Synthesis and structure of unsymmetrical cross-conjugated dienones with thienyl substituents

By condensation of thiophenecarbaldehyde and m-nitrobenzaldehyde with furyl-, thienylmethylenecyclohexanones in basic medium 2-(het)arylmethylene-6-thienylmethylenecyclohexanones were prepared. Under the conditions of acid catalysis analogously built dienones were synthesized containing 5-nitrothiophene fragment. Based on the data of IR and ¹H NMR spectroscopy their E,E-configuration was established.     

用不变速度推导卢瑟福散射公式

通过横向速度变换得到两种不变速度，由此推出卢瑟福散射公式。     

基于自相关的激光编码解算

分析了半自主激光制导武器的激光编码规律，提出了运用自相关技术对激光编码进行解算。通过仿真试验验证，运用该技术可准确预测、精确同步复制敌方激光编码，并形成有效的激光诱饵，达到全程自适应干扰的目的。     

5-(对羧基苯偶氮)-8-羟基喹啉与钍的显色反应及应用

研究了钍与5-(对羧基苯偶氮)-8-羟基喹啉(5-CPAHQ)的显色反应条件:在阳离子表面活性剂十六烷基三甲基溴化铵(CTMAB)存在下,pH4.4-5.4缓冲介质中,形成稳定的橙红色络合物,最大吸收波长为490nm,ε=1.10×105L·mol-1·cm-1,钍在0-9μg/25mL范围内符合比尔定律。用TBP萃淋树脂分离,该方法可用于测定矿石中的微量钍。     

Conducting Materials Based on Thermally Expanded Graphite

The electrical conductivity of composites produced from thermally expanded graphite, isoprene rubber, and polyvinyl chloride plastisol was studied as influenced by the process conditions.     

Target Level Method in Linear Multi-Criterion Problems

We consider the target level method for solving linear multi-criterion maximization problems. The method finds an efficient (Pareto-optimal) vector estimate that is closest in the Chebyshev metric to the target level point specified by the decision maker. The proposed method describes (parametrizes and approximates) the efficient set. In the linear case the number of scalar optimization problems needed to describe the set of efficient vector estimates is substantially reduced. A formula is derived which, under certain conditions, can be used to compute efficient vector estimates without solving any optimization problems. An algorithm based on these results is proposed for two-criterion problems.     

Influence of Conditions of Zinc Selenide Oxidation with Atmospheric Oxygen on the Composition of Volatile Products

The qualitative and quantitative composition of volatile products of zinc selenide oxidation with atmospheric oxygen was determined. The influence of the process conditions on quantitative composition of the volatile products was studied.     

椭圆偏振光实验鉴定的新方法

1用λ/4波片和检偏器鉴定椭圆偏振光存在的缺点 鉴定椭圆偏振光常用的方法是先用检偏器鉴定椭圆偏振光长短轴的方位,再用λ/4波片使之转化成线偏振光,然后用检偏器找到消光位置.