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51.
Solid-phase extraction (SPE) is an effective tool for the preconcentration of trace elements and their separation from various sample constituents. Octadecyl and other alkyl-bonded silica gels are most widely used for these purposes. The fundamentals of the SPE of inorganic ions are reviewed and compared with those of related techniques (liquid-liquid extraction and reversed-phase liquid chromatography). The extraction of ions in the form of chelate compounds, inorganic salts solvated by neutral reagents, and ion-pair compounds is considered. Numerous applications of SPE to the separation and preconcentration of different elements and their species, including on-line combinations with instrumental determination techniques, are described and tabulated. 相似文献
52.
A simple and sensitive method was conducted for the determination of trace amounts of proteins with benzeneazo-8-acetylamino-1-naphthol-3,6-disulfonic acid sodium salt (azophloxine, AP) using a Rayleigh light-scattering (RLS) technique. At pH 2.60 and in the presence of an emulsifier OP microemulsion, the RLS of AP can be greatly enhanced by proteins, owing to the interaction between AP and protein. The enhanced intensity is proportional to the concentration of proteins. Four proteins, including bovine serum albumin (BSA), human serum albumin (HSA), lysozyme (Lys) and gamma globulin (gamma-G) have been tested. For example, the linear range of BSA was 0 - 0.06 microg mL(-1) with detection limits of 2.38 ng mL(-1). The method was applied to the analysis of protein in human urine and penicillin samples with satisfactory results. The relative standard deviation was in all instances less than 4.0%, and the recovery was in the range of 97.5 - 104%. 相似文献
53.
E. V. Gavryushin T. I. Gorbunova A. Ya. Zapevalov V. I. Saloutin 《Russian Journal of Applied Chemistry》2006,79(5):861-864
Wetting angles and limits of thermal stability of esters derived from pentaerythritol and perfluoro-, ω-chloropolyfluoro-, and perfluoropolyethercarboxylic acids were studied. 相似文献
54.
We study different moment characteristics of (mostly discrete) distributions: general, central, binomial, and factorial moments,
and also ordinary and factorial semi-invariants. We establish the relations that connect various kinds of “moments” of arbitrary
order, and we derive recursion formulas.
Translated fromMetody Matematicheskogo Modelirovaniya, pp. 34–41, 1998. 相似文献
55.
Experimental study of the stability of stiffened shells (review) 总被引:1,自引:0,他引:1
56.
Using the relations of the improved model of layered anisotropic shells based on the straight line assumption taking account of the thermal compression over the thickness we obtain a resolvent system of equations for shells whose properties depend on temperature. We carry out a study of the stresses in a two-layer cylindrical shell formed by winding as a function of the winding angle.
Translated fromMatematicheskie Metody i Fiziko-Mekhanicheskie Polya, Issue 35, 1992, pp. 82–85. 相似文献
57.
58.
Ya. L. Mordvinov 《Algebra and Logic》1993,32(3):154-164
Translated fromAlgebra i Logika, Vol. 32, No. 3, pp. 288–307, May–June, 1993. 相似文献
59.
I. Ya. Zabotin 《Journal of Mathematical Sciences》1995,74(5):1219-1224
Translated fromIssledovaniya po Prikladnoi Matematike, No. 19, 1992, pp. 24–33. 相似文献
60.
P. A. Bokhan T. Ya. Dubnishcheva D. E. Zakrevskii Yu. V. Nastaushev 《Journal of Russian Laser Research》1995,16(2):164-171
A gas-discharge gold-vapor laser on self-terminating transitions with operating wavelength λ=312.2 nm has been used to develop a highly efficient system for image transfer. An optical scheme and all its parameters have been chosen optimal for image quality. It has been found both theoretically and experimentally that the best results on micron-structure image transfer are obtained with 2–5-times image reduction. Various types of masks have been used. A 1-µm structure has been resolved due to the choice of optimal exposure time of 10 ms under a period of pulse repetition (0.6 – 0.8) ms; in this case, the minimal fringe dimension was ≈2 µm with an image dimension of 2 mm for a laser tube 1.8 cm in diameter. 相似文献