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11.
J. L. Vučina 《Journal of Radioanalytical and Nuclear Chemistry》1996,214(1):29-39
The effect of the preparation conditions on the in vitro stability of99mTc (Sn)-pyrophosphate kit solution has been examined. To extend the shelf-life of the preparation, different methods of protection were tested. Nitrogen purging stabilizes the kit for at least 6 h after labeling when the content of99mTc-pertechnetate raises to about 5%. However, this method is ineffective in the presence of hydrogen peroxide. The protecting ability of two chemicals was also determined. Gentisic acid gave good results. In the presence of 50 g of gentisic acid per ml of the kit the content of pertechnetate was 1–2% throughout the examined time interval. To eliminate the influence of hydrogen peroxide (6 g per ml of the kit) about 100 g of gentisic acid is needed. N, N-diphenyl-p-phenylenediamine (DPPD) performs some protecting effect only when used in the samples protected by nitrogen purging. However its protecting ability is lower that in the case of gentisic acid. 相似文献
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J. Vučina S. Milenković V. Šćepanović 《Journal of Radioanalytical and Nuclear Chemistry》1988,120(1):205-210
The possible effects of several protecting procedures on the quality of99mTc eluates were investigated. The content of99Mo in the eluates (99Mo breakthrough) was expressed in (%) with respect to the total adsorbed99Mo radioactivity and in () i.e. as the ratio of99Mo and99mTc radioactivities in each particular eluate. The radiochemical purity was expressed in (%) of99mTc(VII) in the eluates. The content of Al3+ and Cu2+ as chemical impurities was also determined. 相似文献
14.
Mobilities of H+ and H? in He and in H2, and of H+2 and H+3 in He, are calculated from ion-neutral potentials derived from theory and ion-beam scattering. Agreement with experiment is reasonable except for H? in H2 and H+2 in He, which present unexplained puzzles. 相似文献
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Dang Vu Giang 《Analysis Mathematica》1991,17(2):133-140
, . . [1] - . . 相似文献
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A general, practical and efficient one-pot synthesis of cyclic enecarbamates is described. The protocol proceeds via reduction of lactam carbamate with Super-Hydride®, followed by in situ dehydration with trifluoroacetic anhydride (TFAA) and diisopropylethylamine (DIPEA). 相似文献
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Matilda Vojnović Ana J. Šetrajčić-Tomić Siniša M. Vučenović Jovan P. Šetrajčić 《Optical and Quantum Electronics》2018,50(4):198
Recent research in nano-optical engineering and in nanomedicine as well, seeks for methods of construction of various types of nano-markers, nano-carriers, and ways to deliver drugs to the exactly determined regions of body. In this process it is important to find methods of recognition of certain types of molecules. It is obvious that optical recognition would be the easiest and the most effective way to do it. Our research presents a model of a molecular ultrathin crystalline film and generated exciton system inside it and corresponding methodology of analysis of their optical characteristics. Properties of these spatially very restricted structures are very sensitive to their surrounding surfaces. Using the two-time Green’s functions adapted for crystalline structures with symmetry breaking, and graphical-numerical software, we have calculated the energy spectra and possible exciton states. We have shown that the appearance and the presence of localized states on the surfaces and in the boundary layers of the film depend on the thickness of the film and the film surroundings, presented through the perturbation of parameters on surfaces. Optical properties in these structures demonstrate discrete and very selective resonant absorption spectra, depending on the perturbation on their surfaces. 相似文献