Synthesis of high purity single-walled carbon nanotubes in high yield

A simple method for the synthesis of high purity single wall carbon nanotubes has been developed by using nickel formate as a precursor for the formation of nearly mono-dispersed nickel seed-nanoparticles as catalysts in the CVD growth process.     

加速溶剂萃取-高效液相色谱法测定土壤中的亚当氏剂

加速溶剂萃取仪(ASE)提取土壤中亚当氏剂残留的最佳条件为:甲醇作提取剂,萃取温度90℃,压力为10689.7kPa(1550psi),样品经提取、浓缩后,以高效液相色谱测定含量.方法简便、快速,对土壤中亚当氏剂的回收率为81.2%～102.5%,相对偏差为5.4%,检出限为0.091mg/L.     

具有高稳定性以及光催化产氢活性的奇数环状异金属钛氧纳米团簇

利用太阳能是解决当前能源危机和环境问题的有效途径.二氧化钛是一种稳定性高、环境友好的新型光催化剂.近年来,具有精确结构信息的晶态钛氧团簇(PTCs)作为TiO2的分子结构模型受到广泛关注.目前大多数PTCs含有烷氧基,在空气中易发生水解.这在很大程度上限制了对其光催化性能的研究.在无机钛氧簇的外围修饰大量的共轭有机配体...     

Advances in Chip-Based Quantum Key Distribution

Quantum key distribution (QKD), guaranteed by the principles of quantum mechanics, is one of the most promising solutions for the future of secure communication. Integrated quantum photonics provides a stable, compact, and robust platform for the implementation of complex photonic circuits amenable to mass manufacture, and also allows for the generation, detection, and processing of quantum states of light at a growing system’s scale, functionality, and complexity. Integrated quantum photonics provides a compelling technology for the integration of QKD systems. In this review, we summarize the advances in integrated QKD systems, including integrated photon sources, detectors, and encoding and decoding components for QKD implements. Complete demonstrations of various QKD schemes based on integrated photonic chips are also discussed.     

Logical Entropy of Information Sources

In this paper, we present the concept of the logical entropy of order m, logical mutual information, and the logical entropy for information sources. We found upper and lower bounds for the logical entropy of a random variable by using convex functions. We show that the logical entropy of the joint distributions X1 and X2 is always less than the sum of the logical entropy of the variables X1 and X2. We define the logical Shannon entropy and logical metric permutation entropy to an information system and examine the properties of this kind of entropy. Finally, we examine the amount of the logical metric entropy and permutation logical entropy for maps.     

高效液相色谱与电感耦合等离子体质谱联用技术用于胁迫富硒海带硒形态研究

通过对海带胁迫富硒培养, 研究了海带对硒的富集总量及硒化学形态转变. 建立了反相离子对缓冲盐等3个色谱系统的高效液相色谱与电感耦合等离子体质谱联用(RP-HPLC-ICP-MS)技术测定亚硒酸钠、硒甲基半胱氨酸(MeSeCys)、硒代蛋氨酸(SeMet)三种硒形态. 采用3种提取溶剂, 超声提取缩短提取时间, 分离检测富硒海带的主要硒形态为亚硒酸钠、硒甲基半胱氨酸和硒代蛋氨酸.     

基于FPGA的储存环束流轨道联锁系统设计

上海光源储存环束流轨道联锁系统是加速器机器联锁保护系统(MPS)的重要组成部分,针对日常供光和机器研究的需求,需要对束流位置测量系统前各Libera电子学输出的联锁信号进行标记,以区分联锁信号的先后顺序和误报的联锁信号,同时触发所有Libera电子学前锁存逐圈（TBT）数据。新的联锁系统将所有联锁信号通过光纤传输汇总至FPGA数据采集板卡进行甄别,并将该系统集成储存环EPICS控制系统中。实验室测试显示该系统能够能够分辨数十ns范围内模拟的联锁信号,同时输出特定的触发信号至对应的Libera电子学,表明该系统达到设计要求。     

高功率激光装置的线性传输特性

在菲涅耳数的基础上重新定义了衍射特征量,并将其定义扩展至聚焦或发散光路,定义了一个光学系统中各光学元件衍射特征量的符号。通过全新的定义和扩展,研究了波前畸变对近场调制度的影响以及正弦调频光谱色散平滑光束衍射传输引入的幅频调制的大小。以神光-Ⅲ主机主放大级为例,研究了元件波前畸变对近场调制度的影响以及正弦调频光谱色散平滑光束衍射传输引入的幅频调制的大小。衍射特征量与能流分布F相结合,可以作为评价高功率激光装置线性传输效应的一项受限指标,指导高功率激光装置的设计。     

高功率光学元件校正波前的梯度均方根指标

对高功率固体激光装置中,光学元件波前经过变形镜校正后的梯度均方根指标开展了研究。建立了变形镜校正效果的等效分解方法,分析了校正波前的部分相干叠加特性,对校正波前的梯度均方根与焦斑尺寸的对应关系进行了研究。解决了在有变形镜校正时,如何制定元件波前梯度均方根指标的问题。研究结果对高功率固体激光装置的光学元件波前指标制定有指导意义。