全文获取类型
收费全文 | 154698篇 |
免费 | 17188篇 |
国内免费 | 9504篇 |
专业分类
化学 | 91013篇 |
晶体学 | 1951篇 |
力学 | 9441篇 |
综合类 | 523篇 |
数学 | 15648篇 |
物理学 | 62814篇 |
出版年
2023年 | 2171篇 |
2022年 | 3833篇 |
2021年 | 4068篇 |
2020年 | 4379篇 |
2019年 | 3959篇 |
2018年 | 3821篇 |
2017年 | 3396篇 |
2016年 | 5539篇 |
2015年 | 5047篇 |
2014年 | 6378篇 |
2013年 | 9495篇 |
2012年 | 10700篇 |
2011年 | 11603篇 |
2010年 | 7839篇 |
2009年 | 7670篇 |
2008年 | 8718篇 |
2007年 | 7890篇 |
2006年 | 7569篇 |
2005年 | 6245篇 |
2004年 | 5165篇 |
2003年 | 4260篇 |
2002年 | 3975篇 |
2001年 | 5192篇 |
2000年 | 3974篇 |
1999年 | 3581篇 |
1998年 | 2796篇 |
1997年 | 2770篇 |
1996年 | 2572篇 |
1995年 | 2220篇 |
1994年 | 1977篇 |
1993年 | 1710篇 |
1992年 | 1896篇 |
1991年 | 1815篇 |
1990年 | 1579篇 |
1989年 | 1317篇 |
1988年 | 1156篇 |
1987年 | 1157篇 |
1986年 | 1038篇 |
1985年 | 1211篇 |
1984年 | 1023篇 |
1983年 | 718篇 |
1982年 | 680篇 |
1981年 | 613篇 |
1980年 | 554篇 |
1979年 | 651篇 |
1978年 | 667篇 |
1977年 | 676篇 |
1976年 | 597篇 |
1975年 | 507篇 |
1974年 | 542篇 |
排序方式: 共有10000条查询结果,搜索用时 15 毫秒
51.
For the linear deterministic system with unknown orders and coefficients adaptive controls are given so that the closed-loop system is stabilized and the unknown parameters are consistently estimated. Moreover, if the parameter estimation is ignored, then the system input and output can be reduced to zero with an exponential rate.This project is supported by the National Natural Science Foundation of China.In Commemoration of the 15th Anniversary of the Acta Mathematicae Applicatae Sinica. 相似文献
52.
本文报道了用吸附溶出伏安法测定毗喳酮.以悬汞电极为工作电极,在Na}B,O,-NaOH介质(pH=10)中,毗喳酮产生一尖锐的吸附还原峰,E,二一1. 29V (vs. SCE ),峰电流与毗喳酮浓度在2. 0 X 10-'-8. 0 X 10-smol " L-’范围内呈良好的线性关系.检测限为2. 0 X 10-0mol " L-'(富集90s).本文对毗喳酮在悬汞电极上的电化学行为进行了探讨,对测定毗喳酮的最佳条件进行了详细的选择,利用本法测定了片剂中毗喳酮含量,结果满意. 相似文献
53.
Experiments for the determination of mono-, di and tri-butyltin (MBT, DBT and TBT) by hydride generation/gas chromatography/atomic absorption spectrometry in various matrices (sediment, suspended matter, mussel, algae and water) have revealed that poor butyltin recoveries are obtained in sediments displaying high sulphur and hydrocarbon contents; very poor recoveries were also observed for TBT in sediments with high chlorophyll pigment contents as well as in algal samples. It was however not clear whether the hydride generatin was inhibited by these infering compounds, as was previously assumed in the case of hydrocarbons, or whether interferences affected the atomization rate. Further studies were performed to solve this problem in order to validate this method in the case of analyses of, for example, oil-contaminated sediment and algae. This paper presents the results obtained. It is concluded here that the poor recoveries were due to an inhibition of hydride generation rather than to interference at the atomization stage. 相似文献
54.
55.
A fast electrooptic modulation in a polymer waveguide using a ferroelectric liquid crystal has been proposed. In this device, the surface stabilized ferroelectric liquid crystal and the soft mode ferroelectric liquid crystal are used as an active material on the passive polymer waveguide, and electrooptic switching is realized by controlling the total reflection at the polymer waveguide-liquid crystal interface. The response time is of the order of several microseconds. The analogue electrooptic modulation in the waveguide is realized using the field induced linear molecular tilt of the electroclinic effect in the soft mode ferroelectric liquid crystal. 相似文献
56.
对水热处理后得到的USY沸石作进一步的酸处理以及采用改进的氟硅酸盐溶液骨架富硅工艺,分别得到了经XPS剖面分析证实为铝分布均匀的超稳Y沸石HAY-Ⅰ和HAY-Ⅱ。IR分析表明,在酸处理过程中从USY沸石中去掉的那部分非骨架铝类与3690cm~(-1)处羟基有关,仍残留在HAY-Ⅰ沸石中的那部分非骨架铝类与3670cm~(-1)和3600cm~(-1)处羟基有关。XRD和化学分析表明HAY-Ⅰ沸石仍含有约50%的非骨架铝类,而HAY-Ⅱ沸石则基本上不含非骨架铝类,HAY-Ⅱ沸石还显示更高的结晶保留度。DTA分析表明,HAY-Ⅰ和HAY-Ⅱ两种沸石的热稳定性均高于USY沸石。 相似文献
57.
In this paper, we consider a real-life vehicle routeing problem that occurs in a major Swiss company producing pet food and flour. In contrast with usual hypothetical problems, a large variety of restrictions has to be considered. The main constraints are relative to the accessibility and the time windows at customers, the carrying capacities of vehicles, the total duration of routes and the drivers' breaks. To find good solutions to this problem, we propose two heuristic methods: a fast straightforward insertion procedure and a method based on tabu search techniques. Next, the produced solutions are compared with the routes actually covered by the company. Our outcomes indicate that the total distance travelled can be reduced significantly when such methods are used. 相似文献
58.
59.
The Stokes motions of three-dimensional screw-sensed slender particles in a homogeneous shear field are investigated, including the effects of buoyancy. Conclusions are drawn about the possibility of achieving a separation of mixtures of right- and left-handed particles. The linearity of the Stokes equations allows complex flows to be solved by adding the effects of the several terms which describe the flow in which the particle is immersed. The homogeneous shear flow considered here consists of three such terms; solutions for a series of 12 unit motions are sufficient to determine the hydrodynamic resistance tensors. The forces and torques experienced by screw-sensed particles are calculated from these 51 resistance tensors, using slender-filament theory. The results allow an estimate of the range of buoyancy parameters for which gravitational sedimentation can be neglected. The fundamental component of the particle motion is a rotation, at approximately the same angular velocity as that of the fluid. Superimposed on this are variations, of large period, in the particle orientation. A phase plane analysis is used to find the terminal orientations. Very long calculation times are required for the phase portrait. An approximate method based on azimuthally-averaged equations is developed to avoid the requirements for long time integration. 相似文献
60.
After briefly renewing toxicological data on germanium compounds, the authors report on the subchronic oral toxicity of carboxyethylgermanium sesquioxide in rats. During six months, male and female animals received 1 g kg?1. day?1. No particular toxic symptoms, and no behaviour problems except a small decrease of body weight in male rats, at the end of the six-month experimentation period, were observed. A significant decrease of erythropoiesis and some significant changes in leucocyte ratios were demonstrated. The main marked effect was a moderate renal dysfunction characterized by a tubular disease with the presence of cylinders, swelling of tubulus cells and flocculus deposits. Germanium urinary excretion was constant and linked to the received dose. Six months later, no preferential accumulation in organs was evident. 相似文献