Isolation and Structure Elucidation of Nortriterpenoids from Schisandra rubriflora

Seven new highly oxygenated nortriterpenoids, rubriflorins D–J ( 1 – 7 ), were isolated from the leaves and stems of Schisandra rubriflora, and their structures were elucidated on the basis of extensive analysis of spectroscopic data. These new compounds feature the opening of ring A compared with related known nortriterpenoids isolated from the genus Schisandra and showed weak activity against HIV‐1.     

卡尔曼滤波紫外光度法同时测定酱油、食醋中的山梨酸和苯甲酸

在酸性条件下，采用乙酸乙酯萃取、Na2HPO4溶液反萃取分离酱汪、食醋中的山梨酸、苯甲酸，卡尔曼滤波法计算结果，并与比值导数波谱法进行比较。结果表明，卡尔曼滤波法较地数波谱法有较高准确度和精密度，并能监测干扰物质存在与否。用于实际样品分析有更高的可靠性。     

HL-2A װ��MW ������������ϵͳ��˿��Դ�����������

The main circuit topology, control hardware and control sequence of the cathode filament power supply for the HL-2A neutral beam heating system was introduced. Feedback control simulation of main circuit of filament power supply is carried out through MATLAB simulation software. It is found that the ripple factor is about 1%when the current is about 1000A, and the ripple coefficient increases to 3% when the current drops to 200A. Without the AC filter reactor in series L₁ and parallel harmonic filter LC in the low level control cabinet, the output current ripple coefficient becomes larger obviously. It shows that L₁ and LC not only absorb harmonic current, but also filter the chopper waveform after AC voltage regulation to make the output waveform smoother.     

从芒果皮中提取果胶的工艺研究

果胶是一种大分子多糖类物质 ,具有良好的胶凝作用 ,用途广泛 ,在国内外市场上的销量很好。 1 990年世界上果胶总产量约 2 5 0 0 0吨 ,而我国 1 990年仅在食品工业上消耗的果胶就达 1 0 0 0吨 ,但国内市场上销售的果胶大部分为进口货[1] 。果胶在我国的生产仍处于开发阶段 ,所以发掘新的提取资源、提高果胶质量、降低果胶生产成本的意义十分重大。目前 ,已有以柑桔皮、向日葵盘、苹果皮、香蕉皮、马铃薯渣为原料提取果胶的研究报道 ,如何从芒果皮中提取果胶却未见报道。芒果在制造罐头和饮料中副产大量下脚料———芒果皮 ,未能得到充分利用…     

Chiral Salen Manganese Complex Immobilized on SBA-15： A New Heterogenized Enantioselective Catalyst for the Epoxidation of Alkenes

Jacobsen‘s catalyst was immobilized onto SBA-15 by multi-step grafting, and this heterogenized catalyst exhibited comparable catalytic performance with the corresponding homogeneous counterpart for the epoxidation of alkenes, and the catalyst could be recycled effectively several times.     

麻黄中伪麻黄碱在小鼠组织中的分布研究

为了解麻黄(Herba ephedrae,简称HE)中伪麻黄碱(Pseudoephedrine,简称PE)在小鼠脑、肺、心、肝、肾的分布变化,探讨HE的归经,用GC-MS/SIM法,分析了用药后30、60、120 min PE在小鼠脏器分布量。结果表明,PE于不同时间点在小鼠脏器的分布由多到少的顺序是:30 min时,肺脏(肾脏、肝脏、脑),心脏;60 min时,肾脏,心脏(肝脏),脑,肺脏;120 min时,脑,肾脏,心脏,肝脏(肺脏)。本试验从PE在小鼠体内脏器的分布量初步反映了HE的归经趋势。     

硅氧化合物化学蒸气沉积法精细调变沸石分子筛

本文报告了用化学蒸气沉积法精细调变沸石孔径的结果，着重考察了正硅酸乙酯和六甲基硅醚沉积条件的关系。间二甲苯和均三甲苯的吸附动力学实验表明，用Ｓｉ－（ＯＥｔ）４制得的ＳｉＨβ和ＳｉＨＺＳＭ－５上的吸附速率及吸附量明显下降，证实沸石的孔口得到了调变。正己烷的吸附等温线和异丙醇探针反应，沸石孔容和孔道内酸性未受孔口调变的影响。结果还表明Ｓｉ（ＯＥｔ）４未进入沸石孔道，而六甲基硅醚分子则进入Ｈβ沸石孔道，