LiNi1-xAlxO2(x=0～1.0)固溶体结构的XRD研究

利用溶胶凝胶法制备了新型锂离子二次电池正极材料LiNi_1-xAl_xO₂(x=0,0.1～1.0)固溶体,X射线衍射结果表明,在0≤x≤1范围内,材料均为具有α-NaFeO₂型结构的LiNi_1-xAl_xO₂固溶体单相.随着Al固溶量的增加,晶胞参数发生变化,a轴缩短,c/a比增大,晶胞体积V₀减小,材料的层状属性更加明显.     

Long Excursions of a Random Walk

In Csáki et al. ⁽¹⁾ and Révész and Willekens⁽⁹⁾ it was proved that the length of the longest excursion among the first n excursions of a plane random walk is nearly equal to the total sum of the lenghts of these excursions. In this paper several results are proved in the same spirit, for plane random walks and for random walks in higher dimensions.     

线性空间中向量极值问题的最优性条件

文 [1]建立了线性拓扑空间中向量极值问题的广义 Kuhn- Tucker条件和 L agrange乘子存在定理 .本文将在线性空间中讨论这方面问题 ,首先在线性空间中建立了次似凸向量值映射的择一定理 ,进而得出序线性空间中向量极值问题的最优性条件及其标量化定理 .     

Mass transport characteristics and chromatographic behavior of preparative electrochromatography on hydroxyapatite.

Introducing an electric field into chromatography on hydroxyapatite (HAP) was attempted in order to enhance mass transfer and separation performance. A membrane spaced multicompartment electrolyzer was developed for electrochromatography on HAP. The high performance of liquid transport by electroosmotic flux was identified and described in terms of dynamic electroosmotic pressure. The application of the electric field resulted in an improved adsorption of bovine serum albumin as shown by the breakthrough curve as function of the electric field. An improved elution was also obtained in the presence of the electric field. The results show that electroosmosis is a powerful tool of liquid transport and dispersion in a packed bed of fine particles and has potential in the large-scale chromatography of biological molecules.     

高功率准连续激光二极管抽运的Q开关内腔倍频固体激光器的研究

对高功率准连续激光二极管抽运的Q开关内腔倍频Nd:YAG和Nd:YVO4激光器进行了实验研究,分别获得了输出功率为3．5W和3．2W,输出波长为532nm的激光脉冲,其重复率达22kHz。     

基于模糊综合评判方法的DEA模型

利用数据包络分析和多目标规划的有关理论,对模糊综合评判方法进行进一步探讨,给出一个建立在模糊综合评判过程基础上的DEA模型,该方法不仅能够增强模糊综合评判结果的客观性,更重要的是它可以找出模糊综合评判中较差单元无效的原因,并能为较差单元的改进提供许多有用的信息。     

关于参数设计的一个注记

本文提出了参数设计中方差估计的一种新方法 -非参数估计方法 ,用以代替田口的信噪比中的方差估计。实例表明 ,该方法不但可以对因子进行分类 ,而且可以进行模型拟合的检查     

Hydrothermal growth of boron nitride microcrystals

Boron nitride (BN) crystals with size of several micrometers have been successfully synthesized by hydrothermal method. The reactants used in our experiments were boric acid (H₃BO₃), sodium azide (NaN₃) and white phosphor (P). The samples were characterized by X‐ray diffraction (XRD), Fourier transformation infrared spectroscopy (FTIR), selective area electron diffraction (SAED). It is found that the existence of Cl^‐ in the reaction mixture has much effect on the synthesis of BN. (© 2005 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim)     

Cl+HN3产生NCl(a1Δ)和NCl(b1∑)的实验研究

对利用微波放电直接解离Cl2生成Cl, Cl与HN3反应生成NCl(a1Δ )和NCl(b1∑)的过程进行了实验研究。得到了较强的NCl(a1Δ 和NCl(b1∑)自发辐射光谱,考察了Cl2流量和He/Cl2配比对NCl(a1Δ 和NCl(b1∑)生成的影响。发现对于一定的He流量,Cl2流量对NCl(a1Δ 和NCl(b1∑)生成的影响存在一最佳范围,而最佳He/Cl2配比不是一定值,而是随He流量升高而变大,在实验所考察的He流量范围（5~40 L/min）内,最佳He/Cl 2配比在30∶1~100∶1之间。     

光纤制导双向传输系统

光纤制导战术导弹是一种精确制导武器,它主要用于远距离打击敌方的高价值目标,光纤制导战术导弹具有射程远,抗电磁干扰,隐蔽发射,图像制导等一系列优点,因而受到军方的高度重视并得到迅速的发展,光纤双向传输系统是光纤制导导弹系统中一个重要标志性的组成部分。本文详细地介绍弛光纤制导双向传输系统的特点,构成及工作原理。