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131.
132.
Lejeune C Coelho C Bonhomme-Coury L Azaïs T Maquet J Bonhomme C 《Solid state nuclear magnetic resonance》2005,27(4):242-246
We show that it is possible to efficiently transfer magnetization from 31P to 29Si, using variable amplitude CP MAS experiment. This experiment is demonstrated by using Si5O(PO4)6, the synthesis protocol of which is described. From the obtained results, we show that the experiment allows the spectral edition of 29Si spectra from 31P→29Si CP, enabling the studies of derivatives involving Si–O–P linkages, such as phosphosilicate glasses, microporous silicoaluminophosphates (SAPO) and bioactive phosphosilicates. 相似文献
133.
Driss?BoussaoudEmail author Judith?Tanné-Gariépy Thierry?Wannier Eric?M?Rouiller 《BMC neuroscience》2005,6(1):67
Background
The lateral premotor cortex plays a crucial role in visually guided limb movements. It is divided into two main regions, the dorsal (PMd) and ventral (PMv) areas, which are in turn subdivided into functionally and anatomically distinct rostral (PMd-r and PMv-r) and caudal (PMd-c and PMv-c) sub-regions. We analyzed the callosal inputs to these premotor subdivisions following 23 injections of retrograde tracers in eight macaque monkeys. In each monkey, 2–4 distinct tracers were injected in different areas allowing direct comparisons of callosal connectivity in the same brain. 相似文献134.
135.
Thierry Monteil 《Journal of statistical physics》2004,114(5-6):1619-1623
A planar polygonal billiard $\mathcal{P}$ is said to have the finite blocking property if for every pair (O, A) of points in $\mathcal{P}$ there exists a finite number of “blocking” points B 1,...,B n such that every billiard trajectory from O to A meets one of the B i 's. As a counter-example to a theorem of Hiemer and Snurnikov, we construct a family of rational billiards that lack the finite blocking property. 相似文献
136.
137.
Henry-dit-Quesnel A Toupet L Pommelet JC Lequeux T 《Organic & biomolecular chemistry》2003,1(14):2486-2491
The synthesis of difluoromethylphosphonates is becoming difficult due to environmental protective laws restricting the use of HCFCs and CFCs as starting chemicals. To circumvent this limitation, we report the preparation of a thioether as a new source of the lithiodifluoromethylphosphonate. This methodology avoiding the use of HCFCs involves a selective fluorination of sulfide followed by a thiaphilic addition of an organometallic reagent, which offers an alternative route to obtain phosphonodifluoromethyl carbanion. A contrasted reactivity, due to a medium effect, was also noted which allows addition of a wide range of electrophiles including nitroalkenes and DMF to thioethers. 相似文献
138.
Thierry?De?PauwEmail author Robert?Hardt 《Calculus of Variations and Partial Differential Equations》2003,17(4):405-442
We consider Plateau type variational problems related to the size minimization of rectifiable currents. We realize the limit of a size minimizing sequence as a stationary varifold and a minimal set. Other examples of functionals to be minimized include the integral over the underlying carrying set of a power q of the multiplicity function, with
.Because minimizing sequences may have unbounded mass we make use of a more general object called a rectifiable scan for describing the limit. This concept is motivated by the possibility of recovering a flat chain from a sufficiently large collection of its slices. In case the given boundary is smooth and compact, the limiting scan has finite mass and corresponds to a rectifiable current.Received: 11 February 2002, Accepted: 16 June 2002, Published online: 17 December 2002Mathematics Subject Classification (2000):
49Q15, 28A75Thierry De Pauw: The research of the first author was supported by a Marie Curie fellowship of the European Community program Human Potential under contract HMPF-CT-2001-01235Robert Hardt: The research of the second author was partially supported by NSF grant DMS-0072486 相似文献
139.
Robert Morel Ariel BrenacCéline Portemont Thierry DeutschLucien Notin 《Journal of magnetism and magnetic materials》2007
Magnetic anisotropy has been measured in multiply twinned, icosahedral cobalt clusters. It is found that the low-temperature magnetization of deposited cluster layers is well defined with the Stoner–Wohlfarth model by averaging over clusters with a range of anisotropy energy. Anisotropy energy calculation based on Néel's pair model shows that the icosahedral structure and the layer-by-layer growth of the clusters induce oscillations of the magnetic anisotropy as a function of the filling of the outer surface of the particle. The magnetization measurement at room temperature indicates a weakly correlated cluster glass, as deduced from the approach to saturation that is well described with 2D random anisotropy model. 相似文献
140.
In this paper, we consider the complex Ginzburg–Landau equation ${u_t = e^{i\theta} [\Delta u + |u|^\alpha u] + \gamma u}$ on ${\mathbb{R}^N}$ , where ${\alpha > 0,\,\gamma \in \mathbb{R}}$ and ${-\pi /2 < \theta < \pi /2}$ . By convexity arguments, we prove that, under certain conditions on ${\alpha,\theta,\gamma}$ , a class of solutions with negative initial energy blows up in finite time. 相似文献