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Single crystals of nickel(II) divanadium(V) ditellurium(IV) decaoxide, NiV2Te2O10, were synthesized via a transport reaction in sealed evacuated silica tubes. The compound crystallizes in the triclinic system (space group P). The Ni atoms are positioned in the 1c position on the inversion centre, while the V and Te atoms are in general positions 2i. The crystal structure is layered, the building units within a (010) layer being distorted VO6 octahedra and NiO6 octahedra. The metal–oxide layers are connected by distorted TeO4E square pyramids (E being the 5s2 lone electron pair of TeIV) to form the framework. The structure contains corner‐sharing NiO6 octahedra, corner‐ and edge‐sharing TeO4E square pyramids, and corner‐ and edge‐sharing VO6 octahedra. NiV2Te2O10 is the first oxide containing all of the cations NiII, VV and TeIV. 相似文献
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Terry F. Hamilton Jussi Jernströem Roger E. Martinelli Steven R. Kehl Mats Eriksson Ross W. Williams Marek Bielewski Ariel N. Rivers Thomas A. Brown Scott J. Tumey Maria Betti 《Journal of Radioanalytical and Nuclear Chemistry》2009,282(3):1019-1026
Runit Island on Enewetak Atoll was very heavily impacted by the U.S. nuclear testing campaign in the northern Marshall Islands (1946–58). The primary source of contamination on Runit Island was the 1958 Quince safety test where a large quantity of device plutonium (Pu) was scattered over the area near the GZ. A second low-yield device was detonated on the same site 10 days later, further disturbing the soil and leaving behind a very heterogeneous pattern of contamination including milligram-size particles of plutonium. A limited cleanup of the Fig-Quince zone was carried out in 1979. During this period, the effectiveness of the cleanup operations was primarily evaluated on the basis of bulk soil concentration data with little consideration given to the heterogeneity and long-term material-, biological-, and environmental-specific impacts of residual high activity (hot) particle contamination. The aim of the present study was twofold; (i) to characterize the levels and distribution of residual contamination in the Fig-Quince zone, and (ii) to develop pertinent data on the frequency distribution, elemental and isotopic composition, and physico-chemical properties of hot particles isolated from surface soils from Fig-Quince with a view towards providing recommendations on the future management and possible cleanup of the site. Today, Runit Island remains under an administrative quarantine. 相似文献
135.
Mats Boman 《BIT Numerical Mathematics》2006,46(2):249-260
We consider the orthogonal L2-projection P onto continuous finite element spaces. We prove estimates for P in a weighted Lp-norm and use these to prove corresponding approximation properties.
AMS subject classification (2000) 65N60, 35K85 相似文献
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We prove new sharper estimates of solutions to the -corona problem in strictly pseudoconvex domains; in particular we show that the constant is independent of the number of
generators. We also obtain sharper estimates for solutions to the BMOA corona problem. The proofs also lead to new results about the Taylor spectrum of analytic Toeplitz operators on and BMOA.
Received: 28 August 1998 / in final form: 9 February 1999 相似文献
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