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71.
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V. Ye. Zaichick 《Fresenius' Journal of Analytical Chemistry》1995,352(1-2):219-223
The contents of 21 chemical elements (Ag, Br, Ca, Cl, Co, Cr, Cs, Fe, Hg, K, Mg, Mn, Na, P, Rb, Sb, Sc, Se, Sr, Zn, Zr) in synthetic reference materials (SRMs) were compared with those in natural reference materials (NRMs) using short- and long-lived radionuclides. SRMs called synthetic standards (SSs) and synthetic standards, biological (SSBs) were prepared on the basis of phenol-formaldehyde resol resins in the Institute of Physics, Georgian Academy of Science. The NRMs included such IAEA reference materials as H-4 (animal muscle), A-13 (animal blood), H-5 (animal bone), SL-1 (lake sediment), SOIL-7 (soil), A-9 (mixed human diet), and IAEA-153 (milk powder). It was shown that SSB-SRMs possessed good representativity of the 30–50 mg tablets, high precision, operational convenience, and could be recommended for the INAA of a wide range of medico-biological and bioecological objects. 相似文献
74.
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76.
B. Pignataro L. Chi S. Gao B. Anczykowski C. Niemeyer M. Adler H. Fuchs 《Applied Physics A: Materials Science & Processing》2002,74(3):447-452
Self-assembled oligomeric nanostructures consisting of bisbiotinylated DNA fragments connected by the protein streptavidin
(STV) are studied by dynamic scanning force microscopy (SFM) operating in air. A comparison of the images taken in repulsive
and attractive regimes is systematically made on DNA and STV structures. Stable and reproducible SFM images are obtained in
the attractive regime by using a special feedback circuit, called Q-control. On the other hand, when SFM is operating in the
repulsive regime, deformation of the structures that reduce the resolution and the image quality are clearly observable. The
heights of both DNA and STV have been measured as a function of the tip/molecule interaction forces. This study offers the
possibility to suggest a different mechanical behavior of DNA with respect to STV.
Received: 24 July 2001 / Accepted: 3 December 2001 / Published online: 4 March 2002 相似文献
77.
Since its discovery in 1946, NMR has become a valuable tool in physics, chemistry, biology, and medicine. With the invention of NMR logging tools that take the medical MRI or laboratory NMR equipment and turn it inside-out, the application of sophisticated laboratory techniques to determine formation properties in situ is now available. The capability has opened a new era in formation evaluation just as the introduction of NMR has revolutionized the other scientific areas. 相似文献
78.
J Z Hu R J Pugmire A M Orendt D M Grant C Ye 《Solid state nuclear magnetic resonance》1992,1(4):185-195
Taking advantage of the long 13C T1 values generally encountered in solids, selective saturation and inversion of more than one resonance in 13C CP/MAS experiments can be achieved by sequentially applying several DANTE pulse sequences centered at different transmitter frequency offsets. A new selective saturation pulse sequence is introduced composed of a series of 90 degrees DANTE sequences separated by interrupted decoupling periods during which the selected resonance is destroyed. Applications of this method, including the simplification of the measurement of the principal values of the 13C chemical shift tensor under slow MAS conditions, are described. The determination of the aromaticity of coal using a relatively slow MAS rate is also described. 相似文献
79.
本文通过对大量的黄酮类化合物13C NMR图谱的分析和研究,总结了不同类型的黄酮类化合物的13C NMR图谱特征及化学位移规律.对影响黄酮类化合物结构骨架上不同位置碳原子化学位移的因素进行了分析,建立了用于黄酮类天然产物13C NMR图谱智能解析的知识库. 相似文献
80.
YIN JIANXING 《高校应用数学学报(英文版)》1994,(4)
PACKINGPAIRSBYQUINTUPLES:THECASEOFZEROCONGRUENCEMOD4YINJIANXINGAbstract:LetD(v)denotethemaximumnumberofquintuplesofav-setofpo... 相似文献