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101.
102.
A convenient method is proposed for the synthesis of all the individual methyl ethers of methyl 2-acetamido-2-deoxy-α-D-glucopyranoside based on the partial methylation of 2-acetamido-2-deoxy-α-D-glucopyranoside with dimethyl sulfate in an alkaline medium followed by preparative liquid column chromatography on silica gel of the resulting mixture of methyl ethers. 相似文献
103.
104.
The main result of the paper is a theorem, using which a new proof of Roth’s theorem is obtained, a new solvability criterion
for the matrix equation AX-YB = C is proved, a formula for a particular solution of the latter is derived, and the least of
the orders of square nonsingular matrices containing a given rectangular matrix as a submatrix is determined. Bibliography:
5 titles.
__________
Translated from Zapiski Nauchnykh Seminarov POMI, Vol. 323, 2005, pp. 15–23. 相似文献
105.
Summary The main purpose of this paper is to introduce the concepts of η-sets, ηζ-sets,η-continuity and ηζ-continuity and to obtain
a decomposition of continuity. 相似文献
106.
The paper mentioned above is a contribution of the authors to Volume 18 (2002) of this journal, see . Recently, J. Domsta pointed out to us that the proof of Theorem 4.2 in that paper contains an error. The purpose of this
addendum is to present a correct argument for it. 相似文献
107.
Wolfram Bremser Roland Becker Heinrich Kipphardt Petra Lehnik-Habrink Ulrich Panne Antje Töpfer 《Accreditation and quality assurance》2006,11(10):489-495
ISO Guide 35 deals with RM stability issues and scrutinizes the evaluation of stability testing results under the assumption that either there is no trend at all (a rather rare situation), or any observed deterministic change is insignificant and thus can be neglected. However, market demands for reliable reference materials are obviously not limited to stable or at least seemingly stable materials. In many analytical applications, analytes and measurands under consideration are known, or at least suspected, to be unstable on time scales that may vary widely from measurand to measurand. The Federal Institute for Materials Research and Testing (BAM) has developed (and successfully uses) an integrated approach in its certification practice. The approach is based on an initial stability study and subsequent post-certification monitoring. Data evaluation is model-based and takes advantage of all information collected in the stability testing scheme(s). It thus allows one to deal with any kind of instability observed, to assess limiting time intervals at any stress condition in the range tested, to estimate a final expiry date for materials with detected instabilities or the maximum admissible re-testing interval for seemingly stable materials, and to assess maximum admissible stress loads during delivery of the material to the customer. The article describes (and exemplifies) typical study layout, the model selection, and the integrated data assessment. 相似文献
108.
Yu. I. Matveev 《Polymer Science Series A》2006,48(11):1185-1189
An expression for the ratio of the glass transition temperature to the melting temperature, T g/T m, was derived with allowance for fluctuations of the packing factor in the amorphous state. This relationship made it possible to describe the actual range of variation in T g/T m depending on a change in the packing factor in the crystalline state k o, cr. The proposed approach forms the basis for the method of determination of increments in the packing ratio k o, cr and formulation of the principles of selection of experimental data for calculations. The glass transition temperatures in polyethylene depending on the type of unit cell were calculated. 相似文献
109.
Zarubitskii O. G. Budnik V. G. Omel'chuk A. A. Melekhin V. T. Opanasyuk V. P. Zakharchenko N. F. 《Russian Journal of Applied Chemistry》2002,75(4):558-561
Electrochemical separation of lead-silver alloys into the constituents by thin-layer electrolysis in molten electrolytes, with bismuth as metal separator, is studied. It is proposed to determine the extent of component recovery by potentiometry. 相似文献
110.
Data Envelopment Analysis (DEA) offers a piece-wise linear approximation of the production frontier. The approximation tends to be poor if the true frontier is not concave, eg in case of economies of scale or of specialisation. To improve the flexibility of the DEA frontier and to gain in empirical fit, we propose to extend DEA towards a more general piece-wise quadratic approximation, called Quadratic Data Envelopment Analysis (QDEA). We show that QDEA gives statistically consistent estimates for all production frontiers with bounded Hessian eigenvalues. Our Monte-Carlo simulations suggest that QDEA can substantially improve efficiency estimation in finite samples relative to standard DEA models. 相似文献