脑细胞激活素药物的化学成分分析

采用日本岛津LC-60A型高压液相色谱仪和美国P-E3030型原子吸收分光光度计，对该药进行了氨基酸、维生素和化学元素的含量测定。结果表明，该药含有18种氨基酸，不少于3种维生素和20几种化学元素，为进一步改进该药物的合理配制方法和临床应用提供了参考数据。     

橙皮素A的NMR研究

橙皮素A是从中药北沙参(Glehnia littoralis Fr. Schmidt ex Miquel)的正丁醇萃 取物中分离得到的一种8-O-4′-型异木脂素苷类化合物. 通过化学方法和波谱分析鉴 定了该 化合物的结构. 采用2D NMR技术对其NMR信号进行了全归属. DMSO-d₆代替CD₃OD作为溶剂，并利用重水交换，能准确读出偶合常数J_7,8值.      

用峰面积判据改善Delsuc法预测的谱

基于Prony算法的Delsuc谱预测是目前NMR LPSVD(Linear Prediction SingularValue Decomposition)法中比较实用的方法。但在高噪声的条件下,时有失峰和假峰出现且要事先知道谱的峰数。本文通过跟踪迭代过程发现Delsuc法的判别因子r_(mis) 很难选定。如果它太小会失峰,而过大又会出现假峰。同时,由于噪声的影响,弱信号的采样点之间的相关性比强信号小,从而在迭代过程中会增加数值不稳定性。文中引入峰面积判据来改善Delsuc法,经模拟与实验均证明结果有效。     

表面粗糙度测量的磁光位相调制和锁相干涉

提出了一种表面粗糙度测量的新方法，该方法采用了微分偏振干涉的原理，利用由法拉第磁光调制器所组成的调制系统对偏振干涉光路的位相进行调制，利用锁相干涉原理对位相进行探测，该方法可实现无参考面快速非接触测量，在普通实验条件下，也可保持良好的稳定恶性循环 ，实验装置即可给出表面的轮廓又可给出其它统计数据，其横向分辨率为１．２μｍ纵向为２ｎｍ。     

The prediction of the peak width at half height in HPLC

The prediction of the peak width at half height is an important aspect in the optimization of the chromatographic operating conditions. In this paper, a linear relationship, between the peak widths at half height and the retention values with various isocratic elution is observed. In gradient elution, however, the relationship between the peak widths at half height and the so-called invented retention values that correspond to the mobile phase composition by eluting the solute from the column end is developed. We believe that there is almost the same band width at half height inside the column (in unit of length) for different solutes. The peak width at half height in the chromatogram (in unit of time) is mainly determined by the capacity factor of the solute when it is eluted from the column end. The larger the capacity factor of a solute eluted from the column end, the more slowly will be the solute eluted from the column end and the wider will be the peak width at half height. It is possible to predict the peak width at half height in various isocratic and gradient elutions by using this linear relationship.     

在CPM非稳腔Nd:YAG激光器中用被—被动锁模方法选单脉冲的探讨

在CPM Nd:YAG非稳腔激光器中,我们使用透过率较大的可饱和吸收体使单脉冲序列中的脉冲个数减少到3—5个,在输出的单序列中再使用非线性介质进行处理,可以得到比较接近的单脉冲输出。     

一种适于自适应光学的旋转软刀口波面传感器的研究

利用傅里叶光学理论,证明了一种新型波面传感器——旋转软刀口波面传感器的概念.在经典刀口法的刀口区,以渐变透过率代替突变透过率函数,在光瞳象面上可获得反映光瞳面位置待测波面位相梯度及位相梯度方向的调制信号.文中给出了实验结果和讨论.     

应用加权列联表分析预测汛期（4─9月）洪涝趋势

本文根据汉寿县１９６０─１９８８年洪涝灾害资料，应用加权列联表分析法，与前期气候因子建立洪涝趋势预测模式。最后对１９８９─１９９０年洪涝试报，取得了满意的效果。     

Differential determination of arsenic(III) and total arsenic using flow injection on-line separation and preconcentration for graphite furnace atomic absorption spectrometry

Arsenic(III) can be quantitatively extracted using sodium diethyldithiocarbamate (NaDDTC) as the complexing agent and C18 reversed phase packing as the column material for solid phase extraction. Arsenic(V) must be reduced to its trivalent oxidation state prior to extraction. A mixture of sodium sulphite, hydrochloric acid, sodium thiosulphate and potassium iodide was found to be optimum for on-line reduction. When the sorbent extraction is carried out without and with the addition of the reduction mixture, arsenic(III) and total arsenic can be determined sequentially by graphite furnace atomic absorption spectrometry with detection limits (3 σ) of 0.32 ng for As(III) and 0.43 ng for total arsenic. A 7.6-fold enhancement in peak area compared to direct injection of 40 μl samples was obtained after 60 s preconcentration. Results obtained for sea water standard reference materials, using aqueous standards for calibration, agree well with certified values. A precision of 5.5% RSD was obtained for total arsenic in a sea water sample (1.65 As). Results obtained for synthetic mixtures of trivalent and pentavalent arsenic agreed well with expected values.     

Multi-cracks problem for piezoelectric materials strip subjected to dynamic loading

This paper analyses and models the dynamic interaction among permeable multi-cracks in a piezoelectric strip under anti-plane shear waves by the Schmidt method. The Fourier transform is applied and then two pairs of triple integral equations can be solved using the Schmidt method. The results show that the stress and the electric displacement intensity factors of cracks depend on not only the crack length and the piezoelectric coefficient, but also the thickness of the piezoelectric strip, the distance between multi-cracks and the frequency of incident wave.