尿素和尿素—Fe配位化合物的晶格振动光谱研究

采用直接固相反应将尿素与氯化铁(摩尔比6∶1)混合,经充分研磨合成了尿素铁盐配位化合物,并对其拉曼光谱和红外吸收光谱进行了研究。由于金属原子的影响,尿素分子的一些特征振动频率发生了变化:CO伸缩振动和NH2的对称弯曲振动的频率下降;而CN伸缩振动和NH2反对称弯曲振动的频率增加。对尿素以及尿素—Fe(III)的晶格振动模进行了识别。研究结果表明:Fe与尿素中的氧原子发生了配合而形成配位物。     

Novel Bone-targeted Agents for Treatment of Osteoporosis

The novel bone-targeted agents were designed and synthesized by the combination of raloxifene and bisphosphonates. The anti-osteoporosis effect was evaluated by bone mineral density (BMD) obtained from OVX mice in vivo. The results indicated that the compound 8, 9 not only prevented ovariectomy induced loss of bone but also enhanced BMD to 0.87% and 19.67% compared to Sham, respectively.     

带脉冲的EmdenFowler方程次线性奇异边值问题的正解

该文讨论了带脉冲的Emden Fowler方程次线性奇异Dirichlet边值问题,利用上下解方法得到了该类问题正解存在的充分必要条件. 在脉冲的影响下得到了多解的存在性结果。     

DSC and NMR Study on the Inclusion Complex of Lappaconitine with b-Cyclodextrin

Lappaconitine (Figure 1) is a diterpenoid alkaloid, naturally occurring in roots and rhizomes of Aconitum and delphinium1. Lap reveals bradycardic and hypotensive activity2. But its application is restrained owing to its poor water solubility, toxicity and side effects on humans. In a number of pharmaceutical studies, b-CD has been reported to interact with many drug molecules to form inclusion complexes for improving the water solubility of drugs, and reducing their toxicity3. We have p…     

Regional characteristics of ultrasonic structural scattering in liver

I.IntroductionInrecentyears,manyhomeandabroadscholarshavedoneagreatdealofstudiesontissuecharacterizationusingacousticparametersincludingultrasonicattenuationcoefficient,scatteringcoefficiellt,andnonlinearparameterB/Aofbiologicaltissue.Theseresearcheshavelearntmuchknowledgeoftheacousticpropertiesofsofttissue.Butbecauseofthedifferenceinresearchmethodsandtestingconditions,thediscrepa-nceofmeasuredresultsisstilllargeandnosteadycharacterizationmodelcanbeformed-Atthesametime,thestudyofrevealingthe…     

结肠癌病人几种细胞的Raman光谱

文章给出了结肠癌病人的几种细胞的拉曼光谱。从实验谱线中得到,均有构像不灵敏的苯丙氨酸的单取代苯环的伸缩振动谱线1002cm~(-1),谱线强而半高宽较小,且不易改变,可作为生物细胞拉曼谱线的内标。白细胞拉曼谱线弱而少,红细胞拉曼谱线强而丰富,且有一个吡咯环的C—N呼吸振动谱带,窄而强的1919cm~(-1)的特征峰,宽而强的谱线1577,1560,1548cm~(-1),这是其他细胞不具有的。腺癌细胞的拉曼谱线相对较弱,许多谱线消失,生长在不同部位癌变细胞的荧光强度分布不同。通过这些特征拉曼谱线的不同,为癌症的诊断和治疗提供了有力的实验依据。     

关于自旋变相过程的耦合问题

本文给出了自旋变相过程耦合最优和保序的充分必要条件，同时研究了基本耦合的这些性质．     

Brusselator方程解的存在性和稳定性

本文研究了一种Brusselator方程的。用不变区域证明了解的全局存在性，并通过构造上下解给出了非常数定态解渐进稳定的条件。最后推出吸引域。     

Theoretical study of adsorption of water vapor on surface of metallic uranium

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星可数网和局部S可数网

The concept of local s-countablity is introduced, and the relations between locally s-countable collections and star-countable collections are discussed.