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排序方式: 共有10000条查询结果,搜索用时 13 毫秒
961.
Abakumov G. A. Druzhkov N. O. Kurskii Yu. A. Shavyrin A. S. 《Russian Chemical Bulletin》2003,52(3):712-717
Products of thermal transformation of substituted N-aryl-o-quinoneimines were studied using NMR spectroscopy. The formation of 4aH-phenoxazine, which was further dimerized by the Diels—Alder reaction, was established. 相似文献
962.
R W Milne R L Nation G D Reynolds A A Somogyi J T Van Crugten 《Journal of chromatography. A》1991,565(1-2):457-464
Improvements to previously reported methods for the determination of morphine, morphine-3-glucuronide (M3G) and morphine-6-glucuronide (M6G) in human plasma are described. The improved methods involve the use of a solid-phase extraction cartridge and a chromatographic system which uses paired-ion reversed-phase high-performance liquid chromatography with a radially compressed column. Only one cartridge is used to prepare each sample for chromatography and each cartridge may be used for at least fourteen 1-ml plasma samples. The recovery is greater than 85%. The improvements to the method of sample pretreatment and in the chromatographic conditions have allowed determination of morphine, M3G and M6G in human plasma down to 13.3 nmol/l (coefficient of variation = 9.3%), 108 nmol/l (6.6%) and 41 nmol/l (6.7%), respectively, using ultraviolet detection alone. It was shown that all three compounds were stable in plasma for up to 101 weeks when stored at -20 degrees C. 相似文献
963.
Per Sjölin 《Mathematische Zeitschrift》2007,256(2):265-278
Generalized conjugate partial Fourier integrals are used to find jumps of functions. The rate of convergence is studied and
sharp results are obtained. 相似文献
964.
This paper describes symmetries of all integrable difference equations that belong to the famous Adler–Bobenko–Suris classification. For each equation, the characteristics of symmetries satisfy a functional equation, which we solve by reducing it to a system of partial differential equations. In this way, all five-point symmetries of integrable equations on the quad-graph are found. These include mastersymmetries, which allow one to construct infinite hierarchies of local symmetries. We also demonstrate a connection between the symmetries of quad-graph equations and those of the corresponding Toda type difference equations. 相似文献
965.
966.
E. D. Aluker A. G. Krechetov A. Yu. Mitrofanov A. S. Pashpekin 《Russian Journal of Physical Chemistry B, Focus on Physics》2007,1(6):570-572
A new method for studying the kinetics of the expansion of explosion products based on measuring the time elapsed from explosion initiation to the short-circuiting of the discharge gap by the products was proposed. It was revealed that, at the initial stage of expansion of the silver azide explosion products, they move with uniform acceleration, a behavior suggestive that, during this period, the exothermic reaction 2N3 → 3N2 occurs. 相似文献
967.
968.
969.
The early evolution of gas chromatography in the former German Democratic Republic (GDR) is surveyed and instrument development is outlined, describing the most important models manufactured in the GDR. The organization of the Arbeitsgemeinschaft für Gas-Chromatographie (Working Group for GC) is chronicled and its activities are discussed. Subsequent parts of this article will deal with the six symposia organized by the Arbeitsgemeinschaft between 1958 and 1968. 相似文献
970.
In this paper we investigate the distribution of the Heisenberg evolution of the number operator in the stochastic limit of
the quantum electromagnetic field without dipole approximation. We prove that in this case the usual Poisson statistics of
the free fields has to be replaced by a hypergeometric series whose coefficients we compute explicitly. The physical effects
of the new statistics should manifest themselves in situation which are not yet in the relativistic regime, but in which the
dipole approximation is no longer valid.
The text was submitted by the authors in English. 相似文献