大平面二极管虚阴极振荡器的宽脉冲微波辐射

给出了产生宽脉冲微波辐射的大平面天鹅绒二极管虚阴极振荡器的结构和测试装置，测得了二极管中阴－阳极等离子体的闭合速率为３０～４３ｋｍ／ｓ，获得了微波辐射的最大脉宽为１．５μｓ，产生的微波峰值功率约为１５ＭＷ，频率为０．５ＧＨＺ，指出这种平面二极管型虚阴极振荡器在辐射脉宽，辐射频率和辐射功率三者之间存在着物理上的制约关系，认为同轴型虚阴极振荡器是突破这种制约关系的一个新途径．     

H—空间的覆盖性质及其应用

我们得到了Ｈ－空间闭（开）覆盖性质的几个定理，改进和推广了Ｓｐｅｒｎｅｒ，Ｋｌｅｅ，Ａｌｅｘａｎｄｒｏｆｆ－Ｐａｓｙｎｋｏｆｆ，Ｂｅｒｇｅ，Ｇｈｏｕｉｌａ－Ｈｏｕｒｉ，Ｄａｎｚｅｒ－Ｇｒｕｎｂａｕｍ－Ｋｌｅｅ，Ｋｙ Ｆａｎ，ｓｈｉｈ－Ｔａｎ，Ｈｏｒｖａｔｈ和Ｌａｓｓｏｎｄｅ等人的相应结果。作为应用，我们对ｌ．ｃ．－空间内的下半连续集值映象证明了一个几站不动点定理并且推广吉洪诺夫不动点定理到ｌ．ｃ．     

Determination of Herbicide Residues in Garlic by GC–MS

A rapid multi-residue method has been developed for the determination of 16 herbicides in garlic. The analytical procedure is based on prior microwave heating prevention of the generation of sulfur-containing compounds. The garlic samples which had been pretreated were extracted with acetonitrile and cleaned up by solid-phase extraction. The herbicide residues were detected by gas chromatography–mass spectrometry with selected ion monitoring. The recoveries of 16 herbicides ranged from 69.0 to 105.4% with the relative standard deviations (RSD) below 10.1%. The limit of quantification (LOQ) ranged from 0.003 to 0.015 mg kg^?1.     

Liquid-liquid extraction of protactinium(V) using tri-iso-octylamine

Solvent extraction of protactinium with tri-iso-octyl-amine (TIOA) in xylene, benzene, carbon tetrachloride and chloroform from HCl, HF, HNO₃, HClO₄ and H₂SO₄ media was studied using ²³³Pa as a radiotracer. The extraction efficiencies of protactinium were determined as a function of shaking time, concentrations of mineral acids in aqueous phase, extractant concentrations and diluents in organic phase. The extraction mechanism was discussed. The results show that the extracted species in the organic phase is [(R₃N⁻H)_nPa(OH)_xCl _y ^5−x−y ].     

广义线性回归极大似然估计的强相合性

设有该文第1节所描述的广义线性回归模型,以$\underline{\lambda}_n$和$\overline{\lambda}_n$分别记$\sum\limits_{i=1}^{n}Z_iZ_i^{\prime}$的最小和最大特征根,$\hat{\beta}_n$记$\beta_0$的极大似然估计.在文献[1]中,当\{$Z_i,i\ge1$\}有界时得到$\hat{\beta}_n$强相合的充分条件,在自然联系和非自然联系下分别为$\underline{\lambda}_n\rightarrow\infty$, $(\overline{\lambda}_n)^{1/2+\delta}=O(\underline{\lambda}_n)$（对某$\delta>0$)以及$\underline{\lambda}_n\rightarrow\infty$, $\overline{\lambda}_n=O(\underline{\lambda}_n)$.作者将后一结果改进为只要求$(\overline{\lambda}_n)^{1/2+\delta}=O(\underline{\lambda}_n)$,从而与自然联系情况下的条件达到一致.     

Investigation on laser brazing AA6056 Al alloy to XC18 low-carbon steel

Based on the studies of influence of YAG laser heating conditions for Al alloy melt and steel on wettability,the mechanics of the laser overlap braze welding of 6056 Al and XC18 steel sheet has been investigated.Under the temperature range which is above the melting point of the Al alloy and below the melting point of the steel, two dissimilar metals can be joined by means of laser braze welding. There is no crack observed in the joining area, i.e. Al-Fe intermetallic phase (Fe3Al/FeAl/FeAl3/Fe2Al5) layer formed by solution and diffusion between liquid-solid interface. The temperature range can be defined as the process temperatures of laser braze welding of Al-Fe materials. Selecting a higher laser heating temperature can improve the wettability of Al melt to steel surface, but the intermetallic phase layer is also thicker. When the laser heating temperature is so high that the joining surface of steel is melted, there is a crack trend in the joining area.     

Preparation and characterization of a nanoscale poly(vinyl alcohol) fiber aggregate produced by an electrospinning method

Nanoscale poly(vinyl alcohol) (PVA) fiber (100–500 nm) aggregates were prepared with an electrospinning technique. Additionally, a chemical crosslinking method was used to crosslink the nanoscale PVA fiber aggregates. Differential scanning calorimetry, wide‐angle X‐ray diffraction, and scanning electron microscopy techniques were employed to characterize the PVA fiber aggregates. The different crosslinking densities of the PVA fiber aggregates were obtained through the control of the weight percentage of glyoxal to PVA. The crosslinking densities due to heat treatment and chemical crosslinking were studied. The influence of heat treatment could be neglected in contrast to chemical crosslinking when the curing temperature was 120 °C. The primary factor that affected the crosslinking density was the volume of the chemical crosslinking agent. The results showed that the properly crosslinked PVA fiber aggregates had better antiwater solubility and mechanical properties than the noncrosslinked PVA fiber aggregates. © 2002 Wiley Periodicals, Inc. J Polym Sci Part B: Polym Phys 40: 1261–1268, 2002     

More precise determination of thermal lens focal length for end-pumped solid-state lasers

A method of more precise determination of the focal length of equivalent thermal lens (TL) is presented in this paper. The method is based on the diffraction theory of aberrations. By numerically calculating the optical path difference (OPD) distribution and the Strehl ratio, the focal lengths for “top-hat” pumping and Gaussian pumping are obtained and the equations for the focal lengths are presented by curve fitting. Also the equations for average pump radii are presented. The experiment on a fiber-coupled LD pumped Nd:YAG laser is carried out. The experimental results verify the validity of the method.     

Generalized KKM type theorems in FC-spaces with applications (II)

This paper is a continuum of the preceding paper of author. By applying a coincidence theorem in noncompact FC-space without any convexity structure due to author, a new KKM type theorem is first proved under noncompact setting of FC-spaces. The equivalent relation between the coincidence theorem and the KKM type theorem is also established. As applications of the KKM type theorem, we establish some new existence theorems of solutions for three classes of generalized vector equilibrium problems under noncompact setting of FC-spaces. These theorems improve and generalize many known results in literature.     

人工脑的三维模型及应用

将二维人工脑模型推广到三维，并给出了一个实际应用算例，还将二、三维模型的计算结果进行了对比，发现三维模型的计算效果明显优于二维模型。