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Crystal determination of a complex between 2,6-dimethoxyflavone and perchloric acid revealed that the inclusion compound contains a water of crystallization that participates in hydrogen bonds connecting the perchloric anion and the carbonyl oxygen of the flavone. The torsion angle between the-benzopyrene and the phenyl rings O(1)C(2)C(1)C(6) is –45, which gives a less twisted molecule than the parent molecule or other inclusion compounds with carboxylic acids. A comparative study with these structures shows that the hydrogen bond forces coplanarity between the-benzopyrone and phenyl rings. 相似文献
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J.‐C. Wallet Elies Molins Carlos Miravitlles 《Acta Crystallographica. Section C, Structural Chemistry》2000,56(9):e414-e414
Crystals of a second triclinic modification of the title compound, 2‐(2,6‐dimethoxyphenyl)‐4H‐1‐benzopyran‐4‐one, C17H14O4, were grown from a hot cyclohexane solution. In the molecule, the O—C—C—C torsion angle at the junction between the benzopyran and phenyl rings is 67.6 (3)°. 相似文献
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W. Maniukiewicz E. Molins C. Miravitlles J. -C. Wallet E. M. Gaydou 《Journal of chemical crystallography》1996,26(10):691-694
The 11 adduct of chlorotriphenyltin with 2,6-dimethoxyflavone, (C35H29O4ClSn)Mr=667.78, crystallizes in the triclinic space groupP1 with the following data:a-9.094(2),b=12.369(3),c=14.674(3) Å, =74.78(2), =77.00(2), =73.06(3)°,V=1503.8(4) Å3,Z=2, Mo-K, =9, 8 cm–1,Dc=1.475 g cm–3, F(000)=676,T=293K. The structure was solved by direct-methods and has been refined to a finalR value (l>3(I)) of 0.0301. The flavone coordinates to the tin atom through the carbonyl oxygen atom. The metal center exhibits a trigonal bipyramidal configuration with the three phenyl groups in equatorial positions. 相似文献
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Shashwati Sen DK Aswal Ajay Singh TV Chandrasekhar Rao KP Muthe JC Vyas LC Gupta SK Gupta VC Sahni 《Pramana》2002,58(5-6):867-870
The MgB2 superconductor, synthesized using solid-state and liquid-phase sintering methods, have been characterized for various properties.
The upper critical field, irreversibility line and critical current density have been determined using magnetization data.
The current-voltage characteristics recorded under an applied magnetic field revealed the existence of vortex glass transition.
The surface analysis using X-ray photoelectron spectroscopy shows that MgB2 is sensitive to atmospheric degradation. 相似文献
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In this paper, we revisit some quantum mechanical aspects related to the quantum Hall effect. We consider a Landau type model, paying a special attention to the experimental and geometrical features of quantum Hall experiments. The resulting formalism is then used to compute explicitely the Hall conductivity from a Kubo formula. 相似文献