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991.
The blends composed of polyamide 6 (PA6) and polyamide 66 (PA66) were obtained using two different preparation methods, one of which was the melt‐mixing through a twin‐screw extruder and the subsequent injection molding; and the other, the in situ blending through anionic polymerization of ε‐caprolactam in the presence of PA66. For the former, there existed a remarkable improvement in toughness but a drastic drop in strength and modulus; however, for the latter, a reverse but less significant trend of mechanical properties change appeared. Various characterizations were conducted, including the analyses of crystalline morphology, crystallographic form, and crystallization and melting behaviors using polarized optical microscopy (POM), wide‐angle X‐ray diffraction (WAXD), and differential scanning calorimetry (DSC), respectively; observation of morphology of fractured surface with scanning electron microscope (SEM); measurement of glass transition through dynamic mechanical analysis (DMA); and the intermolecular interaction as well as the interchange reaction between the two components by Fourier transform infrared spectrometry (FT‐IR) and 13C solution NMR. The presence and absence of interchange reaction was verified for the in situ and melt‐mixed blends, respectively. It is believed that the transreaction resulted in a drop in glass transition temperature (Tg) for the in situ blends, contrary to an increase of Tg with increasing PA66 content for the melt‐mixed ones. And the two kinds of fabrication methods led to significant differences in the crystallographic form, spherulite size and crystalline content and perfection as well. Accordingly, it is attempted to explain the reasons for the opposite trends of changes in the mechanical properties for these two blends. © 2007 Wiley Periodicals, Inc. J Polym Sci Part B: Polym Phys 45: 1176–1186, 2007 相似文献
992.
W. Brüggemann K. Fischer H. Jahnke 《Journal of Mathematical Modelling and Algorithms》2003,2(2):153-169
In Part I of this study, we suggest to identify an operations research (OR) problem with the equivalence class of models describing the problem and enhance the standard computer-science theory of computational complexity to be applicable to this situation of an often model-based OR context. The Discrete Lot-sizing and Scheduling Problem (DLSP) is analysed here in detail to demonstrate the difficulties which can arise if these aspects are neglected and to illustrate the new theoretical concept. In addition, a new minimal model is introduced for the DLSP which makes this problem eventually amenable to a rigorous analysis of its computational complexity. 相似文献
993.
994.
M. K. Richharia 《Pramana》2007,68(6):1007-1012
The cosmic ray (CR) intensity data recorded in Deep River Neutron Monitoring Station have been investigated on quietest days
(QD) for third harmonics of daily variation during solar cycles 21 and 22. It has been observed that in spite of abrupt change
in the amplitude and phase of tri-diurnal anisotropy in CR intensity, the amplitude is quite significant throughout the period
of investigation with larger amplitude during the years 1980 and 1985. Thus, tri-diurnal anisotropy clearly shows 11-year
variation at the mid latitude neutron monitoring station.
相似文献
995.
996.
Optical heterodyne magnetic rotation enhanced velocity modulation spectroscopy was employed to observe the visible absorption spectra of the B^2Σ^+_u-X^2Σ^+_g electronic transition of C^-_2. Four hot bands (0,1), (1,2), (2,3) and (3,4) have been observed and the band (3,4) is measured directly for the first time, so far as we know, by absorption. A rotational analysis was carried out to obtain molecular constants. With the Franck-Condon principle and the vibrational Boltzmann distribution, we have estimated the vibrational temperature of C^-_2 to be about 3000K. 相似文献
997.
998.
C. S. Creaser M. R. S. McCoustra K. E. O'Neill 《Journal of mass spectrometry : JMS》1991,26(4):335-338
Two fibre-optic interfaces were constructed for laser photodissociation/tandem mass spectrometry using an ion trap spectrometer. These interfaces allow sample introduction from a liquid reservoir, solids probe and gas chromatograph. The laser/ion trap configuration was applied to the analysis of a mixture of alkylbenenes separated by gas chromatography using 573 nm photons. 相似文献
999.
An initial boundary value problem for the dynamic system of anisotropic elasticity in a half space is studied in the paper. A novel method of finding an exact solution of this problem for a special polynomial form of initial data and inhomogeneous term of the system is described. On the base of this method the simulation of elastic waves in different homogeneous anisotropic half spaces is implemented. 相似文献
1000.
We obtain solutions of new extremal problems of the geometric theory of functions of a complex variable related to estimates
for the inner radii of nonoverlapping domains. Some known results are generalized to the case of open sets.
__________
Translated from Ukrains’kyi Matematychnyi Zhurnal, Vol. 59, No. 10, pp. 1313–1321, October, 2007. 相似文献