首页 | 本学科首页   官方微博 | 高级检索  
文章检索
  按 检索   检索词:      
出版年份:   被引次数:   他引次数: 提示:输入*表示无穷大
  收费全文   32554篇
  免费   5164篇
  国内免费   4993篇
化学   24574篇
晶体学   422篇
力学   1643篇
综合类   328篇
数学   4027篇
物理学   11717篇
  2024年   126篇
  2023年   621篇
  2022年   1078篇
  2021年   1166篇
  2020年   1322篇
  2019年   1285篇
  2018年   1113篇
  2017年   1116篇
  2016年   1569篇
  2015年   1611篇
  2014年   1921篇
  2013年   2560篇
  2012年   2847篇
  2011年   3010篇
  2010年   2191篇
  2009年   1995篇
  2008年   2279篇
  2007年   2034篇
  2006年   1805篇
  2005年   1562篇
  2004年   1273篇
  2003年   1068篇
  2002年   1129篇
  2001年   928篇
  2000年   768篇
  1999年   687篇
  1998年   527篇
  1997年   437篇
  1996年   455篇
  1995年   405篇
  1994年   337篇
  1993年   240篇
  1992年   222篇
  1991年   216篇
  1990年   185篇
  1989年   118篇
  1988年   90篇
  1987年   74篇
  1986年   98篇
  1985年   70篇
  1984年   52篇
  1983年   41篇
  1982年   22篇
  1981年   17篇
  1980年   9篇
  1979年   6篇
  1976年   4篇
  1975年   4篇
  1973年   3篇
  1957年   5篇
排序方式: 共有10000条查询结果,搜索用时 8 毫秒
11.
李国亮 《数学杂志》2003,23(2):166-168
本文应用紧集上的连续函数是一致连续的性质,推广并证明了著名的Slutsky定理。  相似文献   
12.
13.
A low cost, coolerless 980nm diode pumped, gain flattened L band EDFA with fast transient control, high pump efficiency and gain clamping effect was realized by using FBGs as C band seed generators.  相似文献   
14.
Montmorillonite (MMT) was modified with the acidified cocamidopropyl betaine (CAB) and the resulting organo‐montmorillonite (O‐MMT) was dispersed in an epoxy/methyl tetrahydrophthalic anhydride system to form epoxy nanocomposites. The intercalation and exfoliation behavior of the epoxy nanocomposites were examined by X‐ray diffraction and transmission electron microscopy. The curing behavior and thermal property were investigated by in situ Fourier transform infrared spectroscopy and DSC, respectively. The results showed that MMT could be highly intercalated by acidified CAB, and O‐MMT could be easily dispersed in epoxy resin to form intercalated/exfoliated epoxy nanocomposites. When the O‐MMT loading was lower than 8 phr (relative to 100 phr resin), exfoliated nanocomposites were achieved. The glass‐transition temperatures (Tg's) of the exfoliated nanocomposite were 20 °C higher than that of the neat resin. At higher O‐MMT loading, partial exfoliation was achieved, and those samples possessed moderately higher Tg's as compared with the neat resin. O‐MMT showed an obviously catalytic nature toward the curing of epoxy resin. The curing rate of the epoxy compound increased with O‐MMT loading. © 2004 Wiley Periodicals, Inc. J Polym Sci Part B: Polym Phys 42: 1192–1198, 2004  相似文献   
15.
A Nafion-modified glassy carbon electrode incorporated with tobramycin for the voltammetric stripping determination of Cu2+ has been explored. The electrode was fabricated by tobramycin containing Nafion on the glassy carbon electrode surface. The modified electrode exhibited a significantly increased sensitivity and selectivity for Cu2+ compared with a bare glassy carbon electrode and the Nafion modified electrode. Cu2+ was accumulated in HAc-NaAc buffer (pH 4.6) at a potential of -0.6 V (vs. SCE) for 300 s and then determined by differential pulse anodic stripping voltammetry. The effects of various parameters, such as the mass of Nafion, the concentration of tobramycin, the pH of the medium, the accumulation potential, the accumulation time and the scan rate, were investigated. Under the optimum conditions, a linear calibration graph was obtained in the concentration range of 1.0 x 10(-9) to 5.0 x 10(-7) mol l(-1) with a correlation coefficient of 0.9971. The relative standard deviations for eight successive determinations were 4.3 and 2.9% for 1.0 x 10(-8) and 2.0 x 10(-7) mol l(-1) Cu2+, respectively. The detection limit (three times signal to noise) was 5.0 x 10(-10) mol l(-1). A study of interfering substances was also performed, and the method was applied to the direct determination of copper in water samples, and also in analytical reagent-grade salts with satisfactory results.  相似文献   
16.
Metabolites of A Novel Antibiotic Bitespiramycin in Rat Urine and Bile   总被引:3,自引:0,他引:3  
A sensitive analytical method to identify active metabolites of bitespiramycin in rat urine and bile was developed by liquid chromatography-electrospray ionization tandem mass spectrometry(LC/ESI-MS^n).Bitespiramycin and its major active metabolites in rat urine and bile were isolated and identified as M1 serial(spiramycin Ⅰ,Ⅱ,Ⅲ),M2 serial(platenomycin A1,josamycin and leucomycin A1) and M3 serial(deisovalerylplatenomycin A1,deisovaleryljosamycin,deisovalerylleucomycin A1).  相似文献   
17.
Baker‘s yeast mediated reduction of optically active diketone is described. The two keto groups are efficiently differentiated and the ee value of the recovered material is considerably raised. It affords highly optically active key intermediates efficiently for the synthesis of natural polyhydroxylated agarofuran products.  相似文献   
18.
The relation of the isoelectric point (IEP) and the point of zero net charge (PZNC) of the hydrotalcite-like compounds was discussed. It was found that the IEP does not equal to the PZNC and the IEP is higher than the PZNC. The structural positive charges existing in the HTlc,which cause the difference between the IEP and the PZNC. The effects of the structural positive charges of the HTlc on its IEP and PZNC are the same as the specific adsorption of metal cations.  相似文献   
19.
关于具有给定Sylow子群正规化子的有限群Ⅱ   总被引:1,自引:0,他引:1  
郭文彬 《数学学报》1996,39(4):509-513
本文在有限可解群中解决了:任意m-秩≤2的子群闭的局部群系具有性质:“如果群G的非单位Sylow子群的正规化子属于,则群G也属于的一个充分必要条件.  相似文献   
20.
The equivalent geometrical configurations of linear ordered orthogonal arrays are determined when their strengths are 3 and 4. Existence of such geometrical configurations is investigated. They are also useful in the study of (T, M, S)-nets.  相似文献   
设为首页 | 免责声明 | 关于勤云 | 加入收藏

Copyright©北京勤云科技发展有限公司  京ICP备09084417号