二色补血草不同部位总黄酮含量的测定

采用分光光度法测定了二色补血草花、根、茎、叶总黄酮的含量,分别为35.5869、23.5367、24.7081、30.5378mg/g.RSD为0.1016%-0.1410%,稳定性R＞97.5%,平均回收率96.38%-100.2%.     

The general integral expressions for on-axis nonparaxial vectorial spherical waves diffracted at a circular aperture

Based on the vectorial Rayleigh-Sommerfeld integrals, the general propagation integral expressions for on-axis nonparaxial vectorial spherical wave diffracted at a circular aperture are derived. The results are strict integral formulae for the light field on the axis, valid for either strong or weak focusing, both far and near zones, and for the systems in which the size of the aperture is comparable to or smaller than the wavelength. Thus, it has the advantage for general application. For convergent spherical waves, the numerical calculation results are compared with those obtained by using the integral formulae of scalar paraxial approximation and scalar nonparaxial approximation, confirming the consistence in the situation of scalar approximation.     

HL-2A装置中性束发射光谱 诊断系统的研制与测试

在HL-2A装置上完成了一套32通道束发射诊断系统(BES),可对径向r=12~44cm, 极向-7.5~+7.5cm二维空间范围内的长波长()电子密度扰动信息进行测量,其时间分辨率达到0.5ms,空间分辨率1~2cm。系统由内置于真空室的非对称镜头组、传输光纤、高性能探测器模块以及辅助的冷却和真空设备构成。系统的噪声在低频时(f<100kHz)主要由散粒噪声贡献,在较高频率时由散粒噪声和e噪声共同决定。在典型的HL-2A装置放电模式中,对于200kHz以下的扰动,该系统的信噪比(SNR)均大于3。     

含m—增生算子或￠—伪压缩映象具误差的Ishikawa迭代的收敛性问题

主要研究了m-增生算子以及￠-伪压缩映象的分别带两种误差的Ishikawa迭代序列的收敛性问题,推广了Osilike等人的相关结果。     

Palladium nanoparticles/wool keratin-assisted carbon composite-modified flexible and disposable electrochemical solid-state pH sensor

Several p H-dependent processes and reactions take place in the human body;hence,the p H of body fluids is the best indicator of disturbed health conditions.However,accurate and real-time diagnosis of the p H of body fluids is complicated because of limited commercially available p H sensors.Hence,we aimed to prepare a flexible,transparent,disposable,userfriendly,and economic strip-based solid-state p H sensor using palladium nanoparticles(Pd NPs)/N-doped carbon(NC)composite material.The Pd NPs/NC composite material was synthesized using wool keratin(WK)as a precursor.The insitu prepared Pd NPs played a key role in the controlled switching of protein structure to the N-doped carbon skeleton withπ–πarrangement at the mesoscale level,which mimics the A–B type polymeric structure,and hence,is highly susceptible to H+ions.The optimized carbonization condition in the presence of Pd NPs showed that the material obtained using a modified Ag/Ag Cl reference electrode had the highest p H sensitivity with excellent stability and durability.The optimized p H sensor showed high specificity and selectivity with a sensitivity of 55 m V/p H unit and a relative standard deviation of 0.79%.This study is the first to synthesize Pd NPs using WK as a stabilizing and reducing agent.The applicability of the sensor was investigated for biological samples,namely,saliva and gastric juices.The proposed protocol and material have implications in solid-state chemistry,where biological material will be the best choice for the synthesis of materials with anticipated performance.     

THz波的产生及探测技术

THz技术是20世纪90年代发展起来的一门新兴学科,本文较为详细地介绍了目前产生THz波的主要方法、原理以及探测THz波的主要手段和机理.     

Top介子在高能正负电子对撞机上的产生

在顶色辅助的人工色(TC2)模型框架下,研究了中性top介子和顶夸克的联合产生过程e+e–→ttπ0t.结果显示此过程的产生截面比标准模型和最小超对称标准模型中e+e–→ttH过程的产生截面都要大.在TC2模型合理的参数空间内,其产生截面可达20fb.通过此过程可在将来的对撞机上探测中性top介子.     

Bacterial Cellulose Nanopaper as Reinforcement for Polylactide Composites: Renewable Thermoplastic NanoPaPreg

Bacterial cellulose (BC) is often regarded as a prime candidate nano‐reinforcement for the production of renewable nanocomposites. However, the mechanical performance of most BC nanocomposites is often inferior compared with commercially available polylactide (PLLA). Here, the manufacturing concept of paper‐based laminates is used, i.e., “PaPreg,” to produce BC nanopaper reinforced PLLA, which has been called “nanoPaPreg” by the authors. It is demon­strated that high‐performance nanoPaPreg (v_f = 65 vol%) with a tensile modulus and strength of 6.9 ± 0.5 GPa and 125 ± 10 MPa, respectively, can be fabricated. It is also shown that the tensile properties of nanoPaPreg are predominantly governed by the mechanical performance of BC nanopaper instead of the individual BC nanofibers, due to difficulties impregnating the dense nanofibrous BC network.

     

Lewis acid-catalyzed novel [3+2] cycloaddition of methylenecyclopropanes with activated aldehydes or ketones

Methylenecyclopropanes react with activated aldehydes or ketones in the presence of various Lewis acids to give the corresponding [3+2] cycloaddition products having tetrahydrofuran (THF) skeleton in good yields and in some cases with high stereoselectivity.