矿型明显的差异. 关键词：     

Numerical simulation of achromatic deflecting systems

A deflecting system formed by two parallel-plate capacitors on opposite sides of an optoelectronic element that alters the energy of a beam of charged particles, is calculated numerically. The conditions for correcting the chromatic beam spreading in the plane of the target are found. Good agreement with the results of an approximate analytical calculation is demonstrated. Zh. Tekh. Fiz. 67, 86–88 (December 1997)     

Factorization of univalent analytic functions on compact Riemann surfaces with boundary

The paper is devoted to the theory of factorization of univalent analytic functions on a compact Riemann surface with boundary. The main component of the theory is a new method for the removal of the periods of certain functions (the natural analogues of the Schwarz integral and Blaschke products) along the boundary curves and bundle sections.Translated from Zapiski Nauchnykh Seminarov Leningradskogo Otdeleniya Matematicheskogo Instituta im. V. A. Steklova Akademii Nauk SSSR, Vol. 170, pp. 285–313, 1989.     

GRIF-1 experiment on board the SPEKTR/MIR orbital complex: Study of solar X-ray,gamma-ray,and neutron flares and correlation of magnetosphere-charged particle fluxes with solar activity

The SPEKTR module of the MIR orbital station was launched in May 1995. The multipurpose experiment was based on the GRIF-1 research complex consisting of an oriented X-ray spectrometer, a spectrometer of gamma-quanta and neutrons, a spectrometer of electrons and protons with a large geometrical factor, and a spectrometer of electrons, protons, and nuclei with a small geometrical factor. The solar geophysical aspects of the experiment included the measurements of spectral and temporal parameters of solar hard electromagnetic (0.01–50 MeV) and neutron (>20 MзB) radiation, the study of spectral, temporal, and spatial characteristics of energetic electrons (0.04–1.5 MeV), protons, and nuclei (1–200 MeV/nucleon) in the circumterrestrial space, as well as the correlations of these parameters with solar activity phenomena.     

Noncommutative four-dimensional subalgebras of conformal algebra integrable in the space R1,3

D'alambert's equation is used as an example to study the possibilities of a new method of exactly integrating systems of linear differential equations — the method of noncommutative integration (NI). The results confirm that use of the NI is equivalent to complete separation of the variables in the case of four-dimensional subalgebras of conformal algebra. However, the method does simplify determination of the exact solution in this instance.Tomsk University. Translated from Izvestiya Vysshikh Uchebnykh Zavedenii, Fizika, No. 2, pp. 120–124, February, 1995.     

重入自旋玻璃尖晶石系统CoxZn1-x(FeyCr1-y)2O4中的微波磁共振

研究了具有重入自旋玻璃转变的尖晶石系统Co_xZn_1-x(Fe_yCr_1-y)₂O₄(0.4≤x≤0.8,y=O.5,0.8)中的微波磁共振,获得了共振线型、共振线宽、共振场、g因子、积累强度等共振参数与温度的依赖关系,并研究了磁性离子Co²⁺的浓度对共振线宽的影响。采用自旋成团效应及局域混乱场模型讨论了这些实验现象的机制,认为在一定条件下自旋团的形成、发展 关键词：     

Estimates of electron-positron pair production in the interaction of high-power laser radiation with high-Z targets

Electron-positron production processes occurring in the interaction of 10¹⁸–10²⁰ W/cm² laser radiation with high-Z targets are examined. Computational results are presented for the pair production and the positron yield from the target with allowance for the contribution of pair production processes due to electrons and bremsstrahlung photons. Monte Carlo simulations using the PRIZMA code confirm the estimates obtained. The possible positron yield from high-Z targets irradiated with 10²–10³ TW laser radiation is estimated to be 10⁹–10¹¹. Pis’ma Zh. éksp. Teor. Fiz. 67, No. 4, 239–244 (25 February 1998)