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91.
Forsythia suspensa (Thunb.) Vahl is one of the most widely used traditional Chinese medicines, and possesses important biological activities, such as antibacterial, antiviral, anti-inflammatory and antioxidant activities. Phillyrin is the main bioactive component of Forsythia suspensa. In this paper, ultrasound-assisted extraction of phillyrin from Forsythia suspensa was studied with HPLC-photodiode array detection. Effects of several experimental parameters, such as type and concentration of extracting solvent, ratio of liquid to material, extraction temperature, and time of sonication on extraction efficiencies of phillyrin from Forsythia suspensa were evaluated. The optimal extraction conditions were 1g plant sample with 10 ml of 20% methanol and the extraction for 60 min at 60°C under ultrasonic irradiation. Under the optimum conditions, the yield of phillyrin was 0.713±0.009 mg/g. The results indicated that the ultrasound-assisted extraction is a very useful method for the extraction of important phytochemicals from plant materials. 相似文献
92.
(Na0.5K0.5)0.975Li0.025Nb0.82−xSbxTa0.18O3 lead-free piezoceramics were prepared by the conventional solid-state sintering method. All samples possess a pure perovskite phase, and no secondary phase could be certified. The crystal structure changes from tetragonal to pseudo-cubic with increasing amount of Sb. The ferroelectric Curie temperature (Tc) shifts to lower temperature while the tetragonal to orthorhombic phase transition temperature (To-t) shows no obvious change with increasing Sb5+. Enhanced piezoelectric and electromechanical properties are obtained with x=0.06: d33=352 pC/N, kp=47% and kt=38%, showing that they could be promising candidates as lead-free piezoelectric materials. 相似文献
93.
Qinqin Liu Juan YangXiaonong Cheng Xiujuan SunChuanliang Zang 《Physica B: Condensed Matter》2011,406(18):3458-3464
ZrW2O8 displays the unusual property of an isotropic bulk contraction in volume as a function of temperature. We report here on the positive thermal expansion (PTE) property caused by substituting Mo for W sites in ZrW2O8 at room temperature. The room temperature crystal structure of ZrW2−xMoxO8 compounds, which were synthesized using a low temperature route, could be divided into ordered phase with α-ZrW2O8 structure (0≤x≤0.5) and disordered phase with β-ZrW2O8 (0.5<x≤1.5) and c-ZrMo2O8 structure (1.5<x≤2). ZrW2−xMoxO8 adopting β-ZrW2O8 structure shows abnormal PTE property at room temperature due to the existence of water molecules, while ZrW2−xMoxO8 adopting the other two structures (α-ZrW2O8 and c-ZrMo2O8) shows negative thermal expansion (NTE) property from room temperature until decomposition for α-ZrW2O8 structure or trigonal phase transition for c-ZrMo2O8 structure. The reason lies in the fact that the oxygen migration caused by the Mo substitution leads to the re-arrangement of W(Mo)O4 tetrahedra lying along the 3-fold axis, only particular W/Mo ratio (0.5<x≤1.5) produces a special crystal structure, which allows the entrance of water molecules. 相似文献
94.
以超混沌Chen系统和超混沌Lorenz系统为例,研究了慢时变参数超混沌系统的反同步问题.首先利用主动控制的思想,消去超混沌系统中的非线性部分,然后基于Lyapunov稳定性理论,合理地选取参数自适应控制律,很好的解决了时变参数的参数摄动问题,从而实现了两个超混沌系统的反同步.在此基础之上,又进一步研究了分数阶超混沌系统,使用滑模控制方法对其进行控制,理论上分析了该方法的可行性.数值模拟实验进一步验证了所提出方法的有效性.
关键词:
超混沌
分数阶
自适应
滑模 相似文献
95.
We present a extended-cavity diode laser (ECDL) with kilohertz linewidth by optical feedback from a monolithic folded Fabry-Perot cavity (MFC). In our experiments, an MFC replaces the retroreflecting mirror in the traditional ECDL configuration. Beat-note measurements between this MFC-ECDL and a narrow-linewidth reference laser are performed and demonstrate that the linewidth of this MFC-ECDL is about 6.8 kHz. Phase locking of this MFC-ECDL to the reference laser is achieved with a unity gain as small as 10.2 kHz. 相似文献
96.
97.
In this paper, we investigate the temporally discrete reaction-diffusion with delay. By using Schauder’s fixed point theorem, we establish the existence of traveling wave fronts. The main result is applied to a delayed and discretely diffusive model for the population of Daphnia magna. 相似文献
98.
99.
A novel design for a highly efficient 1-kHz single-frequency green laser is proposed.An efficient singlefrequency laser pulse output at 532-nm wavelength may be obtained by combining the injection seeding with intracavity frequency doubling in a compact U-shaped cavity formed by two plano dichroic mirrors in an end-pumping arrangement.The laser is capable of producing green pulses with a total energy of 6.3 mJ at a pulse repetition rate of 1 kHz.The pulse width is about 10 ns and the optical-optical efficiency from the 808-nm pump source to the 532-nm green output is around 12.7%. 相似文献
100.