Influence of Pretreatment of Expanded Graphite on Its Sorption Properties with Respect to Petroleum

Petroleum sorption on expanded graphite prepared from residual graphite hydrosulfate at 300-900°C was studied as influenced by pretreatment of the sorbent with water.     

Use of reference materials in coastal monitoring quality assurance

The NOAA National Status and Trends (NS&T) Program determines the current status of, and changes over time in the environmental health of U.S estuarine and coastal waters. Concentrations of organic and inorganic contaminants are determined in bivalves, bottom-dwelling fish and sediments. The quality of the analytical data generated by the NS&T Program is over-seen by the performance-based Quality Assurance Project, which is designed to document sampling protocols, analytical procedures, and laboratory performance, and to reduce intralaboratory and interlaboratory variation. All NS&T cooperating laboratories are required to participate in yearly intercomparison exercises. The analysis of reference materials, such as the National Research Council of Canada's Certified Reference Materials (CRMs) and National Institute of Standards and Technology's (NIST) Standard Reference Materials (SRMs), and of control materials, is required. Because of the need for marine matrix reference materials and standards, NOAA contributed to the production of eight NIST SRMs and seven internal standard solutions. Analytical data from all control materials and all matrix reference materials are reported to the Program office.     

Numerical simulation of achromatic deflecting systems

A deflecting system formed by two parallel-plate capacitors on opposite sides of an optoelectronic element that alters the energy of a beam of charged particles, is calculated numerically. The conditions for correcting the chromatic beam spreading in the plane of the target are found. Good agreement with the results of an approximate analytical calculation is demonstrated. Zh. Tekh. Fiz. 67, 86–88 (December 1997)     

Factorization of univalent analytic functions on compact Riemann surfaces with boundary

The paper is devoted to the theory of factorization of univalent analytic functions on a compact Riemann surface with boundary. The main component of the theory is a new method for the removal of the periods of certain functions (the natural analogues of the Schwarz integral and Blaschke products) along the boundary curves and bundle sections.Translated from Zapiski Nauchnykh Seminarov Leningradskogo Otdeleniya Matematicheskogo Instituta im. V. A. Steklova Akademii Nauk SSSR, Vol. 170, pp. 285–313, 1989.     

Decomposition methods: A new proof of convergence

We propose a new convergence proof of Adomian's technique based on properties of convergent series. Then we deduce some results about the speed of convergence of this method allowing us to solve nonlinear functional equations.     

Noncommutative four-dimensional subalgebras of conformal algebra integrable in the space R1,3

D'alambert's equation is used as an example to study the possibilities of a new method of exactly integrating systems of linear differential equations — the method of noncommutative integration (NI). The results confirm that use of the NI is equivalent to complete separation of the variables in the case of four-dimensional subalgebras of conformal algebra. However, the method does simplify determination of the exact solution in this instance.Tomsk University. Translated from Izvestiya Vysshikh Uchebnykh Zavedenii, Fizika, No. 2, pp. 120–124, February, 1995.     

Cellulose-polyamide 66 blends. Part II: Mechanical behavior

Blends of the natural polymer cellulose with a synthetic polymer, polyamide 66, are studied in order to determine if the expected strong interaction between them, due to hydrogen bonds, could improve their mechanical properties such as strength and elongation at break. In a previous work {Part I, J. Polym. Sci. Polym. Phys., 32 , 1437 (1994)}, the preparation technique and the characterization of cellulose-polyamide 66 (PA66) blends were described in detail. Several samples in the composition range between 0 to 70 wt % of PA66 were carefully dried and examined using dynamic mechanical and tensile tests. Based on previous work a new percolation model has been developed. It takes both linear and nonlinear mechanical behaviors into account and allows for the effect of adhesion between material domains. From comparison between experimental and predicted data, it is concluded that a partial miscibility between the amorphous phases of cellulose and PA66 exists and is responsible for a strong adhesion at their interface. Solid-state ¹³C nuclear magnetic resonance has also been used to study these samples and supports the existence of strong interactions between both homopolymers. © 1995 John Wiley & Sons, Inc.     

Role of Na(+)-Ca2+ exchange system in the pathogenesis of myocardial ischemia-reperfusion damage

Results from a systematic experiment on isolated perfused rat heart and isolated myocytes of adult rat showed that the mechanism of calcium influx during myocardial ischemia-reperfusion is due to the development of intracellular sodium overload during ischemic period; on reperfusion, the high intracellular Na+ content activated the reverse direction of Na(+)-Ca2+ exchange over myocardial sarcolemma (SL), thus a large quantity of extracellular Ca2+ fluxed over the SL to the intracellular space, forming a condition of intracellular Ca2+ overload, which leads to irreversible damage of the myocardium.     

Microdetermination of hyaluronic acid in human urine by high performance liquid chromatography.

A high performance liquid chromatographic (HPLC) system is described for determination of the unsaturated disaccharide (delta Di-HA) derived from hyaluronic acid (HA) in human urine by digestion with hyaluronidase SD. The effects of eluents on the separation of delta Di-HA and delta Di-0S, which is derived from the reaction of chondroitin with the enzyme, have been studied. The established chromatographic conditions were as follows--column: a stainless steel tube (4 mm i.d. x 250 mm) packed with TSKgel NH2-60; eluent: a mixture of acetonitrile and 0.1 M Tris-HCl buffer containing 0.1 M boric acid and 10 mM sodium sulphate, pH 7.0 (64:36, v/v). The strong fluorescence of unsaturated disaccharide after the reaction with 2-cyanoacetamide in alkaline medium was used for post-column detection. The calibration curve for delta Di-HA was linear in the range 5 pmol-5nmol with a practical detection limit of 2 pmol. The assay coefficients of variation (n = 5) at 200 pmol for delta Di-HA and delta Di-0S were 1.7 and 1.5%, respectively. This HPLC system has been applied to the determination of HA in human urine.