多尺度分析在激光微多普勒效应特征提取中的应用

由于小波变换具有准确度高、抗噪性好等优点,在微多普勒效应探测方面具有很好的应用前景。利用多尺度分析（MRA）将信号进行分解并提取出含有微多普勒效应的低频平滑信息,获取了目标微小振动引起的微多普勒效应。用频谱分析和基于瞬时频率(Instfreq)的时-频域联合分析方法对原始信号及通过MRA分解得到的结果进行了对比研究。结果表明：利用时-频分析对MRA处理后的低频信号进行分析,可更加有效地提取微多普勒效应中振动信号的特征,为目标特征的识别、分类和探测提供了便利。     

一种三环并联Rayleigh后向散射式光纤转动传感器

以单环后向Rayleigh散射式光纤转动传感器原理为基础,提出了一种三环形腔并联Rayleigh后向散射式光纤转动传感器新结构.利用三个2×2单模光纤耦合器,建立了并联三环形腔Rayleigh后向散射式光纤转动传感器的理论模型,给出了用光时域反射计（OTDR）探测到的信号强度表达式.通过计算机仿真优化了参量,选择三环的长度分别为1 500 m、1 078 m和680 m.三个2×2光纤耦合器的耦合系数分别为95.23%、94.88%和95.26%构建了测试系统,对不同转速所探测到的后向Rayleigh散射信号进行测量,得到与理论相一致的实验结果.三环的采用,增加了测试的有效数据,使其更有利于识别,提高了测量转速的准确度.     

顶空气相色谱法同时测定水中甲醇及苯

顶空气相色谱同时测定水中甲醇及苯含量,方法简单、快速,不需要专门的FFPA色谱柱.甲醇检出限0.01mg/mL,苯检出限0.01μg/mL.     

Nanostructured BiVO4 Derived from Bi-MOF for Enhanced Visible-light Photodegradation

BiVO4,a promising visible-light responding photocatalyst,has aroused extensive research interest because of inexpensiveness and excellent chemical stability.However,its main drawback is the poor photoinduced charge-transfer dynamics.Building nanostructures is an effective way to tackle this problem.Herein,we put forward a new method to prepare nanostructured BiVO4 from Bi-based metal-organic frameworks[Bi-MOF(CAU-17)]precursor.The as-prepared material has a rod-like morphology inherited from the Bi-MOF sacrificial template and consists of small nanoparticle as building blocks.Compared with its counterparts prepared by conventional methods,MOF-derived nanostructured BiVO4 shows better light absorption ability,narrower bandgap,and improved electrical conductivity as well as reduced recombination.Consequently,BiVO4 nanostructure demonstrates high photocatalytic activity under visible light towards the degradation of methylene blue.Methylene blue can be degraded up to 90%within 30 min with a reaction rate constant of 0.058 min-1.Moreover,the cycling stability of the catalyst is excellent to withstand unchanged degradation efficiency for at least 5 cycles.     

Effect of Support on Catalytic Performance of Photothermal Fischer-Tropsch Synthesis to Produce Lower Olefins over Fe5C2-based Catalysts

Photothermal Fischer-Tropsch synthesis(FTS) has been extensively studied, but few reports were focused on systematically exploring the influence of support on catalytic performance. Herein, a series of Fe₅C₂-based catalysts with different supports was fabricated via a one-step wet-chemical method for photothermal conversion of syngas to lower olefins. Under light irradiation, the optimized Fe₅C₂/α-Al₂O₃ catalyst demonstrated remarkable photothermal FTS activity, delivering selectivity to lower olefins of 50.3% with a CO conversion rate of 52.5%. Characterization studies using X-ray diffraction and Mössbauer spectroscopy analysis revealed that the active catalyst mainly contained Fe₅C₂ nanoparticles on α-Al₂O₃ support. It was found that the weak interaction between active phase and α-Al₂O₃ could promote the formation of Fe₅C₂, which contributed to the high selectivity to lower olefins.     

J正交矩阵的一些性质

给出了J正交矩阵的一些性质．     

Intrinsic square function characterizations of Hardy spaces associated with ball quasi-Banach function spaces

Let X be a ball quasi-Banach function space satisfying some mild additional assumptions and H_X({ℝ}^n) the associated Hardy-type space. In this article, we first establish the finite atomic characterization of H_X({ℝ}^n). As an application, we prove that the dual space of H_X({ℝ}^n) is the Campanato space associated with X. For any given \alpha \in (\mathrm{0},\mathrm{1}] and s\in {\mathbb{Z}}_{+}, using the atomic and the Littlewood–Paley function characterizations of H_X({ℝ}^n),we also establish its s-order intrinsic square function characterizations, respectively, in terms of the intrinsic Lusin-area function S_{\alpha ,s},the intrinsic g-function g_{\alpha ,s},and the intrinsic g_{\lambda }^{\ast }-function g_{\lambda ,\alpha ,s}^{\ast }, where λ coincides with the best known range.     

高效液相色谱-荧光检测器法测定2-噁唑烷酮的含量

建立一种利用高效液相色谱结合荧光检测器准确测定2-噁唑烷酮含量的方法。样品中的2-噁唑烷酮和占吨氢醇在60℃的条件下衍生70 min后,直接进样分析。采用月旭XB-C18色谱柱,流动相为0.02 mol/L乙酸钠水溶液和乙腈,检测器波长为λex=213 nm,λem=308 nm,流速1.0 mL/min,柱温35℃的条件下。2-噁唑烷酮浓度在0.5~50.0mg/mL时,线性关系良好(R2=0.9995),检测限和定量限分别为0.005 mg/L、0.016 mg/L。该方法准确、灵敏、快速,适用于2-噁唑烷酮含量的检测。     

Global strong solution of 3D tropical climate model with damping

We establish the global well-posedness of a strong solution to the 3D tropical climate model with damping. We prove that there exists the global and unique solution for α, β, γ satisfying one of the following three conditions: (1) \alpha ,\beta \ge \mathrm{4}; (2) ; (3) .