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231.
232.
Klumpp DA Rendy R Zhang Y McElrea A Gomez A Dang H 《The Journal of organic chemistry》2004,69(23):8108-8110
A variety of aminoalkynes and related heterocycles are reacted in the Bronsted superacid CF(3)SO(3)H (triflic acid), and products are obtained in generally good yields (69-99%) from Friedel-Crafts-type reactions. The reactions are consistent with the formation of novel dicationic intermediates having a vinyl cationic site and an adjacent protonated N-heterocycle or ammonium cation. 相似文献
233.
Stereoselective synthesis of (Z)‐α‐(hydroxyalkyl)‐β‐iodoacrylates (=(2Z)‐2‐(hydroxyalkyl)‐3‐iodoprop‐2‐enoates) was achieved in a one‐pot coupling reaction from methyl prop‐2‐ynoate, Me3SiI, and an alkanal under mild conditions with MgI2 as catalyst (→ 1 – 9 ; see Table and Scheme 1). Baylis‐Hillman β‐iodo adducts were generated in excellent yields with high (Z)‐selectivity. The conversion of methyl prop‐2‐ynoate to an active methyl 3‐iodo‐1‐[(trimethylsilyl)oxy]allenolate intermediate in situ followed by carbonyl addition is proposed as the reaction sequence (Schemes 1 and 2). 相似文献
234.
Determination of Biodegradation Process of Benzene, Toluene, Ethylbenzene and Xylenes in Seabed Sediment by Purge and Trap Gas Chromatography 总被引:1,自引:0,他引:1
Benzene, toluene, ethylbenzene, and xylenes (BTEX) are commonly found in crude oil and are used in geochemical investigations as direct indicators of the presence of oil and gas. BTEX are easily volatile and can be degraded by microorganisms, which affect their precise measurement seriously. A method for determining the biodegradation process of BTEX in seabed sediment using dynamic headspace (purge and trap) gas chromatography with a photoionization detector (PID) was developed, which had a detection limit of 7.3–13.2 ng L?1 and a recovery rate of 91.6–95.0%. The decrease in the concentration of BTEX components was monitored in seabed sediment samples, which was caused by microorganism biodegradation. The results of BTEX biodegradation process were of great significance in the collection, transportation, preservation, and measurement of seabed sediment samples in the geochemical investigations of oil and gas. 相似文献
235.
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237.
本文利用多边形网格上的间断有限元方法离散二阶椭圆方程,在曲边区域上,采用多条直短边逼近曲边的以直代曲的策略,实现了高阶元在能量范数下的最优收敛.本文还将这一方法用于带曲边界面问题的求解,同样得到高阶元的最优收敛.此外我们还设计并分析了这一方法的\linebreakW-cycle和Variable V-cycle多重网格预条件方法,证明当光滑次数足够多时,多重网格预条件算法一致收敛.最后给出了数值算例,证实该算法的可行性并验证了理论分析的结果. 相似文献
238.
Numerical Algorithms - Iterative algorithms based on thresholding, feedback, and null space tuning (NST+HT+FB) for sparse signal recovery are exceedingly effective and efficient, particularly for... 相似文献
239.
Shutao Zhang & Yazhou Han 《分析论及其应用》2022,38(2):178-203
For conformal Hardy-Littlewood-Sobolev(HLS) inequalities [22] and reversed conformal HLS inequalities [8] on $\mathbb{S}^n,$ a new proof is given for the attainability
of their sharp constants. Classical methods used in [22] and [8] depends on rearrangement inequalities. Here, we use the subcritical approach to construct the extremal
sequence and circumvent the blow-up phenomenon by renormalization method. The
merit of the method is that it does not rely on rearrangement inequalities. 相似文献
240.
New Results on Generalized $c$-Distance Without Continuity in Cone $b$-Metric Spaces over Banach Algebras 下载免费PDF全文
Yan Han & Shaoyuan Xu 《分析论及其应用》2022,38(3):335-350
In this work, some new fixed point results for generalized Lipschitz mappings on generalized $c$-distance in cone $b$-metric spaces over Banach algebras are obtained, not acquiring the condition that the underlying cone should be normal or the
mappings should be continuous. Furthermore, the existence and the uniqueness of the
fixed point are proven for such mappings. These results greatly improve and generalize several well-known comparable results in the literature. Moreover, some examples
and an application are given to support our new results. 相似文献