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991.
The magnetization reversal behaviour for SmCo6.8Zr0.2 and SmCo6.8Zr0.2/α-(Fe,Co) nanocrystalline magnets at low temperature 下载免费PDF全文
This paper reports that the SmCo 6.8 Zr 0.2 nanocrystalline permanent magnets and SmCo 6.8 Zr 0.2 /α-(Fe,Co) nanocomposite permanent magnets are successfully produced by mechanical alloying and subsequently annealing at 700 C for 10 minutes.The x-ray diffraction results show that the phase structure of SmCo 6.8 Zr 0.2 nanocrystalline permanent magnets is composed of SmCo 7 phase and SmCo 6.8 Zr 0.2 /α-(Fe,Co) nanocomposite permanent magnets is composed of SmCo 7 and α-(Fe,Co) phases.The mechanism of magnetization reversal is mainly controlled by inhomogeneous domain wall pinning in SmCo 6.8 Zr 0.2 and SmCo 6.8 Zr 0.2 /α-(Fe,Co) magnets.The inter-grain exchange interaction at low temperature is investigated,which shows that the inter-grain exchange interaction of SmCo 6.8 Zr 0.2 /α-(Fe,Co) magnets increases greatly by the decrease of the measured temperature.According to Δm irr-H/H cj,Δm rev-H/H cj and χ irr-H/H cj curves at room temperature and 100 K,the changes of irreversible and reversible magnetization behaviours of SmCo 6.8 Zr 0.2 and SmCo 6.8 Zr 0.2 /α-(Fe,Co) magnets with the decreasing temperature are analysed in detail.The magnetic viscosity and the activation volume of SmCo 6.8 Zr 0.2 and SmCo 6.8 Zr 0.2 /α-(Fe,Co) magnets at different temperatures are also studied. 相似文献
992.
白光LED用Ca_8Mg(SiO_4)_4Cl_2:Eu~(2+),Dy~(3+)发光粉的发光性能 总被引:1,自引:2,他引:1
采用高温固相法合成了白光LED用Ca8Mg(SiO4)4Cl2:Eu和Ca8Mg(SiO4)4Cl2:Eu,Dy绿色发光粉。研究发现:共掺Dy可以明显地提高Ca8Mg(SiO4)4Cl2:Eu发光粉的发光性能,表明Dy3+和Eu2+之间存在着能量传递过程。当Dy3+的最佳掺杂摩尔分数为0.02时,发光粉505nm处绿光发射的强度约提高12%。通过对Dy3+和Eu2+光谱特性的分析,Dy3+和Eu2+之间的能量传递机制可归因于无辐射交叉弛豫。 相似文献
993.
994.
大蓟多糖提取分离及含量测定 总被引:1,自引:1,他引:1
用水提-醇沉法从大蓟中提取多糖,脱脂、去蛋白,经冷冻干燥后得到粗多糖。通过苯酚-硫酸法测定糖的含量,粗多糖得率为6.5%。再采用DEAE-纤维素离子交换柱层析进一步分离纯化,得到5个次级组分DJ1,DJ2,DJ3,DJ4和DJ5。其中得率最高的是DJ2组分,为8.06‰。 相似文献
995.
996.
建立漂移-扩散模型来模拟敏化电池的电荷分离过程.该模型能够计算在稳态和非稳态条件下光生电子的多步受限扩散及其与电子受体的复合反应.通过对电池的电流-电压曲线的数值模拟,优化了电池的薄膜厚度并获得了最大的光电转换效率.发现膜厚的增加降低了电荷收集效率,但有利于提高电子注入流率,光电流的输出正是受控于这两个因素.复合速率常数严重影响了膜厚优化的结果.较厚的薄膜适合于电子复合被充分抑制的电池,而较薄的薄膜有利于降低快复合电池的电子复合损失.在开路条件下,膜厚的提高会减小电子浓度,在造成光电压的降低的同时会提高电子寿命. 相似文献
997.
通过在三维还原氧化石墨烯孔径中原位生长ZIF-8纳米粒子,制备了三维金属有机骨架/石墨烯催化剂.这种ZIF-8/rGO纳米复合材料同时具有介孔和微孔,并且拥有高比表面积和大量催化位点,是生物质转化的理想催化剂.将纤维素溶解于氢氧化钠水溶液中,在水热条件下,使用这种催化剂,纤维素可以被充分降解转化.纤维素转化率可以达到100%,其主要产物是甲酸,产率最高可达93.66%.催化剂还可以被回收,重复使用依然具有很好的催化效果. 相似文献
998.
A filter construction technique is presented for enhanced defect identification in rotary machine systems. Based on the generalized harmonic wavelet transform, a series of sub-frequency band wavelet coefficients are constructed by choosing different harmonic wavelet parameter pairs. The energy and entropy associated with each sub-frequency band are then calculated. The filtered signal is obtained by choosing the wavelet coefficients whose corresponding sub-frequency band has the maximum energy-to-entropy ratio. Experimental studies using rolling bearings that contain different types of structural defects have confirmed that the developed new technique enables high signal-to-noise ratio for effective machine defect identification. 相似文献
999.
Detailed model, analysis and design technique are presented for simulating a high-speed polymer Mach-Zehnder interferometer (MZI) electro-optic switch with push-pull dual driving electrodes and rib waveguides. The novel formulas of the time-domain response are derived. Thorough optimization and simulation for the designed device are performed. The total length of the basic function unit of the switch is about 5049 μm, the push-pull switching voltage is 2.23 V, the switching time is 18.1 ps, and the insertion loss and crosstalk are less than 2.64 and −30 dB, respectively, within the range of the operation wavelength from 1534 to 1566 nm. These results are in good agreement with those obtained from the beam propagation method (BPM). 相似文献
1000.
Min Wu Yan Lv Zhengping Fu Jiao Xu Ting Guo Yongxun Zhao 《Applied Surface Science》2010,256(23):7125-9486
The simultaneous Ag loaded and N-doped TiO2 hollow nanorod arrays with various contents of silver (Ag/N-THNAs) were successfully synthesized on glass substrates by one-pot liquid phase deposition (LPD) method using ZnO nanorod arrays as template. The catalysts were characterized by Raman spectrum, field-emission scanning electron microscopy (FESEM), high-resolution transmission electron microscope (HRTEM), ultraviolet-vis (UV-vis) absorption spectrum and X-ray photoelectron spectroscopy (XPS). The results suggest that AgNO3 additive in the precursor solutions not only can promote the anatase-to-rutile phase transition, but also influence the amount of N doping in the samples. The photocatalytic activity of all the samples was evaluated by photodegradation of methylene blue (MB) in aqueous solution. The sample exhibited the highest photocatalytic activity under UV light illumination when the AgNO3 concentration in the precursor solution was 0.03 M, due to Ag nanoparticles acting as electron sinks; When the AgNO3 concentration was 0.07 M, the sample performed best under visible light illumination, attributed to the synergetic effects of Ag loading, N doping, and the multiphase structure (anatase/rutile). 相似文献